JPH10506945A - オリゴアミン又はポリアミンの製法 - Google Patents
オリゴアミン又はポリアミンの製法Info
- Publication number
- JPH10506945A JPH10506945A JP8512292A JP51229296A JPH10506945A JP H10506945 A JPH10506945 A JP H10506945A JP 8512292 A JP8512292 A JP 8512292A JP 51229296 A JP51229296 A JP 51229296A JP H10506945 A JPH10506945 A JP H10506945A
- Authority
- JP
- Japan
- Prior art keywords
- oxide
- polyamines
- water
- polyamine
- added
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/04—Breaking emulsions
- B01D17/047—Breaking emulsions with separation aids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/04—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reaction of ammonia or amines with olefin oxides or halohydrins
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/02—Polyamines
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G73/00—Macromolecular compounds obtained by reactions forming a linkage containing nitrogen with or without oxygen or carbon in the main chain of the macromolecule, not provided for in groups C08G12/00 - C08G71/00
- C08G73/02—Polyamines
- C08G73/0206—Polyalkylene(poly)amines
- C08G73/0213—Preparatory process
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G33/00—Dewatering or demulsification of hydrocarbon oils
- C10G33/04—Dewatering or demulsification of hydrocarbon oils with chemical means
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Polymers & Plastics (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Thermal Sciences (AREA)
- Physics & Mathematics (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Polyethers (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Macromolecular Compounds Obtained By Forming Nitrogen-Containing Linkages In General (AREA)
Abstract
Description
Claims (1)
- 【特許請求の範囲】 1.第1工程で、水、アルコール又は酸もしくはこれらの混合物の存在下に、中 性又は塩基性の触媒の不存在下に、オリゴアミン又はポリアミンへのNH−基1 個当たり1分子のアルキレンオキサイドの付加を行い、かつ、第2工程で、水及 び酸の除去の後に、通常の中性又は塩基性の触媒の存在下に、更なるアルキレン オキサイドと反応させることより成る、2工程操作法によりオリゴアミン又はポ リアミンのオキシアルキレートを製造する方法において、 第2工程の実施の前に、次の群: (a)アルコール及びフェノール及びそれらのアルコキシレート、 (b)エチレンオキサイド、プロピレンオキサイド、ブチレンオキサイド又は これらの混合物をベースとするポリアルコール、 (c)N−置換カルボン酸アミド、 (d)アルカノールモノアミン及びアルカノールポリアミン及びこれらのアル コキシレート、 (e)オリゴアミン又はポリアミンの他のオキシアルキレート、 (f)芳香族炭化水素、 (g)脂肪族炭化水素、 (h)エーテル及び (i)スルホン又はスルホキシド からの有機の溶剤又は希釈剤又はこれらの混合物を添加することを特徴とする 、オリゴアミン又はポリアミンのオキシアルキレートの製法。 2.第1工程からの付加生成物の重量に対して2〜400重量部の量で有機の溶 剤又は希釈剤を添加する、請求の範囲1に記載の方法。 3.有機の溶剤又は希釈剤を群(b)、(c)、(d)、(f)及び(h)から 選択する、請求の範囲1又は2に記載の方法。 4.オリゴアミン又はポリアミンとして、1分子当たり3〜10個のN−原子を 有するポリアルキレンポリアミン、重量平均分子量600〜10000000を 有するポリビニルアミン又は重量平均分子量2000〜50000を有するポリ エチレンイミンを使用する、請求の範囲1から3のいずれかに記載の方法。 5.アルキレンオキサイドとして、エチレンオキサイド、プロピレンオキサイド 、ブチレンオキサイド又はこれらの混合物を使用する、請求の範囲1から4のい ずれかに記載の方法。 6.化合物(a)〜(i)の群からの使用溶剤又は希釈剤又はこれらの混合物を 含有する、請求の範囲1から5のいずれかに記載の方法により製造されたオリゴ アミン又はポリアミンのオキシアルキレートの 原油エマルジヨンの分解剤としての使用。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4435688.9 | 1994-10-06 | ||
DE4435688A DE4435688A1 (de) | 1994-10-06 | 1994-10-06 | Verfahren zur Herstellung von Oligoaminen oder Polyaminen |
PCT/EP1995/003809 WO1996011225A1 (de) | 1994-10-06 | 1995-09-26 | Verfahren zur herstellung von oligoaminen oder polyaminen |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH10506945A true JPH10506945A (ja) | 1998-07-07 |
JP3955319B2 JP3955319B2 (ja) | 2007-08-08 |
Family
ID=6530077
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP51229296A Expired - Fee Related JP3955319B2 (ja) | 1994-10-06 | 1995-09-26 | オリゴアミン又はポリアミンの製法 |
Country Status (15)
Country | Link |
---|---|
US (1) | US5846453A (ja) |
EP (1) | EP0784645B1 (ja) |
JP (1) | JP3955319B2 (ja) |
KR (1) | KR970706335A (ja) |
CN (2) | CN1087316C (ja) |
AU (1) | AU3742595A (ja) |
BR (1) | BR9509248A (ja) |
CA (1) | CA2201782C (ja) |
DE (2) | DE4435688A1 (ja) |
DK (1) | DK0784645T3 (ja) |
ES (1) | ES2131336T3 (ja) |
FI (1) | FI971418A (ja) |
MX (1) | MX198647B (ja) |
NO (1) | NO971540D0 (ja) |
WO (1) | WO1996011225A1 (ja) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2008530278A (ja) * | 2005-02-08 | 2008-08-07 | ベーアーエスエフ アクツィエンゲゼルシャフト | アルコキシル化されたポリエチレンイミンの生産物を作る方法 |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ID22843A (id) | 1997-02-27 | 1999-12-09 | Akzo Nobel Nv | Proses untuk n,n,n,n-tetra-(2-hidroksietil)-etilena diamina |
DE19801437A1 (de) | 1998-01-16 | 1999-07-22 | Basf Ag | Verfahren zur Herstellung von Aldehyden |
DE10028636A1 (de) | 2000-06-09 | 2001-12-13 | Basf Ag | Verfahren zur Herstellung von Alkanolaminen |
DE10048874A1 (de) * | 2000-09-29 | 2002-04-11 | Basf Ag | Katalysatorsystem und Verfahren zur Carbonylierung |
DE10228293A1 (de) | 2001-07-28 | 2003-02-13 | Basf Ag | Verfahren zur Herstellung von Dialkylketonen |
DE102005006030A1 (de) * | 2005-02-09 | 2006-08-10 | Basf Ag | Hyperverzweigte Polymere als Demulgatoren zum Spalten von Rohölemulsionen |
US7431845B2 (en) * | 2005-06-23 | 2008-10-07 | Nalco Company | Method of clarifying oily waste water |
EP2197938B1 (de) | 2007-10-08 | 2013-05-08 | Basf Se | Verwendung von hyperverzweigten polyestern zum spalten von öl-wasser-emulsionen |
CN101965219B (zh) * | 2008-03-04 | 2013-11-13 | 巴斯夫欧洲公司 | 烷氧基化聚链烷醇胺用于使油-水乳液破乳的用途 |
MX2011006960A (es) | 2008-12-29 | 2011-07-20 | Basf Se | Poliesteres y policarbonatos hiperramificados como desemulsionantes para separar emulsiones de petroleo crudo. |
DE102009041983A1 (de) * | 2009-09-17 | 2011-04-07 | Clariant International Ltd. | Alkoxylierte Trialkanolaminkondensate und deren Verwendung als Emulsionsspalter |
CN104066711B (zh) * | 2011-12-29 | 2017-04-19 | 塔明克公司 | 生产氢氧化胆碱的方法 |
BR102017022800A2 (pt) * | 2017-10-23 | 2019-05-07 | Oxiteno S A Ind E Comercio | processo de alcoxilação de uma composição polimérica e uso de uma composição polimérica alcoxilada |
WO2020121031A1 (en) | 2018-12-12 | 2020-06-18 | Sabic Global Technologies B.V. | Polyethylenimine as a new emulsion breaker for quench water systems |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2227546C3 (de) * | 1972-06-07 | 1979-04-05 | Basf Ag, 6700 Ludwigshafen | Verwendung von oxalkylierten PoIyalkylenpolyaminen zur SchneUentwässening von Rohölen |
DE2557501A1 (de) * | 1975-12-19 | 1977-06-30 | Bayer Ag | Verfahren zur herstellung von polyaminen |
DE3347257A1 (de) * | 1983-12-28 | 1985-07-11 | Basf Ag, 6700 Ludwigshafen | Vernetzte oxalkylierte polyalkylenpolyamine und ihre verwendung als erdoelemulsionsspalter |
CN1027869C (zh) * | 1991-07-23 | 1995-03-15 | 中国石油天然气总公司胜利设计院 | 阳离子聚醚型反相破乳剂的制备方法 |
DE4136661A1 (de) * | 1991-11-07 | 1993-05-13 | Basf Ag | Erdoelemulsionsspalter |
-
1994
- 1994-10-06 DE DE4435688A patent/DE4435688A1/de not_active Withdrawn
-
1995
- 1995-09-26 JP JP51229296A patent/JP3955319B2/ja not_active Expired - Fee Related
- 1995-09-26 CN CN95195536A patent/CN1087316C/zh not_active Expired - Fee Related
- 1995-09-26 WO PCT/EP1995/003809 patent/WO1996011225A1/de not_active Application Discontinuation
- 1995-09-26 CA CA002201782A patent/CA2201782C/en not_active Expired - Fee Related
- 1995-09-26 US US08/809,720 patent/US5846453A/en not_active Expired - Lifetime
- 1995-09-26 KR KR1019970702216A patent/KR970706335A/ko not_active Application Discontinuation
- 1995-09-26 DE DE59505927T patent/DE59505927D1/de not_active Expired - Lifetime
- 1995-09-26 ES ES95935382T patent/ES2131336T3/es not_active Expired - Lifetime
- 1995-09-26 BR BR9509248A patent/BR9509248A/pt not_active IP Right Cessation
- 1995-09-26 CN CNB011435739A patent/CN100415855C/zh not_active Expired - Fee Related
- 1995-09-26 EP EP95935382A patent/EP0784645B1/de not_active Expired - Lifetime
- 1995-09-26 MX MX9702367A patent/MX198647B/es unknown
- 1995-09-26 DK DK95935382T patent/DK0784645T3/da active
- 1995-09-26 AU AU37425/95A patent/AU3742595A/en not_active Abandoned
-
1997
- 1997-04-04 NO NO971540A patent/NO971540D0/no not_active Application Discontinuation
- 1997-04-04 FI FI971418A patent/FI971418A/fi unknown
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2008530278A (ja) * | 2005-02-08 | 2008-08-07 | ベーアーエスエフ アクツィエンゲゼルシャフト | アルコキシル化されたポリエチレンイミンの生産物を作る方法 |
Also Published As
Publication number | Publication date |
---|---|
US5846453A (en) | 1998-12-08 |
DE4435688A1 (de) | 1996-04-11 |
ES2131336T3 (es) | 1999-07-16 |
DE59505927D1 (de) | 1999-06-17 |
CA2201782C (en) | 2000-11-28 |
CN1087316C (zh) | 2002-07-10 |
FI971418A0 (fi) | 1997-04-04 |
DK0784645T3 (da) | 1999-11-01 |
BR9509248A (pt) | 1997-10-21 |
MX198647B (es) | 2000-09-18 |
CN100415855C (zh) | 2008-09-03 |
KR970706335A (ko) | 1997-11-03 |
WO1996011225A1 (de) | 1996-04-18 |
JP3955319B2 (ja) | 2007-08-08 |
NO971540L (no) | 1997-04-04 |
EP0784645A1 (de) | 1997-07-23 |
CN1160409A (zh) | 1997-09-24 |
AU3742595A (en) | 1996-05-02 |
NO971540D0 (no) | 1997-04-04 |
FI971418A (fi) | 1997-04-04 |
CN1375543A (zh) | 2002-10-23 |
EP0784645B1 (de) | 1999-05-12 |
CA2201782A1 (en) | 1996-04-18 |
MX9702367A (es) | 1997-06-28 |
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