JPH0220563B2 - - Google Patents
Info
- Publication number
- JPH0220563B2 JPH0220563B2 JP16508582A JP16508582A JPH0220563B2 JP H0220563 B2 JPH0220563 B2 JP H0220563B2 JP 16508582 A JP16508582 A JP 16508582A JP 16508582 A JP16508582 A JP 16508582A JP H0220563 B2 JPH0220563 B2 JP H0220563B2
- Authority
- JP
- Japan
- Prior art keywords
- silicate
- fatty acid
- liquid medium
- surfactant
- droplets
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 18
- 239000007788 liquid Substances 0.000 claims description 18
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 16
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Natural products CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 14
- 239000008187 granular material Substances 0.000 claims description 11
- 238000003756 stirring Methods 0.000 claims description 10
- 238000000034 method Methods 0.000 claims description 9
- 239000001569 carbon dioxide Substances 0.000 claims description 8
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 8
- -1 fatty acid ester Chemical class 0.000 claims description 8
- 239000004094 surface-active agent Substances 0.000 claims description 7
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 6
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 6
- 239000000194 fatty acid Substances 0.000 claims description 6
- 229930195729 fatty acid Natural products 0.000 claims description 6
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical group [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 5
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- CYTYCFOTNPOANT-UHFFFAOYSA-N Perchloroethylene Chemical group ClC(Cl)=C(Cl)Cl CYTYCFOTNPOANT-UHFFFAOYSA-N 0.000 claims description 3
- 239000003350 kerosene Substances 0.000 claims description 3
- 235000019353 potassium silicate Nutrition 0.000 claims description 3
- 229950011008 tetrachloroethylene Drugs 0.000 claims description 3
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 claims description 2
- 239000002202 Polyethylene glycol Substances 0.000 claims description 2
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 2
- 239000004115 Sodium Silicate Substances 0.000 claims description 2
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 claims description 2
- 150000005215 alkyl ethers Chemical class 0.000 claims description 2
- 125000005037 alkyl phenyl group Chemical group 0.000 claims description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 2
- 150000004665 fatty acids Chemical class 0.000 claims description 2
- 229920001223 polyethylene glycol Polymers 0.000 claims description 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 2
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 2
- 239000008096 xylene Substances 0.000 claims description 2
- 125000003944 tolyl group Chemical group 0.000 claims 1
- 239000002245 particle Substances 0.000 description 16
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- 239000000499 gel Substances 0.000 description 4
- 238000001879 gelation Methods 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- 239000007864 aqueous solution Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 239000000839 emulsion Substances 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 229910004298 SiO 2 Inorganic materials 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 239000002736 nonionic surfactant Substances 0.000 description 2
- 239000000741 silica gel Substances 0.000 description 2
- 229910002027 silica gel Inorganic materials 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 238000004438 BET method Methods 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- HVUMOYIDDBPOLL-XWVZOOPGSA-N Sorbitan monostearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O HVUMOYIDDBPOLL-XWVZOOPGSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000001771 impaired effect Effects 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000006224 matting agent Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 description 1
- 229920000053 polysorbate 80 Polymers 0.000 description 1
- 238000004626 scanning electron microscopy Methods 0.000 description 1
- 239000011163 secondary particle Substances 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000001256 steam distillation Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
Landscapes
- Silicates, Zeolites, And Molecular Sieves (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP16508582A JPS5954619A (ja) | 1982-09-24 | 1982-09-24 | 珪酸塩粒状体の製造方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP16508582A JPS5954619A (ja) | 1982-09-24 | 1982-09-24 | 珪酸塩粒状体の製造方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5954619A JPS5954619A (ja) | 1984-03-29 |
JPH0220563B2 true JPH0220563B2 (pt) | 1990-05-09 |
Family
ID=15805588
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP16508582A Granted JPS5954619A (ja) | 1982-09-24 | 1982-09-24 | 珪酸塩粒状体の製造方法 |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5954619A (pt) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2010087262A1 (ja) | 2009-01-30 | 2010-08-05 | 旭化成ケミカルズ株式会社 | シリカ担持触媒の製造方法、及び不飽和カルボン酸又は不飽和ニトリルの製造方法 |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2528315B2 (ja) * | 1987-05-22 | 1996-08-28 | 扶桑化学工業株式会社 | 高純度球状シリカの製造方法 |
DE69502788T2 (de) * | 1994-09-30 | 1999-02-25 | Asahi Glass Co Ltd | Zinkoxid enthaltende Kieselsäure und Verfahren zu ihrer Herstellung |
EP1733786B1 (en) * | 1999-02-05 | 2010-04-14 | Waters Technologies Corporation | Porous hybrid particles for chromatographic separations |
US6686035B2 (en) | 1999-02-05 | 2004-02-03 | Waters Investments Limited | Porous inorganic/organic hybrid particles for chromatographic separations and process for their preparation |
JP4216716B2 (ja) | 2001-08-09 | 2009-01-28 | ウォーターズ・インヴェストメンツ・リミテッド | クロマトグラフィー分離用多孔質有機・無機ハイブリッドモノリス状物質、およびその製造方法 |
WO2004041398A2 (en) | 2002-10-30 | 2004-05-21 | Waters Investments Limited | Porous inorganic/organic hybrid materials and preparation thereof |
US10773186B2 (en) | 2004-07-30 | 2020-09-15 | Waters Technologies Corporation | Porous inorganic/organic hybrid materials with ordered domains for chromatographic separations and processes for their preparation |
JP5308665B2 (ja) | 2004-07-30 | 2013-10-09 | ウオーターズ・テクノロジーズ・コーポレイシヨン | クロマトグラフィー分離用の秩序領域を有する多孔質無機/有機のハイブリッド材料およびこれらの調製方法 |
EP2101999A4 (en) | 2007-01-12 | 2017-12-27 | Waters Technologies Corporation | Porous carbon-heteroatom-silicon hybrid inorganic/organic materials for chromatographic separations and process for the preparation thereof |
WO2010141426A1 (en) | 2009-06-01 | 2010-12-09 | Waters Technologies Corporation | Hybrid material for chromatographic separations |
US11439977B2 (en) | 2009-06-01 | 2022-09-13 | Waters Technologies Corporation | Hybrid material for chromatographic separations comprising a superficially porous core and a surrounding material |
WO2012018598A1 (en) | 2010-07-26 | 2012-02-09 | Waters Technologies Corporation | Superficially porous materials comprising a substantially nonporous core having narrow particle size distribution; process for the preparation thereof; and use thereof for chromatographic separations |
US20190134604A1 (en) | 2016-03-06 | 2019-05-09 | Waters Technologies Corporation | Porous materials with controlled porosity; process for the preparation thereof; and use thereof for chromatographic separations |
-
1982
- 1982-09-24 JP JP16508582A patent/JPS5954619A/ja active Granted
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2010087262A1 (ja) | 2009-01-30 | 2010-08-05 | 旭化成ケミカルズ株式会社 | シリカ担持触媒の製造方法、及び不飽和カルボン酸又は不飽和ニトリルの製造方法 |
EP3466533A1 (en) | 2009-01-30 | 2019-04-10 | Asahi Kasei Kabushiki Kaisha | Methods for the oxidation or ammoxydation of propane characterized by the catalyst |
Also Published As
Publication number | Publication date |
---|---|
JPS5954619A (ja) | 1984-03-29 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JPH0220563B2 (pt) | ||
US4420442A (en) | Manufacturing process for hollow microspheres | |
US4421562A (en) | Manufacturing process for hollow microspheres | |
JP2000516269A (ja) | 固体難燃剤および煙抑制剤のコロイド粒子ならびにそれらの製造方法 | |
JPH0151455B2 (pt) | ||
JP2000169132A (ja) | エ―ロゾルを用いて酸化アルミニウムをド―ピングした熱分解法二酸化珪素、その製法、その使用およびその配合物 | |
CN113056512B (zh) | 基于纤维素的可热膨胀微球 | |
IE44307B1 (en) | Vesiculated silica microspheres | |
PL185969B1 (pl) | Kompozycja żelowa oraz izolacja cieplna zawierająca kompozycję żelową | |
KR20010034188A (ko) | 분말 도료 조성물 | |
TW200307006A (en) | Method for the production of coated, fine-particle, inorganic solids and use thereof | |
KR101089897B1 (ko) | 펠렛화된 실리카 | |
US3161468A (en) | Process for producing hollow spheres of silica | |
JPH0114163B2 (pt) | ||
JP2002097385A (ja) | 珪酸をワックスで被覆する方法および被覆された珪酸の使用 | |
US4036663A (en) | Inorganic pigments and methods for producing the pigments and aqueous slurries thereof | |
US2167674A (en) | Manufacture of carbon black | |
TW500779B (en) | Matting agents based on silicon dioxide | |
US2736669A (en) | Method of activating and esterifying the surface of finely divided particles of silica having surface silanol groups | |
JPS63146966A (ja) | ジオキサジンバイオレツト顔料の製造方法 | |
JPH04506979A (ja) | 水系媒体中に分散可能な固形添加剤系、その製造方法及びポリマー粒子へのその適用 | |
JP3525677B2 (ja) | Ic基板用充填剤及びic封止用樹脂組成物 | |
JPH06279589A (ja) | 球状シリコーン微粒子の製造方法 | |
JP2007176738A (ja) | 安定化された表面処理葉状シリカ2次粒子粉末及びその製造方法 | |
JP2557403B2 (ja) | 珪酸ゲルの製造方法 |