JP6235769B2 - フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法 - Google Patents

フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法 Download PDF

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Publication number
JP6235769B2
JP6235769B2 JP2011511056A JP2011511056A JP6235769B2 JP 6235769 B2 JP6235769 B2 JP 6235769B2 JP 2011511056 A JP2011511056 A JP 2011511056A JP 2011511056 A JP2011511056 A JP 2011511056A JP 6235769 B2 JP6235769 B2 JP 6235769B2
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Prior art keywords
reaction
oxime
microreactor
photonitration
beckmann
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Japanese (ja)
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JP2011521004A (ja
JP2011521004A5 (enExample
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ティエリ オベール，
ティエリ オベール，
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Arkema France SA
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Arkema France SA
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/04—Preparation of lactams from or via oximes by Beckmann rearrangement
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/10—Preparation of lactams from cycloaliphatic compounds by simultaneous nitrosylation and rearrangement
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/06—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by nitrosation of hydrocarbons or substituted hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D225/00—Heterocyclic compounds containing rings of more than seven members having one nitrogen atom as the only ring hetero atom
    • C07D225/02—Heterocyclic compounds containing rings of more than seven members having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D227/00—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00
    • C07D227/02—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00 with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D227/06—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00 with only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D227/08—Oxygen atoms
    • C07D227/087—One doubly-bound oxygen atom in position 2, e.g. lactams
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/18—Systems containing only non-condensed rings with a ring being at least seven-membered
    • C07C2601/20—Systems containing only non-condensed rings with a ring being at least seven-membered the ring being twelve-membered

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
JP2011511056A 2008-05-26 2009-05-14 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法 Active JP6235769B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR08.53419 2008-05-26
FR0853419A FR2931478B1 (fr) 2008-05-26 2008-05-26 Prodece de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann
PCT/FR2009/050886 WO2009153470A1 (fr) 2008-05-26 2009-05-14 Procede de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann

Related Child Applications (2)

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JP2015117852A Division JP6567332B2 (ja) 2008-05-26 2015-06-10 フォトニトロゼーション段階とそれに続くベックマン転位とを含むラクタムの製造方法
JP2017003575A Division JP2017081987A (ja) 2008-05-26 2017-01-12 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法

Publications (3)

Publication Number Publication Date
JP2011521004A JP2011521004A (ja) 2011-07-21
JP2011521004A5 JP2011521004A5 (enExample) 2017-10-12
JP6235769B2 true JP6235769B2 (ja) 2017-11-22

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ID=40134955

Family Applications (5)

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JP2011511056A Active JP6235769B2 (ja) 2008-05-26 2009-05-14 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法
JP2015117852A Active JP6567332B2 (ja) 2008-05-26 2015-06-10 フォトニトロゼーション段階とそれに続くベックマン転位とを含むラクタムの製造方法
JP2017003575A Pending JP2017081987A (ja) 2008-05-26 2017-01-12 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法
JP2017075888A Pending JP2017132797A (ja) 2008-05-26 2017-04-06 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法
JP2018235757A Pending JP2019055999A (ja) 2008-05-26 2018-12-17 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法

Family Applications After (4)

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JP2015117852A Active JP6567332B2 (ja) 2008-05-26 2015-06-10 フォトニトロゼーション段階とそれに続くベックマン転位とを含むラクタムの製造方法
JP2017003575A Pending JP2017081987A (ja) 2008-05-26 2017-01-12 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法
JP2017075888A Pending JP2017132797A (ja) 2008-05-26 2017-04-06 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法
JP2018235757A Pending JP2019055999A (ja) 2008-05-26 2018-12-17 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法

Country Status (7)

Country Link
US (2) US20110137027A1 (enExample)
EP (2) EP2291357B1 (enExample)
JP (5) JP6235769B2 (enExample)
CN (2) CN103588706B (enExample)
FR (1) FR2931478B1 (enExample)
PL (2) PL3101011T3 (enExample)
WO (1) WO2009153470A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2017132797A (ja) * 2008-05-26 2017-08-03 アルケマ フランス フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法

Families Citing this family (12)

* Cited by examiner, † Cited by third party
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JP5359064B2 (ja) * 2008-06-30 2013-12-04 東レ株式会社 シクロアルカノンオキシムの製造方法および光化学反応装置
JP5359063B2 (ja) * 2008-06-30 2013-12-04 東レ株式会社 シクロアルカノンオキシムの製造方法
JP5821623B2 (ja) * 2010-12-28 2015-11-24 東レ株式会社 シクロアルカノンオキシムの製造方法およびラクタムを製造する方法
KR101276149B1 (ko) 2012-06-26 2013-06-18 도레이 카부시키가이샤 시클로알카논 옥심의 제조 방법
TWI564278B (zh) 2012-06-27 2017-01-01 東麗股份有限公司 環烷酮肟之製造方法及內醯胺之製造方法
ES2794123T3 (es) * 2014-10-09 2020-11-17 Toray Industries Dispositivo de reacción fotoquímica, método de reacción fotoquímica que lo utiliza, y método de producción de lactamas para utilizar dicho método
CN107438594B (zh) 2015-04-02 2020-11-06 安西娅芳香剂私人有限公司 一种用于合成环酰胺的有效的工艺
WO2017133995A1 (de) 2016-02-01 2017-08-10 Basf Se Verfahren zur herstellung von c4-c15-lactamen
CN108409646B (zh) * 2018-01-19 2020-05-19 南京红太阳生物化学有限责任公司 一种烟酰胺的合成方法
FR3107612B1 (fr) 2020-02-20 2022-03-04 Arkema France Lampe pour réacteur photochimique à base de diodes électroluminescentes
CN115260073B (zh) * 2022-08-31 2024-09-20 中国天辰工程有限公司 一种无硫酸铵副产重排工艺制备月桂精内酰胺的方法
CN119258936B (zh) * 2023-07-07 2025-11-11 中国石油化工股份有限公司 一种微反应设备脱除原油中有机氯的方法

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FR2417501A1 (fr) * 1978-02-17 1979-09-14 Ato Chimie Procede de preparation de lactames par isomerisation d'oximes en milieu sulfurique
BE893651A (fr) * 1982-06-25 1982-12-27 Desaar Rene Nez poreux pour le bullage d'acier
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FR2784103B1 (fr) * 1998-09-21 2000-12-08 Atochem Elf Sa Procede de preparation de lauryllactame par photonitrosation de cyclododecane et transposition de beckmann en presence d'acide methanesulfonique
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JP5110779B2 (ja) * 2005-07-21 2012-12-26 日東電工株式会社 光反応生成物シート類の製造方法及び装置
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JP5030222B2 (ja) 2006-09-08 2012-09-19 国立大学法人東京工業大学 光触媒系マイクロ反応装置
JP2009235365A (ja) 2008-03-28 2009-10-15 Toyota Motor Corp ポリ乳酸複合成形体、ポリ乳酸複合成形体の製造方法及び自動車内装材用表面部材
FR2931478B1 (fr) * 2008-05-26 2012-08-03 Arkema France Prodece de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann
JP5359063B2 (ja) * 2008-06-30 2013-12-04 東レ株式会社 シクロアルカノンオキシムの製造方法
JP5359064B2 (ja) * 2008-06-30 2013-12-04 東レ株式会社 シクロアルカノンオキシムの製造方法および光化学反応装置

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2017132797A (ja) * 2008-05-26 2017-08-03 アルケマ フランス フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法

Also Published As

Publication number Publication date
JP2019055999A (ja) 2019-04-11
WO2009153470A1 (fr) 2009-12-23
CN102046604B (zh) 2015-02-25
JP2011521004A (ja) 2011-07-21
FR2931478A1 (fr) 2009-11-27
CN103588706B (zh) 2016-08-24
EP2291357A1 (fr) 2011-03-09
CN103588706A (zh) 2014-02-19
JP2017132797A (ja) 2017-08-03
PL3101011T3 (pl) 2018-09-28
PL2291357T3 (pl) 2016-12-30
US20140246303A1 (en) 2014-09-04
EP3101011B1 (fr) 2018-06-20
CN102046604A (zh) 2011-05-04
US20110137027A1 (en) 2011-06-09
EP2291357B1 (fr) 2016-07-13
JP2017081987A (ja) 2017-05-18
JP2015157871A (ja) 2015-09-03
US9499481B2 (en) 2016-11-22
EP3101011A1 (fr) 2016-12-07
JP6567332B2 (ja) 2019-08-28
FR2931478B1 (fr) 2012-08-03

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