JP6577188B2 - 層状酸化物カソード組成物の合成のための方法 - Google Patents
層状酸化物カソード組成物の合成のための方法Info
- Publication number
- JP6577188B2 JP6577188B2 JP2014517142A JP2014517142A JP6577188B2 JP 6577188 B2 JP6577188 B2 JP 6577188B2 JP 2014517142 A JP2014517142 A JP 2014517142A JP 2014517142 A JP2014517142 A JP 2014517142A JP 6577188 B2 JP6577188 B2 JP 6577188B2
- Authority
- JP
- Japan
- Prior art keywords
- lithium
- temperature
- calcination
- hours
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- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G45/00—Compounds of manganese
- C01G45/12—Complex oxides containing manganese and at least one other metal element
- C01G45/1221—Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G45/00—Compounds of manganese
- C01G45/12—Complex oxides containing manganese and at least one other metal element
- C01G45/1221—Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof
- C01G45/1228—Manganates or manganites with trivalent manganese, tetravalent manganese or mixtures thereof of the type (MnO2)-, e.g. LiMnO2 or Li(MxMn1-x)O2
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G51/00—Compounds of cobalt
- C01G51/40—Complex oxides containing cobalt and at least one other metal element
- C01G51/42—Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2
- C01G51/44—Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2 containing manganese
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G51/00—Compounds of cobalt
- C01G51/40—Complex oxides containing cobalt and at least one other metal element
- C01G51/42—Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2
- C01G51/44—Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2 containing manganese
- C01G51/50—Complex oxides containing cobalt and at least one other metal element containing alkali metals, e.g. LiCoO2 containing manganese of the type (MnO2)n-, e.g. Li(CoxMn1-x)O2 or Li(MyCoxMn1-x-y)O2
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/40—Complex oxides containing nickel and at least one other metal element
- C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
- C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G53/00—Compounds of nickel
- C01G53/40—Complex oxides containing nickel and at least one other metal element
- C01G53/42—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2
- C01G53/44—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese
- C01G53/50—Complex oxides containing nickel and at least one other metal element containing alkali metals, e.g. LiNiO2 containing manganese of the type (MnO2)n-, e.g. Li(NixMn1-x)O2 or Li(MyNixMn1-x-y)O2
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/64—Burning or sintering processes
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/131—Electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/139—Processes of manufacture
- H01M4/1391—Processes of manufacture of electrodes based on mixed oxides or hydroxides, or on mixtures of oxides or hydroxides, e.g. LiCoOx
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/50—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese
- H01M4/505—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of manganese of mixed oxides or hydroxides containing manganese for inserting or intercalating light metals, e.g. LiMn2O4 or LiMn2OxFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/48—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides
- H01M4/52—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron
- H01M4/525—Selection of substances as active materials, active masses, active liquids of inorganic oxides or hydroxides of nickel, cobalt or iron of mixed oxides or hydroxides containing iron, cobalt or nickel for inserting or intercalating light metals, e.g. LiNiO2, LiCoO2 or LiCoOxFy
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Ceramic Engineering (AREA)
- Structural Engineering (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Compositions Of Oxide Ceramics (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13/168,516 | 2011-06-24 | ||
| US13/168,516 US8992794B2 (en) | 2011-06-24 | 2011-06-24 | Process for synthesis of a layered oxide cathode composition |
| PCT/US2012/043479 WO2012177833A2 (en) | 2011-06-24 | 2012-06-21 | Process for synthesis of a layered oxide cathode composition |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2018073328A Division JP2018150231A (ja) | 2011-06-24 | 2018-04-05 | 層状酸化物カソード組成物の合成のための方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2014523070A JP2014523070A (ja) | 2014-09-08 |
| JP2014523070A5 JP2014523070A5 (cg-RX-API-DMAC7.html) | 2015-08-06 |
| JP6577188B2 true JP6577188B2 (ja) | 2019-09-18 |
Family
ID=47360973
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014517142A Active JP6577188B2 (ja) | 2011-06-24 | 2012-06-21 | 層状酸化物カソード組成物の合成のための方法 |
| JP2018073328A Ceased JP2018150231A (ja) | 2011-06-24 | 2018-04-05 | 層状酸化物カソード組成物の合成のための方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2018073328A Ceased JP2018150231A (ja) | 2011-06-24 | 2018-04-05 | 層状酸化物カソード組成物の合成のための方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US8992794B2 (cg-RX-API-DMAC7.html) |
| EP (1) | EP2724397B8 (cg-RX-API-DMAC7.html) |
| JP (2) | JP6577188B2 (cg-RX-API-DMAC7.html) |
| KR (1) | KR20140051184A (cg-RX-API-DMAC7.html) |
| CN (1) | CN103620829B (cg-RX-API-DMAC7.html) |
| HU (1) | HUE044067T2 (cg-RX-API-DMAC7.html) |
| PL (1) | PL2724397T3 (cg-RX-API-DMAC7.html) |
| WO (1) | WO2012177833A2 (cg-RX-API-DMAC7.html) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2966798C (en) | 2014-11-26 | 2022-11-29 | Basf Se | Process for making a lithiated transition metal oxide |
| CN108139159A (zh) | 2015-10-14 | 2018-06-08 | 巴斯夫欧洲公司 | 含有复合纤维陶瓷的热渗透管 |
| US20180316004A1 (en) * | 2016-06-09 | 2018-11-01 | Hitachi Metals, Ltd. | Method for producing cathode active material used for lithium secondary battery |
| JP6646129B1 (ja) * | 2018-12-07 | 2020-02-14 | 住友化学株式会社 | リチウム二次電池用正極活物質の製造方法 |
| KR102565910B1 (ko) | 2019-01-21 | 2023-08-10 | 주식회사 엘지화학 | 이차전지용 양극 활물질의 제조방법 |
| JP6936909B1 (ja) * | 2020-08-07 | 2021-09-22 | Basf戸田バッテリーマテリアルズ合同会社 | 非水電解質二次電池用正極活物質及びそれを用いた非水電解質二次電池 |
| CN121263885A (zh) * | 2023-05-31 | 2026-01-02 | 雅宝公司 | 用于生产含锂混合金属氧化物材料的方法 |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5874058A (en) * | 1995-10-06 | 1999-02-23 | Kerr-Mcgee Chemical Llc | Method of preparing Li1+x MN2-x O4 for use as secondary battery electrode |
| US5728367A (en) | 1996-06-17 | 1998-03-17 | Motorola, Inc. | Process for fabricating a lithiated transition metal oxide |
| JPH11111286A (ja) * | 1997-09-30 | 1999-04-23 | Mitsui Mining & Smelting Co Ltd | リチウム二次電池用正極材料の製造方法 |
| JP4122710B2 (ja) * | 1998-02-09 | 2008-07-23 | トダ・コウギョウ・ヨーロッパ・ゲゼルシャフト・ミット・ベシュレンクテル・ハフツング | リチウム−遷移金属混合物の調製法 |
| US5908291A (en) * | 1998-05-01 | 1999-06-01 | Harper International Corp. | Continuous cross-flow rotary kiln |
| US6267943B1 (en) | 1998-10-15 | 2001-07-31 | Fmc Corporation | Lithium manganese oxide spinel compound and method of preparing same |
| JP3446639B2 (ja) * | 1998-12-10 | 2003-09-16 | 松下電器産業株式会社 | リチウム二次電池用正極活物質の製造方法およびリチウム二次電池 |
| US6344366B1 (en) | 1999-09-15 | 2002-02-05 | Lockheed Martin Energy Research Corporation | Fabrication of highly textured lithium cobalt oxide films by rapid thermal annealing |
| EP1142834A4 (en) | 1999-11-15 | 2009-06-17 | Mitsubishi Chem Corp | LITHIUM MANGANESE COMPOSITE OXIDE, POSITIVE ELECTRODE MATERIAL FOR LITHIUM SECONDARY ACCUMULATOR, POSITIVE ELECTRODE AND LITHIUM SECONDARY ACCUMULATOR, AND PROCESS FOR THE PREPARATION OF LITHIUM MANGANESE COMPOSITE OXIDE |
| US6350543B2 (en) | 1999-12-29 | 2002-02-26 | Kimberly-Clark Worldwide, Inc. | Manganese-rich quaternary metal oxide materials as cathodes for lithium-ion and lithium-ion polymer batteries |
| JP2002260655A (ja) * | 2001-02-28 | 2002-09-13 | Nichia Chem Ind Ltd | リチウムイオン二次電池用正極活物質の製造方法 |
| US7211237B2 (en) * | 2003-11-26 | 2007-05-01 | 3M Innovative Properties Company | Solid state synthesis of lithium ion battery cathode material |
| JP4797332B2 (ja) * | 2004-03-24 | 2011-10-19 | 三菱化学株式会社 | リチウム二次電池正極活物質用リチウム遷移金属複合酸化物粉体、リチウム二次電池正極及びリチウム二次電池 |
| US7381496B2 (en) * | 2004-05-21 | 2008-06-03 | Tiax Llc | Lithium metal oxide materials and methods of synthesis and use |
| KR101130589B1 (ko) * | 2005-05-17 | 2012-03-30 | 에이지씨 세이미 케미칼 가부시키가이샤 | 리튬 2 차 전지 정극용 리튬 함유 복합 산화물의 제조 방법 |
| WO2007000286A1 (en) | 2005-06-28 | 2007-01-04 | Toda Kogyo Europe Gmbh | Inorganic compounds |
| JP4221448B1 (ja) | 2007-07-19 | 2009-02-12 | 日鉱金属株式会社 | リチウムイオン電池用リチウムマンガン複合酸化物及びその製造方法 |
| CN101679074B (zh) * | 2008-02-04 | 2012-02-22 | 松下电器产业株式会社 | 含锂过渡金属氧化物的制造方法 |
| JP5006830B2 (ja) * | 2008-04-30 | 2012-08-22 | 一般財団法人電力中央研究所 | 石炭ガス化スラグ発泡体の製造システム |
| JP5231171B2 (ja) * | 2008-10-30 | 2013-07-10 | パナソニック株式会社 | 非水電解質二次電池用正極活物質およびその製造方法 |
| CN101521272A (zh) * | 2009-03-20 | 2009-09-02 | 广州鸿森材料有限公司 | 一种高压煅烧制备锂镍锰氧锂离子电池正极材料的方法 |
| US8333950B2 (en) * | 2009-08-27 | 2012-12-18 | Honeywell International Inc. | Process for the preparation of lithium metal oxides involving fluidized bed techniques |
| CA2784686C (en) | 2009-12-17 | 2018-02-20 | Phostech Lithium Inc. | Method for improving the electrochemical performances of an alkali metal oxyanion electrode material and alkali metal oxyanion electrode material obtained therefrom |
| US8980475B2 (en) * | 2010-06-25 | 2015-03-17 | Basf Se | Process for preparing lithium mixed metal oxides and their use as cathode material |
| TWI468367B (zh) * | 2011-03-29 | 2015-01-11 | Jx日鑛日石金屬股份有限公司 | Production method of positive electrode active material for lithium ion battery and positive electrode active material for lithium ion battery |
-
2011
- 2011-06-24 US US13/168,516 patent/US8992794B2/en active Active
-
2012
- 2012-06-21 PL PL12802556T patent/PL2724397T3/pl unknown
- 2012-06-21 EP EP12802556.6A patent/EP2724397B8/en active Active
- 2012-06-21 JP JP2014517142A patent/JP6577188B2/ja active Active
- 2012-06-21 WO PCT/US2012/043479 patent/WO2012177833A2/en not_active Ceased
- 2012-06-21 CN CN201280030849.2A patent/CN103620829B/zh active Active
- 2012-06-21 KR KR1020137034698A patent/KR20140051184A/ko not_active Ceased
- 2012-06-21 HU HUE12802556A patent/HUE044067T2/hu unknown
-
2018
- 2018-04-05 JP JP2018073328A patent/JP2018150231A/ja not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| WO2012177833A2 (en) | 2012-12-27 |
| JP2018150231A (ja) | 2018-09-27 |
| EP2724397B1 (en) | 2019-04-10 |
| HUE044067T2 (hu) | 2019-09-30 |
| CN103620829A (zh) | 2014-03-05 |
| JP2014523070A (ja) | 2014-09-08 |
| KR20140051184A (ko) | 2014-04-30 |
| EP2724397A2 (en) | 2014-04-30 |
| EP2724397A4 (en) | 2015-11-25 |
| WO2012177833A3 (en) | 2013-02-21 |
| US8992794B2 (en) | 2015-03-31 |
| US20120326077A1 (en) | 2012-12-27 |
| EP2724397B8 (en) | 2019-06-12 |
| PL2724397T3 (pl) | 2019-09-30 |
| CN103620829B (zh) | 2017-03-15 |
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