JP6407277B2 - 軽量合わせガラス板およびその製造方法 - Google Patents
軽量合わせガラス板およびその製造方法 Download PDFInfo
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- JP6407277B2 JP6407277B2 JP2016528401A JP2016528401A JP6407277B2 JP 6407277 B2 JP6407277 B2 JP 6407277B2 JP 2016528401 A JP2016528401 A JP 2016528401A JP 2016528401 A JP2016528401 A JP 2016528401A JP 6407277 B2 JP6407277 B2 JP 6407277B2
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- Japan
- Prior art keywords
- glass plate
- glass
- organic layer
- plate
- laminated glass
- Prior art date
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- B29C66/00—General aspects of processes or apparatus for joining preformed parts
- B29C66/01—General aspects dealing with the joint area or with the area to be joined
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- B29C66/022—Mechanical pre-treatments, e.g. reshaping
- B29C66/0224—Mechanical pre-treatments, e.g. reshaping with removal of material
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- B32B2315/00—Other materials containing non-metallic inorganic compounds not provided for in groups B32B2311/00 - B32B2313/04
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- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
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Description
並びに任意で、着色性酸化物、例えばNd2O3、Fe2O3、CoO、NiO、V2O5、Nd2O3、MnO2、TiO2、CuO、CeO2、Cr2O3、希土類酸化物を0〜1質量%、並びに清澄剤、例えばAs2O3、Sb2O3、SnO2、SO3、Cl、F、CeO2を0〜2質量%。
並びに任意で、着色性酸化物、例えばNd2O3、Fe2O3、CoO、NiO、V2O5、Nd2O3、MnO2、TiO2、CuO、CeO2、Cr2O3、希土類酸化物を0〜5質量%、又は「黒色ガラス」のためには0〜15質量%、並びに清澄剤、例えばAs2O3、Sb2O3、SnO2、SO3、Cl、F、CeO2を0〜2質量%。
並びに任意で、着色性酸化物、例えばNd2O3、Fe2O3、CoO、NiO、V2O5、Nd2O3、MnO2、TiO2、CuO、CeO2、Cr2O3、希土類酸化物を0〜5質量%、又は「黒色ガラス」のためには0〜15質量%、並びに清澄剤、例えばAs2O3、Sb2O3、SnO2、SO3、Cl、F、CeO2を0〜2質量%。
並びに任意で、着色性酸化物、例えばNd2O3、Fe2O3、CoO、NiO、V2O5、Nd2O3、MnO2、TiO2、CuO、CeO2、Cr2O3、希土類酸化物を0〜5質量%、又は「黒色ガラス」のためには0〜15質量%、並びに清澄剤、例えばAs2O3、Sb2O3、SnO2、SO3、Cl、F、CeO2を0〜2質量%。
並びに任意で、着色性酸化物、例えばNd2O3、Fe2O3、CoO、NiO、V2O5、Nd2O3、MnO2、TiO2、CuO、CeO2、Cr2O3、希土類酸化物を0〜5質量%、又は「黒色ガラス」のためには0〜15質量%、並びに清澄剤、例えばAs2O3、Sb2O3、SnO2、SO3、Cl、F、CeO2を0〜2質量%。
並びに任意で、着色性酸化物、例えばNd2O3、Fe2O3、CoO、NiO、V2O5、Nd2O3、MnO2、TiO2、CuO、CeO2、Cr2O3、希土類酸化物を0〜5質量%、又は「黒色ガラス」のためには0〜15質量%、並びに清澄剤、例えばAs2O3、Sb2O3、SnO2、SO3、Cl、F、CeO2を0〜2質量%。
比較例2:「総発熱量試験」に耐えない合わせガラス板の構造
例4〜12は、様々な実施態様における軽量合わせガラス板を示す。
・有機層の総厚:350μm
・ガラス板の厚さ対、有機層の総厚の比、1:0.206。
例6
・有機層の総厚:200μm
・ガラス板の厚さ対、有機層の総厚の比、1:0.263。
Claims (43)
- 少なくとも1つの無機のガラス板若しくはガラスセラミック板と、少なくとも1つの有機層Aとを有する、航空機用内部窓ガラス板又は軽量窓ガラス板としての、又は、航空機の車両キャビン用の内装要素としての軽量合わせガラス板において、前記軽量合わせガラス板の単位面積あたりの質量は、その下限が、0.5kg/m2であり、その上限が5.5kg/m2であり、1つ以上の無機のガラス板若しくはガラスセラミック板の総厚対、全ての有機層の総厚の比が、1:0.01から1:1であり、全ての有機層の総厚は、350μm以下であり、前記軽量合わせガラス板は、JAR/FAR/CS 25, App.(Appendix) F, Part IV & AITM 2.0006に従って測定した絶対的な熱放出量が、65kW×分/m2未満である、前記軽量合わせガラス板。
- 前記単位面積あたりの質量の下限は、1kg/m2以上であり、
前記単位面積あたりの質量の上限は、3kg/m2以下であり、
前記1つ以上の無機のガラス板若しくはガラスセラミック板の総厚対、前記全ての有機層の総厚の比が、1:0.01から1:0.9であり、
前記全ての有機層の総厚は、300μm以下であり、
前記軽量合わせガラス板は、JAR/FAR/CS 25, App.(Appendix) F, Part IV & AITM 2.0006に従って測定した絶対的な熱放出量が、50kW×分/m2未満である、請求項1に記載の軽量合わせガラス板。 - 前記軽量合わせガラス板が耐火性を有し、該耐火性は、FAR/JAR/CS 25, App. F, Part Iに従って測定した、垂直式ブンゼンバーナー試験において炎から外した後の残炎時間が、15秒未満というものである、請求項1又は2に記載の軽量合わせガラス板。
- 前記軽量合わせガラス板の透明度が、80%超である、請求項1から3までのいずれか1項に記載の軽量合わせガラス板。
- 前記軽量合わせガラス板の光学的な散乱性が、1.5%以下である、請求項1から4までのいずれか1項に記載の軽量合わせガラス板。
- 前記少なくとも1つの無機のガラス板若しくはガラスセラミック板の厚さが、1mm以下であり、かつ200μm以上である、請求項1から5までのいずれか1項に記載の軽量合わせガラス板。
- 前記少なくとも1つの無機のガラス板が、リチウムアルミニウムケイ酸塩ガラス、ソーダ石灰ケイ酸塩ガラス、ホウケイ酸塩ガラス、アルカリ金属アルミノケイ酸塩ガラス、アルカリ金属不含若しくはアルカリ金属含分が低いアルミノケイ酸塩ガラスから成る、請求項1から6までのいずれか1項に記載の軽量合わせガラス板。
- 前記少なくとも1つの無機のガラスセラミック板が、セラミック化したアルミノケイ酸塩ガラス、若しくはリチウムアルミノケイ酸塩ガラスから成る、請求項1から7までのいずれか1項に記載の軽量合わせガラス板。
- 少なくとも1つの無機のガラス板若しくはガラスセラミック板の化学的な強化のイオン交換深さが、30μm以上である、請求項7又は8に記載の軽量合わせガラス板。
- 前記少なくとも1つの無機のガラス板若しくはガラスセラミック板の表面圧縮応力が、500MPa以上である、請求項1から9までのいずれか1項に記載の軽量合わせガラス板。
- 前記少なくとも1つの無機のガラス板若しくはガラスセラミック板の内部引張応力が、50MPa以下である、請求項1から10までのいずれか1項に記載の軽量合わせガラス板。
- 前記少なくとも1つの無機のガラス板若しくはガラスセラミック板の4点曲げ強度が、550MPa以上である、請求項1から11までのいずれか1項に記載の軽量合わせガラス板。
- 前記少なくとも1つの無機のガラス板若しくはガラスセラミック板のヤング率が、68GPa以上である、請求項1から12までのいずれか1項に記載の軽量合わせガラス板。
- 前記少なくとも1つの無機のガラス板若しくはガラスセラミック板の剪断モジュールが、25GPa以上である、請求項1から13までのいずれか1項に記載の軽量合わせガラス板。
- 前記少なくとも1つの無機のガラス板若しくはガラスセラミック板のビッカース硬度が、プレストレス加工されていない状態で、500HV2/20以上であるか、又は少なくとも1つの無機のガラス板若しくはガラスセラミック板のビッカース硬度は、プレストレス加工された状態で550HV2/20以上である、請求項1から14までのいずれか1項に記載の軽量合わせガラス板。
- 前記少なくとも1つの無機のガラス板若しくはガラスセラミック板の透明度が、80%超である、請求項1から15までのいずれか1項に記載の軽量合わせガラス板。
- 前記軽量合わせガラス板が、第二の無機のガラス板若しくはガラスセラミック板を有し、少なくとも1つの有機層Aが、1つのガラス板若しくはガラスセラミック板と、第二のガラス板若しくはガラスセラミック板との間に配置されている、請求項1から16までのいずれか1項に記載の軽量合わせガラス板。
- 前記第二の無機のガラス板若しくはガラスセラミック板が、薄層ガラスシートから成る、請求項17に記載の軽量合わせガラス板。
- 前記第二の無機のガラス板若しくはガラスセラミック板の厚さが、1000μm以下であり、かつ20μm以上である、請求項17又は18に記載の軽量合わせガラス板。
- 1つの無機のガラス板若しくはガラスセラミック板と、第二の無機のガラス板若しくはガラスセラミック板の熱膨張係数の差が、7×10-6K-1以下である、請求項17から19までのいずれか1項に記載の軽量合わせガラス板。
- 前記軽量合わせガラス板が、第二の有機層Dを有し、少なくとも1つの有機層Aが、1つの無機のガラス板若しくはガラスセラミック板と、前記第二の有機層Dとの間に配置されている、請求項1から16までのいずれか1項に記載の軽量合わせガラス板。
- 前記第二の有機層Dがポリマーシートである、請求項21に記載の軽量合わせガラス板。
- 前記ポリマーシートの透明度が、70%超である、請求項22に記載の軽量合わせガラス板。
- 前記ポリマーシートの厚さが、300μm以下である、請求項22又は23に記載の軽量合わせガラス板。
- 前記ポリマーシートが、ポリエチレンテレフタレート(PET)、ポリカーボネート(PC)、ポリメチルメタクリレート(PMMA)、ポリアミド(PA)、ポリイミド(PI)、又はポリエチレン(PE)、若しくはポリプロピレン、又はこれらの各種ブレンド、コポリマー、若しくは誘導体の1つから、又はエチレンテトラフルオロエチレン(ETFE)、ポリテトラフルオロエチレン(PTFE)、ポリ塩化ビニル(PVC)、ポリ塩化ビニリデン(PVDC)、ポリフッ化ビニリデン(PVDF)、ポリエチレンナフタレート(PEN)から、又はテトラフルオロエチレン、ヘキサフルオロプロピレン、及びフッ化ビニリデンからのターポリマー(THV)から成る、請求項22から24までのいずれか1項に記載の軽量合わせガラス板。
- 前記軽量合わせガラス板が、第二の有機層B、及び第三の有機層Cを有し、前記第二の有機層Bが、前記第一の有機層Aと、前記第三の有機層Cとの間に配置されたポリマーフィルムであり、これら3つの有機層A、B、及びCは、1つの無機のガラス板若しくはガラスセラミック板と、第二の無機のガラス板若しくはガラスセラミック板との間に、又は1つの無機のガラス板若しくはガラスセラミック板と、第二の有機層Dとの間に配置されている、請求項17から25までのいずれか1項に記載の軽量合わせガラス板。
- 前記ポリマーフィルムの厚さが、100μm以下である、請求項26に記載の軽量合わせガラス板。
- 前記ポリマーフィルムが、ポリエチレンテレフタレート(PET)、ポリカーボネート(PC)、ポリメチルメタクリレート(PMMA)、ポリアミド(PA)、ポリイミド(PI)、又はポリエチレン(PE)、若しくはポリプロピレン、又はこれらの各種ブレンド、コポリマー、若しくは誘導体の1つから、又はエチレンテトラフルオロエチレン(ETFE)、ポリテトラフルオロエチレン(PTFE)、ポリ塩化ビニル(PVC)、ポリ塩化ビニリデン(PVDC)、ポリフッ化ビニリデン(PVDF)、ポリエチレンナフタレート(PEN)から、又はテトラフルオロエチレン、ヘキサフルオロプロピレン、及びフッ化ビニリデンからのターポリマー(THV)から成る、請求項26又は27に記載の軽量合わせガラス板。
- 有機層Aの厚さが、200μm以下である、請求項1から28までのいずれか1項に記載の軽量合わせガラス板。
- 第三の有機層Cの厚さが、100μm以下である、請求項26に記載の軽量合わせガラス板。
- 有機層A及び/又は第三の有機層Cの純透過率は、88%超である、請求項26に記載の軽量合わせガラス板。
- 有機層A及び/又は第三の有機層Cが、接着フィルムとしてのポリビニルブチラール(PVB)、又はウレタン系の熱可塑性エラストマー(TPE−U)、又はイオノマー、又はエチレンビニルアセテート(EVA)、又はポリエチレン(PE)、又はポリエチレンアクリレート(EA)、又はシクロオレフィンコポリマー(COC)から、又は熱可塑性シリコーンから成る、請求項26に記載の軽量合わせガラス板。
- 有機層A及び/又は第三の有機層Cが、透明接着フィルムとして、光学透明接着剤(OCA)から成る、請求項26に記載の軽量合わせガラス板。
- 軽量合わせガラス板にそれぞれ配置された全ての材料の屈折率の差が、0.3以下である、請求項1から33までのいずれか1項に記載の軽量合わせガラス板。
- 請求項1から34までのいずれか1項に記載の軽量合わせガラス板の製造方法であって、以下の工程:
・第一のガラス板若しくはガラスセラミック板を用意する工程、ここで前記ガラス板若しくはガラスセラミック板は、第一の面で下地に置き、
・有機層Aを用意し、存在する場合には保護フィルムを、前記有機層Aの第一の面から引き剥がす工程、
・前記有機層Aを、その第一の面で、前記ガラス板若しくはガラスセラミック板の第二の面にローラで施与する工程、
・存在する場合には保護フィルムを、前記有機層Aの第二の面から引き剥がす工程、
・前記第二のガラスセラミック板若しくはガラスセラミック板、又は有機層Dを、傾いた平面を介して、又はガラスロールによって、前記有機層Aの第二の面に施与する工程、ここで前記有機層Aの第二の面と、前記第二のガラス板若しくはガラスセラミック板、又は有機層Dとの間に、閉じていく角度が存在し、前記第二のガラス板若しくはガラスセラミック板、又は前記有機層Dは、施与の前にたわみを有し、前記第二のガラス板若しくはガラスセラミック板、又は前記有機層Dが、施与後直ちに、ローラによってプレス加工される、
を有することを特徴とする、前記製造方法。 - 前記有機層A、及び/又は前記第二のガラス板若しくはガラスセラミック板をプレス加工するためのローラが、温度調整されており、25℃超に温度調整されている、請求項35に記載の軽量合わせガラス板の製造方法。
- 前記有機層Aの位置に、第一の有機層A、第二の有機層B、及び第三の有機層Cからの複合材、又はさらなる付加的な有機層との複合材、又は第一の有機層A、及び第二の有機層Dからの複合材を、前記第一のガラス板若しくはガラスセラミック板にローラで施与し、3つの有機層A、B、及びCの複合材、又はさらなる有機層との複合材、又は両方の有機層A及びDの複合材を事前に作製する、請求項35又は36に記載の軽量合わせガラス板の製造方法。
- 請求項35から37までのいずれか1項に記載の軽量合わせガラス板の製造方法であって、前記第二のガラス板若しくはガラスセラミック板、又は前記有機層Dを施与及びプレス加工した後に、さらなる工程:
軽量合わせガラス板の積層体を後処理する工程、ここで前記有機層Aは、溶融及び/又は架橋させて硬化させ、この後処理は120℃〜160℃の範囲の温度で最大6時間、任意で真空及び/又は5〜15kg/cm2の圧力を用いて行う、
が意図されている、前記製造方法。 - 航空機の車両キャビン用の内装要素としての、請求項1から34までのいずれか1項に記載の軽量合わせガラス板の使用。
- 航空機の車両キャビン用の、窓要素若しくはドア要素としての、又は窓若しくはドアの構成部材としての、又は間仕切りとしての、又は机要素としての、請求項39に記載の軽量合わせガラス板の使用。
- 航空機の内部窓ガラス板として、請求項39又は40に記載の軽量合わせガラス板の使用。
- 請求項1から34までのいずれか1項に記載の軽量合わせガラス板を用いた、航空機用内部窓ガラス板又は軽量窓ガラス板。
- 請求項42に記載の軽量合わせガラス板を有する、航空機内部窓ガラス板又は窓ガラス板であって、前記航空機内部窓ガラス板又は前記窓ガラス板がさらに、窓枠を有し、軽量合わせガラス板の基礎担持基材として用いられる第一のガラス板若しくはガラスセラミック板は、第二のガラス板若しくはガラスセラミック板よりも幅が広く、前記窓枠は、第一のガラス板若しくはガラスセラミック板の突出面に設けられている、前記航空機内部窓ガラス板又は前記窓ガラス板。
Applications Claiming Priority (3)
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PCT/EP2014/064887 WO2015010922A1 (de) | 2013-07-24 | 2014-07-11 | Verbundelement und dessen verwendung |
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JP (1) | JP6407277B2 (ja) |
CN (1) | CN105408107A (ja) |
CA (1) | CA2919071A1 (ja) |
DE (2) | DE102013214422A1 (ja) |
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-
2013
- 2013-07-24 DE DE102013214422.9A patent/DE102013214422A1/de not_active Withdrawn
-
2014
- 2014-07-11 CN CN201480041938.6A patent/CN105408107A/zh active Pending
- 2014-07-11 WO PCT/EP2014/064887 patent/WO2015010922A1/de active Application Filing
- 2014-07-11 CA CA2919071A patent/CA2919071A1/en not_active Abandoned
- 2014-07-11 DE DE112014003401.0T patent/DE112014003401A5/de active Pending
- 2014-07-11 JP JP2016528401A patent/JP6407277B2/ja active Active
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2016
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Publication number | Publication date |
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CN105408107A (zh) | 2016-03-16 |
US20160136929A1 (en) | 2016-05-19 |
WO2015010922A1 (de) | 2015-01-29 |
CA2919071A1 (en) | 2015-01-29 |
DE102013214422A1 (de) | 2015-01-29 |
JP2016531067A (ja) | 2016-10-06 |
DE112014003401A5 (de) | 2016-05-19 |
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