JPS58180460A - ニトロ化方法 - Google Patents

ニトロ化方法

Info

Publication number
JPS58180460A
JPS58180460A JP57064202A JP6420282A JPS58180460A JP S58180460 A JPS58180460 A JP S58180460A JP 57064202 A JP57064202 A JP 57064202A JP 6420282 A JP6420282 A JP 6420282A JP S58180460 A JPS58180460 A JP S58180460A
Authority
JP
Japan
Prior art keywords
catalyst
reaction
benzene
gas phase
composite oxide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP57064202A
Other languages
English (en)
Japanese (ja)
Other versions
JPH0422897B2 (enExample
Inventor
Hiroshi Sato
洋 佐藤
Shuzo Nakamura
中村　収三
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sumitomo Chemical Co Ltd
Original Assignee
Sumitomo Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sumitomo Chemical Co Ltd filed Critical Sumitomo Chemical Co Ltd
Priority to JP57064202A priority Critical patent/JPS58180460A/ja
Priority to DE8383302083T priority patent/DE3360768D1/de
Priority to EP83302083A priority patent/EP0092372B1/en
Priority to US06/485,453 priority patent/US4551568A/en
Publication of JPS58180460A publication Critical patent/JPS58180460A/ja
Publication of JPH0422897B2 publication Critical patent/JPH0422897B2/ja
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0093—Microreactors, e.g. miniaturised or microfabricated reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063—Titanium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/066—Zirconium or hafnium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00824—Ceramic
    • B01J2219/00826—Quartz
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00781—Aspects relating to microreactors
    • B01J2219/00819—Materials of construction
    • B01J2219/00835—Comprising catalytically active material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24—Chromium, molybdenum or tungsten

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP57064202A 1982-04-16 1982-04-16 ニトロ化方法 Granted JPS58180460A (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP57064202A JPS58180460A (ja) 1982-04-16 1982-04-16 ニトロ化方法
DE8383302083T DE3360768D1 (en) 1982-04-16 1983-04-13 Process for nitration of benzene
EP83302083A EP0092372B1 (en) 1982-04-16 1983-04-13 Process for nitration of benzene
US06/485,453 US4551568A (en) 1982-04-16 1983-04-15 Process for nitration of benzene

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP57064202A JPS58180460A (ja) 1982-04-16 1982-04-16 ニトロ化方法

Publications (2)

Publication Number Publication Date
JPS58180460A true JPS58180460A (ja) 1983-10-21
JPH0422897B2 JPH0422897B2 (enExample) 1992-04-20

Family

ID=13251241

Family Applications (1)

Application Number Title Priority Date Filing Date
JP57064202A Granted JPS58180460A (ja) 1982-04-16 1982-04-16 ニトロ化方法

Country Status (4)

Country Link
US (1) US4551568A (enExample)
EP (1) EP0092372B1 (enExample)
JP (1) JPS58180460A (enExample)
DE (1) DE3360768D1 (enExample)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003506340A (ja) * 1999-07-29 2003-02-18 メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフトング 静止型マイクロミキサー内でのニトロ化
JP2003506339A (ja) * 1999-07-29 2003-02-18 メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフトング スタティックマイクロミキサーにおけるフリーデル−クラフツアシル化方法
KR101183822B1 (ko) * 2009-12-18 2012-09-19 한국화학연구원 고체 산촉매를 이용한 니트로파라핀의 제조방법
WO2013025061A3 (ko) * 2011-08-17 2013-05-30 한국화학연구원 기체상 니트로화 반응에 의한 니트로파라핀의 제조방법
KR101282734B1 (ko) * 2011-08-17 2013-07-05 금호석유화학 주식회사 고체산 촉매를 이용한 니트로파라핀의 제조방법

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4754083A (en) * 1986-04-24 1988-06-28 Amoco Corporation Para selectivity in catalyzed disubstitutions of monosubstituted benzenes containing meta-directing substituents
JPH0249755A (ja) * 1988-05-18 1990-02-20 Sumitomo Chem Co Ltd ニトロベンゼン類の製造法
US5354924A (en) * 1988-06-22 1994-10-11 Olin Corporation Process for the production of dinitrotoluene
US5488187A (en) * 1988-06-22 1996-01-30 Olin Corporation Process for the production of dinitrobenzene and mononitrobenzene
US5001272A (en) * 1988-06-22 1991-03-19 Olin Corporation Process for the production of dinitrotoluene
US4918250A (en) * 1989-04-21 1990-04-17 Olin Corporation Process for the production of dinitrotoluene using an inorganic salt as a phase separation agent
JPH0311042A (ja) * 1989-06-08 1991-01-18 Sumitomo Chem Co Ltd 接触的ニトロ化方法
CH683918A5 (de) * 1991-12-04 1994-06-15 Uetikon Chemie Ag Verfahren zur Herstellung von Nitrobenzol.
CH683919A5 (de) * 1992-01-15 1994-06-15 Uetikon Chemie Ag Verfahren zur Herstellung von Nitrobenzol.
DE10047163A1 (de) * 2000-09-22 2002-04-11 Basf Ag Verfahren zur Nitrierung aromatischer Kohlenwasserstoffe
US6991678B2 (en) * 2002-07-31 2006-01-31 Council Of Scientific And Industrial Research Process for preparing microporous crystalline titanium silicate
ATE527234T1 (de) * 2002-07-31 2011-10-15 Council Scient Ind Res Verfahren zur nitrierung von benzol in der gasphase unter verwendung von salpetersäure über einem molybdänsilikat enthaltenden katalysator
CN102093222A (zh) * 2010-12-23 2011-06-15 南京大学扬州化学化工研究院 固体酸催化剂SO42-/TiO2-HNbMoO6催化甲苯选择性硝化的方法
KR101282735B1 (ko) * 2011-08-17 2013-07-05 금호석유화학 주식회사 고체 염기촉매를 이용하는 기체상 니트로화 반응에 의한 니트로파라핀의 제조방법
CN102432471B (zh) * 2011-11-07 2013-12-18 常州大学 一种利用微通道反应器进行氯苯硝基反应的方法
WO2014195973A2 (en) 2013-06-03 2014-12-11 Council Of Scientific & Industrial Research Liquid phase nitration of aromatics using solid acid catalyst
CN103922940B (zh) * 2013-12-02 2016-04-20 刘凤能 一种生产硝基苯的工艺
CN106431930B (zh) * 2015-08-05 2018-07-17 湘潭大学 从苯制备硝基苯的方法
CN109320423B (zh) * 2018-11-22 2021-08-10 四川金象赛瑞化工股份有限公司 一种微通道反应器合成硝基化合物的方法
CN109675508B (zh) * 2018-12-11 2021-05-07 浙江工业大学 全氟磺酸树脂/固体酸微纤化微通道反应器的制备方法和应用

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5312823A (en) * 1976-07-17 1978-02-04 Hoechst Ag Nitration of tluene

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2109873A (en) * 1938-03-01 Process of nitrating hydrocarbons
GB578044A (en) * 1943-04-23 1946-06-13 Malcolm Percival Appleby Improvements in and relating to the production of nitroparaffins
GB586732A (en) * 1944-06-29 1947-03-28 Alfred Edgar Rout Improvements in the nitration of aromatic hydrocarbons
GB866162A (en) * 1956-12-31 1961-04-26 English Electric Co Ltd Improvements in and relating to electric fusegear
US3792099A (en) * 1972-07-31 1974-02-12 Standard Oil Co Branched polyphenylenes
DE3166081D1 (en) * 1980-11-26 1984-10-18 Monsanto Co A process for the vapor phase nitration of aromatic compounds
EP0078247B1 (en) * 1981-10-21 1985-11-27 Monsanto Company Process and catalysts for vapor phase nitration of aromatic compounds
US4415744A (en) * 1981-10-21 1983-11-15 Monsanto Company Vapor phase nitration of aromatic compounds

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5312823A (en) * 1976-07-17 1978-02-04 Hoechst Ag Nitration of tluene

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2003506340A (ja) * 1999-07-29 2003-02-18 メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフトング 静止型マイクロミキサー内でのニトロ化
JP2003506339A (ja) * 1999-07-29 2003-02-18 メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフトング スタティックマイクロミキサーにおけるフリーデル−クラフツアシル化方法
KR101183822B1 (ko) * 2009-12-18 2012-09-19 한국화학연구원 고체 산촉매를 이용한 니트로파라핀의 제조방법
WO2013025061A3 (ko) * 2011-08-17 2013-05-30 한국화학연구원 기체상 니트로화 반응에 의한 니트로파라핀의 제조방법
KR101282734B1 (ko) * 2011-08-17 2013-07-05 금호석유화학 주식회사 고체산 촉매를 이용한 니트로파라핀의 제조방법

Also Published As

Publication number Publication date
DE3360768D1 (en) 1985-10-17
EP0092372B1 (en) 1985-09-11
US4551568A (en) 1985-11-05
JPH0422897B2 (enExample) 1992-04-20
EP0092372A1 (en) 1983-10-26

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