JP7199409B2 - 難燃化した複合繊維およびその製造方法 - Google Patents
難燃化した複合繊維およびその製造方法 Download PDFInfo
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- JP7199409B2 JP7199409B2 JP2020500505A JP2020500505A JP7199409B2 JP 7199409 B2 JP7199409 B2 JP 7199409B2 JP 2020500505 A JP2020500505 A JP 2020500505A JP 2020500505 A JP2020500505 A JP 2020500505A JP 7199409 B2 JP7199409 B2 JP 7199409B2
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- TWQULNDIKKJZPH-UHFFFAOYSA-K trilithium;phosphate Chemical compound [Li+].[Li+].[Li+].[O-]P([O-])([O-])=O TWQULNDIKKJZPH-UHFFFAOYSA-K 0.000 description 1
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- UNXRWKVEANCORM-UHFFFAOYSA-N triphosphoric acid Chemical compound OP(O)(=O)OP(O)(=O)OP(O)(O)=O UNXRWKVEANCORM-UHFFFAOYSA-N 0.000 description 1
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- BIKXLKXABVUSMH-UHFFFAOYSA-N trizinc;diborate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]B([O-])[O-].[O-]B([O-])[O-] BIKXLKXABVUSMH-UHFFFAOYSA-N 0.000 description 1
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- 125000002948 undecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
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- 125000003774 valeryl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 238000013022 venting Methods 0.000 description 1
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- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
- 229910021489 α-quartz Inorganic materials 0.000 description 1
Images
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- B27N9/00—Arrangements for fireproofing
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B27N3/00—Manufacture of substantially flat articles, e.g. boards, from particles or fibres
- B27N3/04—Manufacture of substantially flat articles, e.g. boards, from particles or fibres from fibres
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- D—TEXTILES; PAPER
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
- D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
- D06M11/56—Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic Table
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- D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
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- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
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- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
- D06M11/71—Salts of phosphoric acids
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- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/72—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with metaphosphoric acids or their salts; with polyphosphoric acids or their salts; with perphosphoric acids or their salts
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Description
(1) 無機粒子と繊維との複合繊維を難燃化剤で処理した複合繊維であって、繊維表面の15%以上が無機粒子によって被覆されている、上記複合繊維。
(2) 難燃化剤が、ホウ素系難燃化剤、または、ケイ素系難燃化剤である、(1)に記載の複合繊維。
(3) 前記繊維がセルロース繊維である、(1)または(2)に記載の複合繊維。
(4) 無機粒子が硫酸バリウム、炭酸マグネシウム及びハイドロタルサイトからなる群より選ばれる少なくとも1種の無機粒子である、(1)または(2)に記載の複合繊維。
(5) 無機粒子の平均一次粒子径が1.5μm以下である、(1)~(4)に記載の複合繊維。
(6) 繊維と無機粒子の重量比が5/95~95/5である、(1)~(5)のいずれかに記載の複合繊維。
(7) シート、モールド、ボードもしくはブロックの形態である、(1)~(6)のいずれかに記載の複合繊維。
(8) 難燃化剤が、リン系薬剤および/または窒素系薬剤である、(1)~(7)のいずれかに記載の複合繊維。
(9) 無機粒子が、炭酸カルシウムまたはシリカ/アルミナを含む、(1)~(8)のいずれかに記載の複合繊維。
(10) (1)~(9)のいずれかに記載の複合繊維の製造方法であって、無機粒子と繊維との複合繊維を難燃化剤によって処理する工程を含む、上記方法。
(11) 難燃化剤を含浸、塗布または噴霧することによって処理する(10)に記載の方法。
(12) 繊維を含有する液体中で無機粒子を合成して前記複合繊維を得る工程を含む、(10)に記載の方法。
本発明において「難燃」とは燃え難いこと、「難燃化」とは燃え難くすること、「難燃組成物(「難燃剤」、「難燃化剤」ともいう)」とは材料を燃え難くするための添加剤を意味する。材料およびその用途によっては法令が整備され、「難燃」に関する詳細な基準や評価方法が規格化されている。それらの中で、炎を伴った燃焼ができないことを意味する「不燃」、火が燃え広がらないことを意味する「防炎」、その他「防火」および「耐火」などの用語が使われているが、本発明では、これらの用語をすべて含めて「難燃」と定義する。
本発明は、無機粒子によってその表面が被覆された繊維を使用する。特に本発明の好ましい態様において、繊維表面の15%以上が無機粒子によって被覆されている繊維・無機複合体を使用する。
本発明において、繊維と複合化する無機粒子は特に制限されないが、水に不溶性または難溶性の無機粒子であることが好ましい。無機粒子の合成を水系で行う場合があり、また、繊維複合体を水系で使用することもあるため、無機粒子が水に不溶性または難溶性であると好ましい。
本発明に係る複合繊維を合成する場合、キャビテーション気泡の存在下で無機粒子を析出させることができる。本発明においてキャビテーションとは、流体の流れの中で圧力差により短時間に泡の発生と消滅が起きる物理現象であり、空洞現象とも言われる。キャビテーションによって生じる気泡(キャビテーション気泡)は、流体の中で圧力がごく短時間だけ飽和蒸気圧より低くなったとき、液体中に存在する100ミクロン以下のごく微小な「気泡核」を核として生じる。
本発明で使用する複合繊維は、セルロース繊維と無機粒子とを複合化したものである。複合繊維を構成するセルロース繊維としては例えば、天然のセルロース繊維はもちろん、レーヨンやリヨセルなどの再生繊維(半合成繊維)や合成繊維などを制限なく使用することができる。セルロース繊維の原料としては、植物由来のパルプ繊維、セルロースナノファイバー、バクテリアセルロース、ホヤなどの動物由来セルロース、藻類などが例示され、木材パルプは、木材原料をパルプ化して製造すればよい。木材原料としては、アカマツ、クロマツ、トドマツ、エゾマツ、ベニマツ、カラマツ、モミ、ツガ、スギ、ヒノキ、カラマツ、シラベ、トウヒ、ヒバ、ダグラスファー、ヘムロック、ホワイトファー、スプルース、バルサムファー、シーダ、パイン、メルクシマツ、ラジアータパイン等の針葉樹、及びこれらの混合材、ブナ、カバ、ハンノキ、ナラ、タブ、シイ、シラカバ、ハコヤナギ、ポプラ、タモ、ドロヤナギ、ユーカリ、マングローブ、ラワン、アカシア等の広葉樹及びこれらの混合材が例示される。
本発明の一つの態様において、繊維を含む溶液中で無機粒子を合成することによって複合体を合成することができるが、無機粒子の合成方法は、それぞれ、公知の方法によることができる。
本発明においては、上述の複合繊維を難燃化剤で処理することによって、燃えにくさを大きく向上させた難燃化した複合繊維を得ることができる。得られる複合繊維の形態は特に限定されず、様々な成形物(体)を製造することが可能である。例えば、本発明の複合繊維をシート化すると、高灰分のシートを容易に得ることができる。また、得られたシートを貼り合せて多層シートとすることもできる。シート製造に用いる抄紙機(抄造機)としては、例えば長網抄紙機、円網抄紙機、ギャップフォーマ、ハイブリッドフォーマ、多層抄紙機、これらの機器の抄紙方式を組合せた公知の抄造機などが挙げられる。抄紙機におけるプレス線圧、後段でカレンダー処理を行う場合のカレンダー線圧は、いずれも操業性や複合繊維シートの性能に支障を来さない範囲内で定めることができる。また、形成されたシートに対して含浸や塗布により澱粉や各種ポリマー、顔料およびそれらの混合物を付与しても良い。
(サンプル1) 硫酸バリウム及び水酸化アルミニウムとセルロース繊維との複合繊維
反応容器(マシンチェスト、容積:4m3)に2%のパルプスラリー(広葉樹晒クラフトパルプ/針葉樹晒クラフトパルプ=8/2、CSF=390mL、平均繊維長:約1.3mm、固形分25kg)と水酸化バリウム八水和物(日本化学工業、75kg)とを投入して混合後、ペリスターポンプを用いて硫酸アルミニウム(硫酸バンド、98kg)を約500g/minで滴下した。滴下終了後、そのまま30分間撹拌を継続してサンプル1を得た(図3)。
水酸化マグネシウム5250g(宇部マテリアルズ、UD653)とクラフトパルプ3500g(LBKP、CSF=360mL、平均繊維長=0.76mm)を含む水性懸濁液170Lを準備した。これを500L容のキャビテーション装置に入れ、反応溶液を循環させながら、反応容器中に炭酸ガスを吹き込んで炭酸ガス法によって炭酸マグネシウム微粒子と繊維との複合繊維を合成した。反応温度は約40℃、炭酸ガスは市販の液化ガスを供給源とし、炭酸ガスの吹き込み量は20L/minとした。反応液のpHが約7.8になった段階でCO2の導入を停止し(反応前のpHは約9.5)、その後30分間、キャビテーションの発生と装置内でのスラリーの循環を継続してサンプル2を得た(図4)。
まず、ハイドロタルサイト(HT)を合成するための溶液を準備した。アルカリ溶液(A溶液)として、Na2CO3(和光純薬)およびNaOH(和光純薬)の混合水溶液を調製した。また、酸溶液(B溶液)として、MgSO4(和光純薬)およびAl2(SO4)3(和光純薬)の混合水溶液を調製した。
・アルカリ溶液(A溶液):Na2CO3濃度:0.1M、NaOH濃度:1.6M
・酸溶液(B溶液):MgSO4濃度:0.6M、Al2(SO4)3濃度:0.1M
A液とB液の量をそれぞれ1.6Lとした以外はサンプル3と同様にして合成し、サンプル4を得た(図6)
NBKP30g(CSF:510mL)を含む水性懸濁液2.2Lを樹脂製容器(5L容)に入れ、ラボミキサーで撹拌した500rpm)。この水性懸濁液に硫酸アルミニウム水溶液(工業用硫酸バンド、濃度9%)をpH=3.7になるまで約10分間滴下した後、硫酸アルミニウム水溶液(工業用硫酸バンド、濃度9%)とケイ酸ナトリウム水溶液(和光純薬社製、濃度8%)をpH=4を維持するよう同時に約90分間滴下した。滴下にはペリスターポンプを使用し、反応温度は約24℃であった。滴下後、そのまま約30分撹拌した後、再びケイ酸ナトリウム水溶液(和光純薬、濃度8%)を約30分間滴下し、pH=8.0に調整した。使用した硫酸アルミニウム水溶液およびケイ酸ナトリウム水溶液の総量はそれぞれ、155gと150gであった。以上によってシリカ/アルミナ粒子とセルロース繊維との複合繊維を合成した(図7)。
WO2018/047749に示すような反応装置(図8)を用い、パルプ繊維(LBKP/NBKP=8/2、CSF=377mL)を含む水性懸濁液に対して、反応開始温度は約15℃、炭酸ガスの吹き込み量を3L/minとして反応を行い、反応液のpHが7~8になった段階で反応を停止した。炭酸ガスをウルトラファインバブル発生装置(図9、せん断式、エンバイロビジョン社YJ-9)に給気し、炭酸ガスを含む大量のウルトラファインバブル(平均粒子径:137nm、気泡の存在時間:60分間以上)を反応液中に発生させ、炭酸カルシウム粒子を炭酸ガス法によってセルロース繊維上に合成し、サンプル6の複合繊維を合成した(図10)。
得られたサンプルを下記の手順により評価した。
<複合繊維シートの製造>
サンプル1~6の複合繊維を以下の手順によりシート化した。各シートの坪量はJIS P 8124:1998、灰分はJIS P 8251:2003に基づいて測定した。
複合繊維のスラリー(サンプル1、濃度:約1%)に、アニオン性の歩留剤(FA230、ハイモ)とカチオン性の歩留剤(ND300、ハイモ)を対固形分で100ppmずつ添加してスラリー(水性懸濁液)を調製した。次いで、長網抄紙機を用いて、抄速10m/minの条件でこのスラリーからシートを製造した(坪量:約160g/m2、灰分:約64%)。
シート1と同様にして、長網抄紙機を用いてサンプル2のシートを製造した(坪量:約100g/m2、灰分:約43%)。
シート1と同様にして、長網抄紙機を用いてサンプル3のシートを製造した(坪量:約100g/m2、灰分:約33%)
サンプル4の水性懸濁液(約0.5%)に、カチオン性歩留剤(ND300、ハイモ社製)を200ppm、アニオン性歩留剤(FA230、ハイモ社製)を200ppm添加し、500rpmにて撹拌して懸濁液を調成した。得られた懸濁液からJIS P 8222に基づいて角形手抄き器にて複合繊維シートを製造した(坪量:約170g/m2、灰分:61%)。
サンプル5の水性懸濁液(約0.5%)を、濾紙(ADVANTEC製、標準用濾紙 No.5B、直径90mm)がセットされたブフナー漏斗に注いだ。10秒間静置後、吸引濾過によって得られた湿紙を乾燥することで複合繊維シートを製造した(直径:約95mm、坪量:約135g/m2、灰分:18%)。
サンプル6の水性懸濁液を用いる以外は上記シート5と同様にして、サンプル6のシートを製造した(直径:約95mm、坪量:約135g/m2、灰分:56%)。
(a)ホウ素系薬剤によるシートの処理
下記のシートサンプルにホウ素系薬剤(商品名:SOUFA、SOUFA社製)を噴霧した後、金属板とアルミホイルに挟んでローラーで余分な薬剤を除去した。その後、乾燥機に移して60℃で1時間緊張乾燥させることで薬剤処理シートを得た。
・複合繊維シート(シート1~4)
・濾紙(ADVANTEC製、標準用濾紙 No.1、260mm×260mm)
・コピー用紙(FUJI XEROX製、商品名:EP GAAA5989、A4サイズ)
・インクジェット用紙(日本製紙製、マットIJ用紙、A4サイズ)
(b)ケイ素系薬剤によるシートの処理
処理する薬剤をケイ素系薬剤(商品名:クリスタルシーラー、墨東化成工業製)とした以外は、上記(a)と同様にして薬剤処理した。
(c)リンおよび窒素系薬剤によるシートの処理
下記のシートサンプルをリンおよび窒素系薬剤(商品名:タイエンN、太洋化学産業製、40wt%水溶液)に含浸した後、金属板とアルミホイルに挟んでローラーで余分な薬剤を除去した。その後、乾燥機に移して50℃で2時間緊張乾燥させることで薬剤処理シートを得た。
・複合繊維シート(シート5)
・濾紙(ADVANTEC製、標準用濾紙 No.5B、直径90mm)
(d)含ホウ素系薬剤によるシートの処理
下記のシートサンプルについて、処理する薬剤を含ホウ素系薬剤(商品名:UBCERA、石塚硝子製、10wt%)とした以外は、上記(c)と同様にして薬剤処理した。
・複合繊維シート(シート5、6)
・濾紙(ADVANTEC製、標準用濾紙 No.5B、直径90mm)
上記の薬剤処理シートについて、下式にしたがって薬剤含有率(対固形分)を算出した。
薬剤含有率(対固形分)[%]=(M1-M0)/M0
ここで、M0は薬剤処理前のシートの絶乾重量[g]、M1は薬剤処理後のシートの絶乾重量[g]を表している。
薬剤処理前・後のシートのしなやかさを評価した。具体的には、両手で曲げた時に感じる抵抗に対して、薬剤処理前のシートを基準とし、薬剤処理によるシートのしなやかさの変化を4段階で評価した。評価基準は下記のとおりであり、4点は薬剤処理前後でシートのしなやかさが損なわれていないことを示し、1点は薬剤処理によりシートが硬く、脆くなったことを示す。
(しなやかさの評価)
・4点:薬剤処理前後でしなやかさに変化はなかった
・3点:薬剤処理後のシートがわずかに硬くなった
・2点:薬剤処理後のシートがやや硬くなった
・1点:薬剤処理後のシートが硬くなった
実験2で得られたシート1~4の燃焼性を、JIS A 1322(JIS Z 2150)を基にして、以下の手順により評価した。まず、それぞれのサンプルを50℃で48時間乾燥した後,乾燥用シリカゲルを入れたデシケータ中に24時間放置し、下記の燃焼性試験に供した。
サンプルを支持枠(25cm×16cm)に取り付けて、たるみのないように燃焼性試験装置に装着した。ガスバーナーに点火後、10秒または1分間サンプルを加熱し、炭化長、残炎時間、残じん時間を測定した(図11)
・炭化長:試験体の加熱面の炭化部分(炭化して明らかに強度が変化)している部分について支持枠の長手方向の最大長さを測定する。
・残炎時間:加熱終了時から試験体が炎をあげて燃え続ける時間を測定する。
・残じん:加熱終了時から無炎燃焼している状態をいう。
・難燃性に関する防炎等級
・防炎1級:炭化長5cm以下、残炎なし、残じんが1分後に存しない
・防炎2級:炭化長10cm以下、残炎なし、残じんが1分後に存しない
・防炎3級:炭化長15cm以下、残炎なし、残じんが1分後に存しない
サンプルの上部をクリップに取り付けて、宙吊りの状態で静置した。そこへ、サンプルの下部へと点火したライター(サンプルに接していない状態で、炎の長さが30mm)を素早く近づけ、サンプルに対して炎が10mm接する状態で固定して5秒間加熱し続けた(図12)。そのときの火の燃え広がり方を観察した。
IJプリンター(Canon PIXUS iP7100、染料インク)を用いてパターンを印刷し、薬剤処理前後のサンプルのIJ印刷適性を評価した。
(滲み) 良 5(未処理IJ用紙)→1 悪
(発色) 良 5(未処理IJ用紙)→1 悪
<複合繊維を用いた成型物の製造>
以下の手順により、発熱性試験に用いる成型物を作製した。下記のボードサンプルには、処理液A(ホウ素系薬剤、商品名:BestBoron、SOUFA社製、36wt%水溶液)を使用した。
サンプル1の水性懸濁液を、底がメッシュになっている型(144mm×144mm×100mm)に流し込み、圧搾成型することでボードを作製した。これを1MPaで1分間、次いで3MPaで2分間プレスしたのち、75℃に設定された恒温槽を用いて10時間乾燥した。得られた乾燥サンプルを100mm角に切り出し、それを75℃の上記処理液Aに60分間浸漬させた後、105℃に設定された恒温槽を用いて5時間乾燥することでボード1を作製した。
底がメッシュになっている四角柱の型(144mm×144mm×10cm)を吸水掃除機の先に取り付け、型をサンプル6の水性懸濁液と炭酸カルシウム(特級、関東化学製)の混合水性懸濁液が入った樹脂容器(25L容)中に沈めた後すぐに吸引を開始した。10秒程度吸引したところで型を引き上げ、そのまま30秒間吸引を続けた。吸引を終了した後、型から内容物をはずし、プレス工程(1MPaで1分間、次いで3MPaで2分間)ののちに75℃設定の恒温槽を用いて10時間乾燥した。得られた乾燥サンプルを100mm角に切り出し、それを75℃の上記処理液Aに60分間浸漬させた後、105℃に設定された恒温槽を用いて5時間乾燥することでボード2を作製した。
サンプル6の水性懸濁液と三石蝋石(竹昇精工製)の混合水性懸濁液を用いた以外は、上記ボード2と同様の手順でボード3を作製した。
ISO5660‐1:2002に準じて、コーンカロリーメーター法における20分間の総発熱量と試験後の寸法収縮を評価した。また、以下3点を満たすことで建築基準法における「不燃材料」に相当すると判断できる。なお、「加熱後のサンプルの収縮量が5mmより大きい」とき、「有害な変形」があると評価した。
(評価項目)
・総発熱量が8MJ/m2以下であること
・有害な変形や裏まで貫通する亀裂及び穴がないこと
(外観や加熱後のサンプルの収縮量に基づいて評価した)
・最大発熱速度が、10秒以上継続して200kW/m2を超えないこと
Claims (10)
- セルロース繊維表面の15%以上が無機粒子によって被覆されており、難燃化剤を含む複合繊維であって、
無機粒子の平均一次粒子径が1.5μm以下であり、無機粒子が、ハイドロタルサイト、炭酸カルシウム、シリカ/アルミナ、水酸化アルミニウムからなる群より選ばれる少なくとも1種であり、難燃化剤が、ホウ素系難燃化剤、ケイ素系難燃化剤、リン系難燃化剤および窒素系難燃化剤のいずれかを含む、上記複合繊維。 - 難燃化剤が、ホウ素系難燃化剤またはケイ素系難燃化剤である、請求項1に記載の複合繊維。
- 難燃化剤が、リン系難燃化剤および/または窒素系難燃化剤である、請求項1または2に記載の複合繊維。
- 無機粒子が、ハイドロタルサイトを含む、請求項1~3のいずれかに記載の複合繊維。
- 無機粒子が、炭酸カルシウムまたはシリカ/アルミナを含む、請求項1~4のいずれかに記載の複合繊維。
- セルロース繊維と無機粒子の重量比が5/95~95/5である、請求項1~5のいずれかに記載の複合繊維。
- 請求項1~6のいずれかに記載の複合繊維を含んでなるシート、モールド、ボードまたはブロック。
- 請求項1~6のいずれかに記載の複合繊維の製造方法であって、
無機粒子とセルロース繊維との複合繊維を難燃化剤によって処理する工程を含む、上記方法。 - 含浸、塗布または噴霧することによって難燃化剤を複合繊維に含ませる、請求項8に記載の方法。
- セルロース繊維を含有する液体中で無機粒子を合成して前記複合繊維を得る工程を含む、請求項8または9に記載の方法。
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JP7123178B2 (ja) * | 2019-09-06 | 2022-08-22 | 日本製紙株式会社 | セルロース繊維と無機粒子の複合繊維およびその製造方法 |
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CN112411229A (zh) * | 2020-11-05 | 2021-02-26 | 江西中竹生物质科技有限公司 | 超声波制造包装纸用高粱秆纤维浆的方法 |
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CN113154596A (zh) * | 2021-04-14 | 2021-07-23 | 上海应用技术大学 | 一种新型空气净化系统 |
CN113265902B (zh) * | 2021-04-28 | 2023-08-11 | 湖北盟科纸业有限公司 | 一种预冷处理的电弧喷铝铝箔纸制备装置 |
CN118119491A (zh) * | 2021-12-06 | 2024-05-31 | 松下知识产权经营株式会社 | 制备纤维板的方法和用于制备纤维板的压缩材料 |
US12018180B2 (en) | 2022-02-11 | 2024-06-25 | Awi Licensing Llc | Fire resistant adhesive compositions and methods of preparing and using the same |
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