JP6317736B2 - パラキシレンの回収法におけるフェノールの除去 - Google Patents

パラキシレンの回収法におけるフェノールの除去 Download PDF

Info

Publication number
JP6317736B2
JP6317736B2 JP2015515013A JP2015515013A JP6317736B2 JP 6317736 B2 JP6317736 B2 JP 6317736B2 JP 2015515013 A JP2015515013 A JP 2015515013A JP 2015515013 A JP2015515013 A JP 2015515013A JP 6317736 B2 JP6317736 B2 JP 6317736B2
Authority
JP
Japan
Prior art keywords
phenol
xylene
aromatic hydrocarbon
stream
hydrocarbon stream
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2015515013A
Other languages
English (en)
Japanese (ja)
Other versions
JP2015521199A (ja
JP2015521199A5 (enExample
Inventor
ジョン ディ−イ オウ
ジョン ディ−イ オウ
グレン エイ ヒーター
グレン エイ ヒーター
シファン エル ルオ
シファン エル ルオ
インデュリス ジェイ エイランズ
インデュリス ジェイ エイランズ
ジーヴァン エス アビチャンダニ
ジーヴァン エス アビチャンダニ
アレン スコット ガウリク
アレン スコット ガウリク
マーク ダブリュ ナッシュ
マーク ダブリュ ナッシュ
テランス シー オズビー
テランス シー オズビー
ロバート ジー ティンガー
ロバート ジー ティンガー
Original Assignee
エクソンモービル ケミカル パテンツ インコーポレイテッド
エクソンモービル ケミカル パテンツ インコーポレイテッド
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by エクソンモービル ケミカル パテンツ インコーポレイテッド, エクソンモービル ケミカル パテンツ インコーポレイテッド filed Critical エクソンモービル ケミカル パテンツ インコーポレイテッド
Publication of JP2015521199A publication Critical patent/JP2015521199A/ja
Publication of JP2015521199A5 publication Critical patent/JP2015521199A5/ja
Application granted granted Critical
Publication of JP6317736B2 publication Critical patent/JP6317736B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
    • C07C2/86—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon
    • C07C2/862—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon the non-hydrocarbon contains only oxygen as hetero-atoms
    • C07C2/864—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon the non-hydrocarbon contains only oxygen as hetero-atoms the non-hydrocarbon is an alcohol
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/245—Stationary reactors without moving elements inside placed in series
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2/00—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms
    • C07C2/86—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon
    • C07C2/862—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon the non-hydrocarbon contains only oxygen as hetero-atoms
    • C07C2/865—Preparation of hydrocarbons from hydrocarbons containing a smaller number of carbon atoms by condensation between a hydrocarbon and a non-hydrocarbon the non-hydrocarbon contains only oxygen as hetero-atoms the non-hydrocarbon is an ether
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/82—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/02—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring monocyclic with no unsaturation outside the aromatic ring
    • C07C39/06—Alkylated phenols
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C5/00—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms
    • C07C5/22—Preparation of hydrocarbons from hydrocarbons containing the same number of carbon atoms by isomerisation
    • C07C5/27—Rearrangement of carbon atoms in the hydrocarbon skeleton
    • C07C5/2729—Changing the branching point of an open chain or the point of substitution on a ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/005—Processes comprising at least two steps in series
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/12—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers
    • C07C7/13—Purification; Separation; Use of additives by adsorption, i.e. purification or separation of hydrocarbons with the aid of solids, e.g. with ion-exchangers by molecular-sieve technique
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/14—Purification; Separation; Use of additives by crystallisation; Purification or separation of the crystals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/82—Phosphates
    • C07C2529/84—Aluminophosphates containing other elements, e.g. metals, boron
    • C07C2529/85—Silicoaluminophosphates (SAPO compounds)

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2015515013A 2012-05-31 2013-05-02 パラキシレンの回収法におけるフェノールの除去 Active JP6317736B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US201261653698P 2012-05-31 2012-05-31
US61/653,698 2012-05-31
US201261681501P 2012-08-09 2012-08-09
US61/681,501 2012-08-09
PCT/US2013/039193 WO2013180888A1 (en) 2012-05-31 2013-05-02 Phenol removal in paraxylene recovery process

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2016230550A Division JP2017066151A (ja) 2012-05-31 2016-11-28 パラキシレンの製造方法

Publications (3)

Publication Number Publication Date
JP2015521199A JP2015521199A (ja) 2015-07-27
JP2015521199A5 JP2015521199A5 (enExample) 2016-03-31
JP6317736B2 true JP6317736B2 (ja) 2018-04-25

Family

ID=49671056

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2015515013A Active JP6317736B2 (ja) 2012-05-31 2013-05-02 パラキシレンの回収法におけるフェノールの除去
JP2016230550A Pending JP2017066151A (ja) 2012-05-31 2016-11-28 パラキシレンの製造方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2016230550A Pending JP2017066151A (ja) 2012-05-31 2016-11-28 パラキシレンの製造方法

Country Status (7)

Country Link
US (3) US9012711B2 (enExample)
JP (2) JP6317736B2 (enExample)
KR (1) KR101632529B1 (enExample)
CN (2) CN107285975A (enExample)
BR (1) BR112014029716A2 (enExample)
TW (3) TWI537249B (enExample)
WO (1) WO2013180888A1 (enExample)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BR112014029716A2 (pt) 2012-05-31 2017-06-27 Exxonmobil Chemical Patents Inc remoção de fenol em processo de recuperação de paraxileno
US9156749B2 (en) * 2012-05-31 2015-10-13 Exxonmobil Chemical Patents Inc. Styrene removal in paraxylene recovery process
US9193645B2 (en) * 2012-08-31 2015-11-24 Exxonmobil Chemical Patents Inc. Xylene isomerization process and catalyst therefor
US9422208B2 (en) 2013-05-07 2016-08-23 Exxonmobil Chemical Patents Inc. Treatment of aromatic hydrocarbon stream
FR3010911B1 (fr) * 2013-09-20 2017-06-09 Ifp Energies Now Procede de separation des xylenes par contre courant simule traitant une charge contenant des impuretes oxygenees aromatiques de type phenols
US9598332B2 (en) 2013-12-20 2017-03-21 Exxonmobil Chemical Patents Inc. Production of para-xylene
WO2015094500A2 (en) 2013-12-20 2015-06-25 Exxonmobil Chemical Patents Inc. Production of para-xylene
WO2016003612A1 (en) 2014-06-30 2016-01-07 Exxonmobil Chemical Patents Inc. Processes for the production of para-xylene
JP6389284B2 (ja) 2014-06-30 2018-09-12 エクソンモービル・ケミカル・パテンツ・インク パラキシレンの製造方法
US9469579B2 (en) 2014-06-30 2016-10-18 Exxonmobil Chemical Patents Inc. Process for the production of xylenes
CN104292083A (zh) * 2014-10-11 2015-01-21 江苏常州酞青新材料科技有限公司 一种丙二醇苯醚精制过程中苯酚的去除方法
US9963403B2 (en) 2014-10-27 2018-05-08 Exxonmobil Chemical Patents Inc. Process and apparatus for the conversion of hydrocarbons
KR101974770B1 (ko) 2015-04-30 2019-05-02 엑손모빌 케미칼 패턴츠 인코포레이티드 파라-자일렌의 제조를 위한 방법 및 장치
CN110914229B (zh) 2017-11-21 2023-01-31 中国石油化工股份有限公司 从煤衍生的液体制备二甲苯和苯酚的方法
US20190241485A1 (en) 2017-12-22 2019-08-08 Exxonmobil Chemical Patents Inc. Catalysts for Producing Paraxylene by Methylation of Benzene and/or Toluene
US11053176B2 (en) 2018-03-30 2021-07-06 Exxonmobil Chemical Patents Inc. Process for co-production of mixed xylenes and high octane C9+ aromatics
TWI773974B (zh) 2019-03-29 2022-08-11 美商艾克頌美孚化學專利股份有限公司 新穎沸石，其製法，及其於轉化芳族烴之用途
KR20210126101A (ko) 2019-03-29 2021-10-19 엑손모빌 케미칼 패턴츠 인코포레이티드 방향족 탄화수소 전환용 mel형 제올라이트, 상기 제올라이트의 제조 방법, 및 상기 제올라이트를 포함하는 촉매 조성물
CN110746255A (zh) * 2019-09-24 2020-02-04 陕西煤化工技术工程中心有限公司 一种粗苯制对二甲苯的方法
CN113443992B (zh) * 2020-03-25 2022-09-27 天津大加化工有限公司 一种低苯酚含量的水杨酸甲酯的制备方法
FR3112289B1 (fr) * 2020-07-10 2022-07-22 Arkema France Purification de liquides aromatiques

Family Cites Families (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2943105A (en) 1957-12-23 1960-06-28 Pan American Petroleum Corp Treatment of hydrocarbon solutions of oxygenated chemicals with solid adsorbents
NL127084C (enExample) 1958-03-03
US3409691A (en) 1966-02-01 1968-11-05 Dow Chemical Co Porous cation exchange resins as selective sorbents in organic systems
US3751507A (en) 1971-07-12 1973-08-07 Rohm & Haas Adsorption process
US4064042A (en) 1975-02-18 1977-12-20 Rohm And Haas Company Purification of blood using partially pyrolyzed polymer particles
JPS5231038A (en) * 1975-09-01 1977-03-09 Toray Ind Inc Separation process of p-xylene by adsorption
JPS54125619A (en) * 1978-03-17 1979-09-29 Teijin Yuka Kk Method of reforming hydrocarbons
JPS6059887B2 (ja) 1979-09-07 1985-12-27 住友化学工業株式会社 有機化合物中に含まれるフェノ−ル類の除去方法
US4453029A (en) 1979-12-19 1984-06-05 Mobil Oil Corporation Selective sorption by zeolites
US4404118A (en) 1981-12-28 1983-09-13 Uop Inc. Regeneration of adsorbents by low temperature hydrogen stripping
US4469805A (en) 1982-10-25 1984-09-04 Gulf Research & Development Company Regeneration of filter clay with liquid methanol
US4899017A (en) * 1987-07-27 1990-02-06 Mobil Oil Corporation Process for the selective separation of para-xylene from C8 aromatic mixtures
GB9017344D0 (en) 1990-08-08 1990-09-19 Laporte Industries Ltd Absorbents and a method for their production
JPH07215901A (ja) 1994-01-28 1995-08-15 Mitsui Toatsu Chem Inc フェノールの分離方法
US6376733B1 (en) * 1996-01-25 2002-04-23 Exxonmobil Chemical Patents Inc. Process for production of paraxylene
US6423879B1 (en) 1997-10-02 2002-07-23 Exxonmobil Oil Corporation Selective para-xylene production by toluene methylation
WO1999038823A1 (en) 1998-01-30 1999-08-05 Exxon Chemical Patents Inc. Reactive distillation process for the production of xylenes
CN1073977C (zh) 1998-11-18 2001-10-31 中国石油化工集团公司 苯乙烯单体的纯化方法
US6313362B1 (en) 1998-12-17 2001-11-06 Exxonmobil Corporation Aromatic alkylation process
WO2001068242A1 (en) 2000-03-14 2001-09-20 Kyowa Chemical Industry Co., Ltd. Adsorbent for aromatic hydroxy compound and utilization thereof
US6281406B1 (en) * 2000-03-31 2001-08-28 Chevron Corporation Adsorption process for paraxylene purifacation using Cs SSZ-25 adsorbent with benzene desorbent
FR2823131B1 (fr) 2001-04-04 2004-10-22 Pro Catalyse Procede d'elimination des molecules oxygenees organiques presentes dans un effluent organique, utilisant des agglomeres d'alumine
WO2008033200A1 (en) * 2006-09-14 2008-03-20 Exxonmobil Chemical Patents Inc. Process for producing para-xylene
WO2009119725A1 (ja) * 2008-03-27 2009-10-01 株式会社ジャパンエナジー パラ置換芳香族炭化水素の製造方法
US8115041B2 (en) * 2008-04-02 2012-02-14 Saudi Basic Industries Corporation Pretreatment of a phosphorus-modified zeolite catalyst for an aromatic alkylation process
JP5495531B2 (ja) * 2008-10-09 2014-05-21 Ｊｘ日鉱日石エネルギー株式会社 パラキシレン製造用合成ゼオライト触媒の製造方法、並びに該方法で製造したパラキシレン製造用触媒を用いた高純度パラキシレンの製造方法
US8252967B2 (en) 2009-04-14 2012-08-28 Exxonmobil Chemical Patents Inc. Process for the purification of paraxylene
EP2632880A4 (en) * 2010-10-29 2016-01-27 Exxonmobil Chem Patents Inc PROCESS FOR PRODUCTION OF PARAXYLENE
US9295962B2 (en) 2011-06-10 2016-03-29 Exxonmobil Chemical Patents Inc. Production of para-xylene
BR112014029716A2 (pt) 2012-05-31 2017-06-27 Exxonmobil Chemical Patents Inc remoção de fenol em processo de recuperação de paraxileno
US9156749B2 (en) 2012-05-31 2015-10-13 Exxonmobil Chemical Patents Inc. Styrene removal in paraxylene recovery process
WO2014047356A1 (en) 2012-09-24 2014-03-27 Exxonmobil Chemical Patents Inc. Functionalized resins obtained via olefin metathesis
US9963403B2 (en) * 2014-10-27 2018-05-08 Exxonmobil Chemical Patents Inc. Process and apparatus for the conversion of hydrocarbons

Also Published As

Publication number Publication date
JP2017066151A (ja) 2017-04-06
WO2013180888A1 (en) 2013-12-05
WO2013180888A8 (en) 2014-07-24
US9434661B2 (en) 2016-09-06
CN104395272A (zh) 2015-03-04
BR112014029716A2 (pt) 2017-06-27
JP2015521199A (ja) 2015-07-27
TW201813948A (zh) 2018-04-16
TWI640506B (zh) 2018-11-11
US9012711B2 (en) 2015-04-21
TW201613844A (en) 2016-04-16
CN107285975A (zh) 2017-10-24
TW201406721A (zh) 2014-02-16
US20130324780A1 (en) 2013-12-05
KR101632529B1 (ko) 2016-06-21
US9205401B2 (en) 2015-12-08
TWI537249B (zh) 2016-06-11
US20150314261A1 (en) 2015-11-05
KR20150013615A (ko) 2015-02-05
TWI624455B (zh) 2018-05-21
US20150299070A1 (en) 2015-10-22

Similar Documents

Publication Publication Date Title
JP6317736B2 (ja) パラキシレンの回収法におけるフェノールの除去
JP5908655B2 (ja) パラキシレンの回収法におけるスチレンの除去
US9295962B2 (en) Production of para-xylene
JP5470448B2 (ja) パラキシレンの精製方法
KR102120885B1 (ko) 톨루엔 및/또는 벤젠의 메틸화에 의한 파라-자일렌의 제조에서의 오프 가스의 처리
KR101974770B1 (ko) 파라-자일렌의 제조를 위한 방법 및 장치
WO2016032639A1 (en) Treatment of aromatic alkylation feedstock

Legal Events

Date Code Title Description
A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20151030

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20151109

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20160208

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20160727

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20171225

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20180330

R150 Certificate of patent or registration of utility model

Ref document number: 6317736

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150