JP7019604B2 - 粒状コラーゲン材料の製造方法及び製造されたコラーゲン材料 - Google Patents
粒状コラーゲン材料の製造方法及び製造されたコラーゲン材料 Download PDFInfo
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- JP7019604B2 JP7019604B2 JP2018560535A JP2018560535A JP7019604B2 JP 7019604 B2 JP7019604 B2 JP 7019604B2 JP 2018560535 A JP2018560535 A JP 2018560535A JP 2018560535 A JP2018560535 A JP 2018560535A JP 7019604 B2 JP7019604 B2 JP 7019604B2
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- 102000008186 Collagen Human genes 0.000 title claims description 55
- 108010035532 Collagen Proteins 0.000 title claims description 55
- 229920001436 collagen Polymers 0.000 title claims description 55
- 239000000463 material Substances 0.000 title claims description 41
- 238000004519 manufacturing process Methods 0.000 title claims description 19
- 238000000605 extraction Methods 0.000 claims description 43
- 238000000034 method Methods 0.000 claims description 20
- 239000008346 aqueous phase Substances 0.000 claims description 19
- 239000012071 phase Substances 0.000 claims description 14
- 239000007790 solid phase Substances 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 239000002245 particle Substances 0.000 claims description 11
- 239000002994 raw material Substances 0.000 claims description 11
- 235000013305 food Nutrition 0.000 claims description 10
- 238000001035 drying Methods 0.000 claims description 9
- 241001465754 Metazoa Species 0.000 claims description 8
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 6
- 238000000227 grinding Methods 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 241000283690 Bos taurus Species 0.000 claims description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 4
- 238000010521 absorption reaction Methods 0.000 claims description 3
- 230000002378 acidificating effect Effects 0.000 claims description 3
- 244000144972 livestock Species 0.000 claims description 3
- 235000013372 meat Nutrition 0.000 claims description 3
- 235000013580 sausages Nutrition 0.000 claims description 3
- 241000251468 Actinopterygii Species 0.000 claims description 2
- 241000271566 Aves Species 0.000 claims description 2
- 241000124008 Mammalia Species 0.000 claims description 2
- 206010033675 panniculitis Diseases 0.000 claims description 2
- 235000015277 pork Nutrition 0.000 claims description 2
- 238000000926 separation method Methods 0.000 claims description 2
- 210000004304 subcutaneous tissue Anatomy 0.000 claims description 2
- 239000006286 aqueous extract Substances 0.000 claims 1
- 108010010803 Gelatin Proteins 0.000 description 11
- 239000008273 gelatin Substances 0.000 description 11
- 229920000159 gelatin Polymers 0.000 description 11
- 235000019322 gelatine Nutrition 0.000 description 11
- 235000011852 gelatine desserts Nutrition 0.000 description 11
- 230000000694 effects Effects 0.000 description 6
- 239000000499 gel Substances 0.000 description 6
- 239000000243 solution Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 5
- 102000004169 proteins and genes Human genes 0.000 description 4
- 108090000623 proteins and genes Proteins 0.000 description 4
- 239000000839 emulsion Substances 0.000 description 3
- 239000000725 suspension Substances 0.000 description 3
- 239000000654 additive Substances 0.000 description 2
- 210000000988 bone and bone Anatomy 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 230000001804 emulsifying effect Effects 0.000 description 2
- 239000003929 acidic solution Substances 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 1
- 239000000920 calcium hydroxide Substances 0.000 description 1
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 238000009837 dry grinding Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 235000021060 food property Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 235000021395 porridge Nutrition 0.000 description 1
- 230000008092 positive effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 238000001238 wet grinding Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/10—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from hair, feathers, horn, skins, leather, bones, or the like
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/20—Animal feeding-stuffs from material of animal origin
- A23K10/26—Animal feeding-stuffs from material of animal origin from waste material, e.g. feathers, bones or skin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/40—Feeding-stuffs specially adapted for particular animals for carnivorous animals, e.g. cats or dogs
- A23K50/42—Dry feed
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/275—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of animal origin, e.g. chitin
- A23L29/281—Proteins, e.g. gelatin or collagen
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/20—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents
- A23L29/275—Foods or foodstuffs containing additives; Preparation or treatment thereof containing gelling or thickening agents of animal origin, e.g. chitin
- A23L29/281—Proteins, e.g. gelatin or collagen
- A23L29/284—Gelatin; Collagen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07K—PEPTIDES
- C07K14/00—Peptides having more than 20 amino acids; Gastrins; Somatostatins; Melanotropins; Derivatives thereof
- C07K14/435—Peptides having more than 20 amino acids; Gastrins; Somatostatins; Melanotropins; Derivatives thereof from animals; from humans
- C07K14/78—Connective tissue peptides, e.g. collagen, elastin, laminin, fibronectin, vitronectin or cold insoluble globulin [CIG]
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H1/00—Macromolecular products derived from proteins
- C08H1/06—Macromolecular products derived from proteins derived from horn, hoofs, hair, skin or leather
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/20—Ingredients acting on or related to the structure
- A23V2200/222—Emulsifier
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/20—Ingredients acting on or related to the structure
- A23V2200/242—Thickening agent
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2200/00—Function of food ingredients
- A23V2200/20—Ingredients acting on or related to the structure
- A23V2200/244—Viscosity modification agent
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/54—Proteins
- A23V2250/542—Animal Protein
- A23V2250/5422—Collagen
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2250/00—Food ingredients
- A23V2250/54—Proteins
- A23V2250/542—Animal Protein
- A23V2250/5432—Gelatine
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Biochemistry (AREA)
- Organic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Molecular Biology (AREA)
- Animal Husbandry (AREA)
- Dispersion Chemistry (AREA)
- Genetics & Genomics (AREA)
- Biophysics (AREA)
- Gastroenterology & Hepatology (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Toxicology (AREA)
- Nutrition Science (AREA)
- General Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Physiology (AREA)
- Biotechnology (AREA)
- Biomedical Technology (AREA)
- Birds (AREA)
- Peptides Or Proteins (AREA)
- Meat, Egg Or Seafood Products (AREA)
- Materials For Medical Uses (AREA)
- Cosmetics (AREA)
- Fodder In General (AREA)
Description
-水性の抽出溶液を用いてコラーゲン及び脂肪を含有する動物性原材料を抽出する工程;
-抽出残留物から水相の少なくとも一部分を任意で分離する工程;
-当該抽出残留物を、コラーゲン固相、水相及び脂肪相に分離する工程;
-少なくとも一部分の水相とコラーゲン固相の少なくとも一部分とを混合する工程;
-当該混合された相を少なくとも部分的に乾燥させる工程;及び
-乾燥した相を粉砕して、粒状のコラーゲン材料を取得する工程;
を含む本発明の方法によって達成される。
下記の本発明の粒状コラーゲン材料を製造するため、ポークラインズを、各条件下、硫酸抽出溶液を用いて6回抽出した。最後の抽出残留物を、コラーゲン固相、水相、及び脂肪相に分離し、固相を各比率で水相と混合した。ローラー乾燥後、材料を平均粒径150μmとなるまで粉砕した。
表1の例において、各抽出は、65℃18時間で異なるpH値で実施された。固相及び水相は、3:7の比率で混合された。
表2の例において、抽出は、65℃及びpH4.8で異なる抽出時間で実施された。固相及び水相は、3:7の比率で混合された。
表3の例において、抽出は、65℃及びpH4.8、抽出時間18時間で実施された。固相及び水相は、異なる比率で混合された。
Claims (12)
- 粒状コラーゲン材料を製造する方法であって、以下の工程:
-pHが3.5~5.5の酸性の水性の抽出溶液を用いてコラーゲン及び脂肪を含有する動物性原材料を抽出する工程;
-抽出残留物から水相の少なくとも一部分を任意で分離する工程;
-当該抽出残留物を、コラーゲン固相、水相及び脂肪相に分離する工程;
-コラーゲン固相の少なくとも一部分と少なくとも一部分の水相とを重量比1:99~1:1で混合する工程;
-当該混合された相を少なくとも部分的に乾燥させる工程;及び
-乾燥した相を粉砕して、平均粒径20~250μmの粒状のコラーゲン材料を取得する工程;
を含み、前記抽出残留物が、前記水相の分離後に水性抽出溶液を用いて2~8回抽出され、最後の抽出残留物のコラーゲン固相が、最後の抽出工程の水相と混合される、方法。 - 前記水性抽出溶液が硫酸又は塩酸を含有する、請求項1に記載の方法。
- 前記水性抽出溶液のpHが4~5である、請求項1又は2のいずれかに記載の方法。
- 前記抽出の時間が、30時間以下、好ましくは25時間以下、より好ましくは15~25時間である、請求項1~3のいずれか1項に記載の方法。
- 前記コラーゲン及び脂肪を含有する動物性原材料が、哺乳類、鳥類及び魚類の皮膚及び皮下組織から、より具体的には、ポークラインズ(pork rinds)又はキャトルスプリット(cattle split)から選択される、請求項1~4のいずれか1項に記載の方法。
- 前記コラーゲン固相及び水相が、1:9~1:2の重量比で互いに混合される、請求項1~5のいずれか1項に記載の方法。
- 前記混合された相の乾燥が、残留水分量が2~20重量%、好ましくは5~15%になるまで行われる、請求項1~6のいずれか1項に記載の方法。
- 前記乾燥が50~150℃の温度で行われる、請求項1~7のいずれか1項に記載の方法。
- 前記乾燥した相の粉砕が、グラインド、好ましくは平均粒径50~150μmとなるまでのグラインドを含む、請求項1~8のいずれか1項に記載の方法。
- 平均粒径が20~250μmであり、請求項1~9のいずれか1項に記載の方法によって製造され、水分吸収容量が、そのネット重量に基づき1:1~50:1であり、及び/又は脂肪及び水における乳化容量が、そのネット重量に基づきそれぞれ1:1~20:1である、粒状コラーゲン材料。
- 平均粒径が50~150μmである、請求項10に記載のコラーゲン材料。
- 食料品、より具体的には肉及びソーセージ製品、又は家畜及びペット用の飼料製品の製造における、請求項10又は11のいずれかに記載の粒状コラーゲン材料の使用。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102016109094.8 | 2016-05-18 | ||
DE102016109094.8A DE102016109094A1 (de) | 2016-05-18 | 2016-05-18 | Verfahren zur Herstellung eines Kollagenmaterials in Partikelform und hergestelltes Kollagenmaterial |
PCT/EP2017/053214 WO2017198351A1 (de) | 2016-05-18 | 2017-02-14 | Verfahren zur herstellung eines kollagenmaterials in partikelform und hergestelltes kollagenmaterial |
Publications (2)
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JP2019521093A JP2019521093A (ja) | 2019-07-25 |
JP7019604B2 true JP7019604B2 (ja) | 2022-02-15 |
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JP2018560535A Active JP7019604B2 (ja) | 2016-05-18 | 2017-02-14 | 粒状コラーゲン材料の製造方法及び製造されたコラーゲン材料 |
Country Status (14)
Country | Link |
---|---|
US (1) | US10939690B2 (ja) |
EP (1) | EP3457864A1 (ja) |
JP (1) | JP7019604B2 (ja) |
KR (1) | KR20190008850A (ja) |
CN (1) | CN109310109A (ja) |
AU (1) | AU2017266120B2 (ja) |
BR (1) | BR112018071794B1 (ja) |
CA (1) | CA3023594A1 (ja) |
CR (1) | CR20180586A (ja) |
DE (1) | DE102016109094A1 (ja) |
MX (1) | MX2018014137A (ja) |
PH (1) | PH12018502392A1 (ja) |
RU (1) | RU2756795C2 (ja) |
WO (1) | WO2017198351A1 (ja) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
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WO2022073090A1 (pt) | 2020-10-06 | 2022-04-14 | Janaina De Andrea Dernowsek Ltda | Método para a produção de uma composição de proteínas de matriz extracelular e produto obtido por tal método |
CN115281319A (zh) * | 2022-07-12 | 2022-11-04 | 山东蓝奥生物技术有限公司 | 一种花胶原液及其制备方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20040010122A1 (en) | 2002-07-15 | 2004-01-15 | Ifendu Nnanna | Process for producing insoluble and soluble collagen protein products from poultry skins and use thereof |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
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DE836982C (de) * | 1949-07-12 | 1952-04-17 | British Glues And Chemicals Lt | Verfahren zum Entfetten von Knochen |
SU1126586A1 (ru) * | 1982-10-25 | 1984-11-30 | Всесоюзный научно-исследовательский институт прикладной энзимологии | Способ получени желатина из м гкого коллагенсодержащего сырь |
JPH0593000A (ja) * | 1991-09-30 | 1993-04-16 | Nippon Kasei Chem Co Ltd | 高純度の酸可溶性魚鱗コラーゲンの製造法 |
NZ519878A (en) * | 1999-11-29 | 2004-02-27 | Nz Inst For Crop & Food Res | Collagen |
GB0120756D0 (en) | 2001-08-25 | 2001-10-17 | Devro Plc | Collagen casing |
ATE455153T1 (de) * | 2006-03-13 | 2010-01-15 | Becker & Co Naturinwerk | Kollagenpulver und auf kollagen basierende thermoplastische zusammensetzung zur herstellung von formkörpern |
DE102008036576A1 (de) * | 2008-07-31 | 2010-02-04 | Gelita Ag | Partikel aus Kollagenmaterial und Verfahren zur Herstellung |
MY160866A (en) * | 2008-12-23 | 2017-03-31 | Univ Putra Malaysia | Collagen extraction from aquatic animals |
CN101787078B (zh) * | 2009-01-23 | 2013-01-09 | 香港百特有限公司 | 一种胶原蛋白多肽及其制备方法和用途 |
CN101589821A (zh) * | 2009-06-08 | 2009-12-02 | 四川省食品发酵工业研究设计院 | 分子胶原蛋白火腿肠制备技术 |
CN103554248A (zh) * | 2013-11-01 | 2014-02-05 | 南昌航空大学 | 一种从淡水珍珠蚌肉中提取胶原蛋白的工艺方法 |
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2016
- 2016-05-18 DE DE102016109094.8A patent/DE102016109094A1/de active Pending
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2017
- 2017-02-14 AU AU2017266120A patent/AU2017266120B2/en not_active Ceased
- 2017-02-14 CR CR20180586A patent/CR20180586A/es unknown
- 2017-02-14 JP JP2018560535A patent/JP7019604B2/ja active Active
- 2017-02-14 RU RU2018143971A patent/RU2756795C2/ru active
- 2017-02-14 EP EP17706426.8A patent/EP3457864A1/de active Pending
- 2017-02-14 KR KR1020187030605A patent/KR20190008850A/ko not_active Application Discontinuation
- 2017-02-14 WO PCT/EP2017/053214 patent/WO2017198351A1/de unknown
- 2017-02-14 CA CA3023594A patent/CA3023594A1/en not_active Abandoned
- 2017-02-14 MX MX2018014137A patent/MX2018014137A/es unknown
- 2017-02-14 CN CN201780030196.0A patent/CN109310109A/zh active Pending
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US20040010122A1 (en) | 2002-07-15 | 2004-01-15 | Ifendu Nnanna | Process for producing insoluble and soluble collagen protein products from poultry skins and use thereof |
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JP2019521093A (ja) | 2019-07-25 |
US10939690B2 (en) | 2021-03-09 |
KR20190008850A (ko) | 2019-01-25 |
US20190075818A1 (en) | 2019-03-14 |
BR112018071794B1 (pt) | 2023-01-10 |
RU2018143971A3 (ja) | 2020-06-18 |
RU2756795C2 (ru) | 2021-10-05 |
EP3457864A1 (de) | 2019-03-27 |
AU2017266120B2 (en) | 2021-09-23 |
BR112018071794A2 (pt) | 2019-02-19 |
PH12018502392B1 (en) | 2019-07-15 |
PH12018502392A1 (en) | 2019-07-15 |
CR20180586A (es) | 2019-04-25 |
CN109310109A (zh) | 2019-02-05 |
MX2018014137A (es) | 2019-07-08 |
RU2018143971A (ru) | 2020-06-18 |
CA3023594A1 (en) | 2017-11-23 |
DE102016109094A1 (de) | 2017-11-23 |
AU2017266120A1 (en) | 2018-12-06 |
WO2017198351A1 (de) | 2017-11-23 |
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