JP6756624B2 - 板状の別個の要素を有する、蓄電システム、板状の別個の要素、その製造方法、並びにその使用 - Google Patents
板状の別個の要素を有する、蓄電システム、板状の別個の要素、その製造方法、並びにその使用 Download PDFInfo
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- JP6756624B2 JP6756624B2 JP2016575012A JP2016575012A JP6756624B2 JP 6756624 B2 JP6756624 B2 JP 6756624B2 JP 2016575012 A JP2016575012 A JP 2016575012A JP 2016575012 A JP2016575012 A JP 2016575012A JP 6756624 B2 JP6756624 B2 JP 6756624B2
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- power storage
- storage system
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- separate
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Description
600・10-6≦θMax・α≦8000・10-6、
特に好ましくは800・10-6≦θMax・α≦5000・10-6。
以下の実施例1〜22には、本発明による板状の別個の要素の基板材料のための例示的な組成がまとめられている。実施例23は、本発明による板状の別個の要素を製造するための被覆法を記載している。
α(20〜300) 3.2・10-6/K
Tg 717℃
密度 2.43g/cm3。
α(20〜300) 7.2・10-6/K
Tg 557℃
密度 2.5g/cm3。
α(20〜300) 9.4・10-6/K
Tg 533℃
密度 2.55g/cm3。
α(20〜300) 3.25・10-6/K
Tg 525℃
密度 2.2g/cm3。
α(20〜300) 8.6・10-6/K
Tg 607℃
密度 2.4g/cm3。
α(20〜300) 8.5・10-6/K
Tg 505℃
密度 2.5g/cm3。
α(20〜300) 9.7・10-6/K
Tg 556℃
密度 2.6g/cm3。
α(20〜300) 8.3・10-6/K
Tg 623℃
密度 2.4g/cm3。
α(20〜300) 8.9・10-6/K
Tg 600℃
密度 2.4g/cm3。
α(20〜300) 3.8・10-6/K
Tg 719℃
密度 2.51g/cm3。
α(20〜300) 3.8・10-6/K
密度 2.5g/cm3。
α(20〜300) 3.73・10-6/K
Tg 705℃
密度 2.49g/cm3。
α(20〜300) 3.2ppm/K
密度 2.38g/cm3。
α(20〜300) 9.0ppm/K
Tg 573℃。
α(20〜300) 9.5ppm/K
Tg 564℃。
本発明による板状の別個の要素を得るために、基板材料(例えば実施例1〜8に挙げたもの)をスパッタリング装置内に移し、10-5mbar未満の圧力に減圧した。この基板を、少なくとも200℃の温度に加熱した。プロセスガス(通常アルゴン)を入れ、これによってプロセス圧力を10-2mbar未満に調整する。スパッタリング装置には、Si含有ターゲットが備え付けられており、これによって反応ガスとして窒素を使用しながら、Si3N4含有材料系が堆積される。良好なバリアは、出力密度が10W/cm2を上回るスパッタリング法によって生じる。上記パラメータによって例えば、厚さが300nmの層を堆積させることができる。バリア層の厚さは一般的に、10nm〜1μmであり得る。バリア層の厚さは好ましくは80〜200nmであり、特に好ましくはバリア層の厚さは、約100nmである。引き続き、この要素を取り出す。
Claims (41)
- ガラスとして存在する少なくとも1つの板状の別個の要素を有する、蓄電システムにおいて、
前記少なくとも1つの板状の別個の要素の少なくとも1つの表面は、該表面が、この表面と接触する材料に対して、透過性が低減され、リチウムに対して働くバリアとして形成されているように、バリア層として形成されており、
ここで前記バリア層が、Siの窒化物、又はAl、Cr、Ti、Zr、Hf、及び/又はTaの窒化物を含有し、前記ガラスは、質量%で示された以下の組成範囲:
ここで選択的に清澄剤が0〜1質量%、例えばSnO2、CeO2、As2O3、Cl-、F-、硫酸塩が含まれていてよく、No.2の範囲においてMgO、CaO、及びBaOの合計含分は、8〜18質量%の範囲にあることを特徴とする、前記蓄電システム。 - 前記バリア層が、前記少なくとも1つの表面の鉛直的な組成変化によって、バルク内への直接的な拡散経路が存在しないように獲得されることを特徴とする、請求項1に記載の蓄電システム。
- 前記少なくとも1つの表面の鉛直的な組成変化内に、アルカリ金属及び/又はアルカリ土類金属のためのゲッター材料が含まれていることを特徴とする、請求項2に記載の蓄電システム。
- 前記少なくとも1つの表面の鉛直的な組成変化が、少なくとも2つの層の連続体によって形成されており、ここで相互に隣接する層は、それぞれ異なる組成を有することを特徴とする、請求項2又は3に記載の蓄電システム。
- バリア層が、プラズマ援用法によって得られることを特徴とする、請求項1から4までのいずれか1項に記載の蓄電システムの製造方法。
- バリア層が、原子層堆積法(ALD)によって得られることを特徴とする、請求項1から4までのいずれか1項に記載の蓄電システムの製造方法。
- 前記バリア層のバリア作用が、別途のアニール工程によって、導電体又はアノードの設置前に引き起こされることを特徴とする、請求項5又は6に記載の蓄電システムの製造方法。
- 前記バリア層のバリア作用が、カソードのアニールの間に引き起こされることを特徴とする、請求項5〜7のいずれかに記載の蓄電システムの製造方法。
- ガラスとして存在する前記少なくとも1つの板状の別個の要素のための基板材料が、30μmの厚さにおいて、200nm〜270nmの範囲で0.1%以上という透過率を有することを特徴とする、請求項1から4までのいずれか1項に記載の蓄電システム。
- ガラスとして存在する前記板状の別個の要素が、基板材料の透過率値と比較して、前記バリア層により60%未満低減されている透過率値を有することを特徴とする、請求項1から4のいずれか又は9に記載の蓄電システム。
- バリア層が非晶質であることを特徴とする、請求項1から4のいずれか、9又は10に記載の蓄電システム。
- ガラスとして存在する前記板状の別個の要素が、直径100mm超の範囲にある、ウェハ若しくは基板の大きさに対して、25μm以下の厚みばらつきを有することを特徴とする、請求項1から4のいずれか、又は、9〜11のいずれかに記載の蓄電システム。
- ガラスとして存在する前記少なくとも1つの板状の別個の要素が、10-3g/(m2・d)未満という水蒸気透過率(WVTR)を有することを特徴とする、請求項1から4のいずれか、又は、9〜12のいずれかに記載の蓄電システム。
- ガラスとして存在する前記少なくとも1つの板状の別個の要素が、2mm未満という厚さを有することを特徴とする、請求項1から4のいずれか、又は、9〜13のいずれかに記載の蓄電システム。
- ガラスとして存在する前記少なくとも1つの板状の別個の要素が、350℃の温度、周波数50Hzの交流において、1.0・106Ωcm超という比電気抵抗を有することを特徴とする、請求項1から4のいずれか、又は、9〜14のいずれかに記載の蓄電システム。
- ガラスとして存在する前記少なくとも1つの板状の別個の要素が、少なくとも300℃という最大負荷温度θMaxを有することを特徴とする、請求項1から4のいずれか、又は、9〜15のいずれかに記載の蓄電システム。
- ガラスとして存在する前記少なくとも1つの板状の別個の要素が、2.0・10-6/K〜10・10-6/Kという範囲の線熱膨張係数αを有することを特徴とする、請求項1から4のいずれか、又は、9〜16のいずれかに記載の蓄電システム。
- ガラスとして存在する前記少なくとも1つの板状の別個の要素の最大負荷温度θMaxと、線熱膨張係数αとの積について、以下の関係;
600・10-6≦θMax・α≦8000・10-6 、
が成り立つことを特徴とする、請求項1から4のいずれか、又は、9〜17のいずれかに記載の蓄電システム。 - ガラスとして存在する前記少なくとも1つの板状の別個の要素の基板材料が、溶融プロセスと、それに続く付形プロセスによって板状に形成されることを特徴とする、請求項5〜8のいずれかに記載の蓄電システムの製造方法。
- 引き続く付形プロセスが、ドロー法であることを特徴とする、請求項19に記載の蓄電システムの製造方法。
- 前記バリア層が、前記少なくとも1つの表面の鉛直構造化によって、バルク内への直接的な拡散経路が存在しないように獲得されることを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21に記載の板状の別個の要素。
- 鉛直構造内に、アルカリ金属及び/又はアルカリ土類金属のためのゲッター材料が含まれていることを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21又は22に記載の板状の別個の要素。
- 前記少なくとも1つの表面の鉛直的な組成変化が、少なくとも2つの層の連続体によって形成されており、ここで相互に隣接する層は、それぞれ異なる組成を有することを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21から23までのいずれか1項に記載の板状の別個の要素。
- バリア層が、プラズマ援用法によって得られることを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21から24までのいずれか1項に記載の板状の別個の要素の製造方法。
- バリア層が、原子層堆積法(ALD)によって得られることを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21から24までのいずれか1項に記載の板状の別個の要素の製造方法。
- 蓄電システムにおける適用のための、ガラスとして存在する請求項21から24までのいずれか1項に記載の板状の別個の要素において、
ガラスとして存在する前記板状の別個の要素の基板材料が、30μmの厚さにおいて、200nm〜270nmの範囲で0.1%以上という透過率を有することを特徴とする、前記要素。 - ガラスとして存在する前記板状の別個の要素が、基板材料の透過率値と比較して、前記バリア層により60%未満低減されている透過率値を有することを特徴とする、ガラスとして存在する請求項21〜24のいずれか又は27に記載の板状の別個の要素。
- バリア層が非晶質であることを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21〜24のいずれか、27又は28に記載の板状の別個の要素。
- ガラスとして存在する前記要素が、直径100mm超の範囲にある、ウェハ若しくは基板の大きさに対して、25μm以下の厚みばらつきを有することを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21〜24のいずれか、又は、27〜29のいずれかに記載の板状の別個の要素。
- ガラスとして存在する前記要素が、2mm未満という厚さを有することを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21〜24のいずれか、又は、27〜30のいずれかに記載の板状の別個の要素。
- 10-3g/(m2・d)未満という水蒸気透過率(WVTR)を特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21〜24のいずれか、又は、27〜31のいずれかに記載の板状の別個の要素。
- 350℃の温度、周波数50Hzの交流において、1.0・106Ωcm超という比電気抵抗を特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21〜24のいずれか、又は、27〜32のいずれかに記載の板状の別個の要素。
- 少なくとも300℃という最大負荷温度θMaxを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21〜24のいずれか、又は、27〜33のいずれかに記載の板状の別個の要素。
- 2・10-6/K〜10・10-6/Kという範囲の線熱膨張係数αを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21〜24のいずれか、又は、27〜34のいずれかに記載の板状の別個の要素。
- 最大負荷温度θMaxと、線熱膨張係数αとの積について、以下の関係;
600・10-6≦θMax・α≦8000・10-6 、
が成り立つことを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21〜24のいずれか、又は、27〜35のいずれかに記載の板状の別個の要素。 - 溶融プロセスと、それに続いた熱間成形を特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項21〜24のいずれか、又は、27〜36のいずれかに記載の板状の別個の要素の基板材料の製造方法。
- 前記熱間成形法が、ドロー法であることを特徴とする、蓄電システムにおける適用のための、ガラスとして存在する請求項37に記載の板状の別個の要素の基板材料の製造方法。
- 蓄電システムにおける基板としての、ガラスとして存在する請求項21〜24のいずれか、又は、27〜36のいずれかに記載の板状の別個の要素の使用。
- 蓄電システムにおけるスーパーストレートとしての、ガラスとして存在する請求項21〜24のいずれか、又は、27〜36のいずれかに記載の板状の別個の要素の使用。
- 蓄電システムにおけるカバーとしての、ガラスとして存在する請求項21〜24のいずれか、又は、27〜36のいずれかに記載の板状の別個の要素の使用。
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DE102014117632.4A DE102014117632A1 (de) | 2014-06-23 | 2014-12-01 | Elektrisches Speichersystem enthaltend ein scheibenförmiges diskretes Element, scheibenförmiges diskretes Element sowie Verfahren zu dessen Herstellung und dessn Verwendung |
PCT/EP2015/064058 WO2015197589A1 (de) | 2014-06-23 | 2015-06-23 | Elektrisches spechersystem mit einem scheibenförmigen diskreten element, scheibenförmiges diskretes element, verfahren zu dessen herstellung sowie dessen verwendung |
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