FR2931478B1 - Prodece de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann - Google Patents

Prodece de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann

Info

Publication number
FR2931478B1
FR2931478B1 FR0853419A FR0853419A FR2931478B1 FR 2931478 B1 FR2931478 B1 FR 2931478B1 FR 0853419 A FR0853419 A FR 0853419A FR 0853419 A FR0853419 A FR 0853419A FR 2931478 B1 FR2931478 B1 FR 2931478B1
Authority
FR
France
Prior art keywords
product
photonitrosation
followed
beckmann transposition
preparing lactams
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR0853419A
Other languages
English (en)
French (fr)
Other versions
FR2931478A1 (fr
Inventor
Thierry Aubert
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR0853419A priority Critical patent/FR2931478B1/fr
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to EP16176645.6A priority patent/EP3101011B1/fr
Priority to PL16176645T priority patent/PL3101011T3/pl
Priority to JP2011511056A priority patent/JP6235769B2/ja
Priority to CN201310505599.XA priority patent/CN103588706B/zh
Priority to CN200980119112.6A priority patent/CN102046604B/zh
Priority to PL09766032.8T priority patent/PL2291357T3/pl
Priority to EP09766032.8A priority patent/EP2291357B1/fr
Priority to PCT/FR2009/050886 priority patent/WO2009153470A1/fr
Priority to US12/993,975 priority patent/US20110137027A1/en
Publication of FR2931478A1 publication Critical patent/FR2931478A1/fr
Application granted granted Critical
Publication of FR2931478B1 publication Critical patent/FR2931478B1/fr
Priority to US14/252,610 priority patent/US9499481B2/en
Priority to JP2015117852A priority patent/JP6567332B2/ja
Priority to JP2017003575A priority patent/JP2017081987A/ja
Priority to JP2017075888A priority patent/JP2017132797A/ja
Priority to JP2018235757A priority patent/JP2019055999A/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/10—Preparation of lactams from cycloaliphatic compounds by simultaneous nitrosylation and rearrangement
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/06—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by nitrosation of hydrocarbons or substituted hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/04—Preparation of lactams from or via oximes by Beckmann rearrangement
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D225/00—Heterocyclic compounds containing rings of more than seven members having one nitrogen atom as the only ring hetero atom
    • C07D225/02—Heterocyclic compounds containing rings of more than seven members having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D227/00—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00
    • C07D227/02—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00 with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D227/06—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00 with only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D227/08—Oxygen atoms
    • C07D227/087—One doubly-bound oxygen atom in position 2, e.g. lactams
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/18—Systems containing only non-condensed rings with a ring being at least seven-membered
    • C07C2601/20—Systems containing only non-condensed rings with a ring being at least seven-membered the ring being twelve-membered

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
FR0853419A 2008-05-26 2008-05-26 Prodece de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann Active FR2931478B1 (fr)

Priority Applications (15)

Application Number Priority Date Filing Date Title
FR0853419A FR2931478B1 (fr) 2008-05-26 2008-05-26 Prodece de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann
US12/993,975 US20110137027A1 (en) 2008-05-26 2009-05-14 Method for preparing lactames, comprising a photonitrosation step, followed by a beckmann transposition step
JP2011511056A JP6235769B2 (ja) 2008-05-26 2009-05-14 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法
CN201310505599.XA CN103588706B (zh) 2008-05-26 2009-05-14 包括光亚硝化步骤然后贝克曼重排作用步骤的制备内酰胺的方法
CN200980119112.6A CN102046604B (zh) 2008-05-26 2009-05-14 包括光亚硝化步骤然后贝克曼重排作用步骤的制备内酰胺的方法
PL09766032.8T PL2291357T3 (pl) 2008-05-26 2009-05-14 Sposób wytwarzania laktamów obejmujący etap fotonitrozowania, a następnie etap przegrupowania Beckmanna
EP09766032.8A EP2291357B1 (fr) 2008-05-26 2009-05-14 Procede de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann
PCT/FR2009/050886 WO2009153470A1 (fr) 2008-05-26 2009-05-14 Procede de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann
EP16176645.6A EP3101011B1 (fr) 2008-05-26 2009-05-14 Procédé de préparation de lactames comprenant une étape de photonitrosation suivie d'une étape de transposition de beckmann
PL16176645T PL3101011T3 (pl) 2008-05-26 2009-05-14 Sposób wytwarzania laktamów obejmujący etap fotonitrozowania, a następnie etap przegrupowania Beckmanna
US14/252,610 US9499481B2 (en) 2008-05-26 2014-04-14 Method for preparing lactames, comprising a photonitrosation step, followed by a Beckmann transposition step
JP2015117852A JP6567332B2 (ja) 2008-05-26 2015-06-10 フォトニトロゼーション段階とそれに続くベックマン転位とを含むラクタムの製造方法
JP2017003575A JP2017081987A (ja) 2008-05-26 2017-01-12 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法
JP2017075888A JP2017132797A (ja) 2008-05-26 2017-04-06 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法
JP2018235757A JP2019055999A (ja) 2008-05-26 2018-12-17 フォトニトロゼーション段階とそれに続くベックマン転移とを含むラクタムの製造方法

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR0853419A FR2931478B1 (fr) 2008-05-26 2008-05-26 Prodece de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann

Publications (2)

Publication Number Publication Date
FR2931478A1 FR2931478A1 (fr) 2009-11-27
FR2931478B1 true FR2931478B1 (fr) 2012-08-03

Family

ID=40134955

Family Applications (1)

Application Number Title Priority Date Filing Date
FR0853419A Active FR2931478B1 (fr) 2008-05-26 2008-05-26 Prodece de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann

Country Status (7)

Country Link
US (2) US20110137027A1 (enExample)
EP (2) EP2291357B1 (enExample)
JP (5) JP6235769B2 (enExample)
CN (2) CN102046604B (enExample)
FR (1) FR2931478B1 (enExample)
PL (2) PL2291357T3 (enExample)
WO (1) WO2009153470A1 (enExample)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2931478B1 (fr) * 2008-05-26 2012-08-03 Arkema France Prodece de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann
JP5359064B2 (ja) * 2008-06-30 2013-12-04 東レ株式会社 シクロアルカノンオキシムの製造方法および光化学反応装置
JP5359063B2 (ja) * 2008-06-30 2013-12-04 東レ株式会社 シクロアルカノンオキシムの製造方法
JP5821623B2 (ja) * 2010-12-28 2015-11-24 東レ株式会社 シクロアルカノンオキシムの製造方法およびラクタムを製造する方法
ES2526796T3 (es) 2012-06-26 2015-01-15 Toray Industries, Inc. Método de producción de oxima de cicloalcanona
US9932296B2 (en) 2012-06-27 2018-04-03 Toray Industries, Inc. Method of producing cycloalkanone oxime
CN107073433B (zh) * 2014-10-09 2020-01-31 东丽株式会社 光化学反应装置、使用该装置的光化学反应方法
EP3277664B1 (en) 2015-04-02 2019-08-07 Anthea Aromatics Private Limited An efficient process for the synthesis of cyclic amides
US10618873B2 (en) 2016-02-01 2020-04-14 Basf Se Method for producing C4-C15 lactams
CN108409646B (zh) * 2018-01-19 2020-05-19 南京红太阳生物化学有限责任公司 一种烟酰胺的合成方法
FR3107612B1 (fr) 2020-02-20 2022-03-04 Arkema France Lampe pour réacteur photochimique à base de diodes électroluminescentes
CN115260073B (zh) * 2022-08-31 2024-09-20 中国天辰工程有限公司 一种无硫酸铵副产重排工艺制备月桂精内酰胺的方法
CN119258936B (zh) * 2023-07-07 2025-11-11 中国石油化工股份有限公司 一种微反应设备脱除原油中有机氯的方法
EP4733296A1 (en) 2024-10-22 2026-04-29 Basf Se Process for the preparation of 2-c3-c4 alkanone oximes

Family Cites Families (21)

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Publication number Priority date Publication date Assignee Title
US3553091A (en) * 1966-08-17 1971-01-05 Fumio Nishikawa Method of photonitrosation of cycloalkanes
US3652552A (en) * 1966-12-16 1972-03-28 Stamicarbon Preparation of lactams from cycloalkanes
FR2417501A1 (fr) * 1978-02-17 1979-09-14 Ato Chimie Procede de preparation de lactames par isomerisation d'oximes en milieu sulfurique
BE893651A (fr) * 1982-06-25 1982-12-27 Desaar Rene Nez poreux pour le bullage d'acier
CN1109671C (zh) * 1997-07-02 2003-05-28 埃勒夫阿托化学有限公司 在一种基本无水的介质氯仿中的环十二烷的光亚硝化
FR2784103B1 (fr) * 1998-09-21 2000-12-08 Atochem Elf Sa Procede de preparation de lauryllactame par photonitrosation de cyclododecane et transposition de beckmann en presence d'acide methanesulfonique
JP2000164931A (ja) 1998-11-27 2000-06-16 Sumitomo Electric Ind Ltd 白色光源
JP2001002636A (ja) * 1999-06-15 2001-01-09 Toray Ind Inc ラクタムの製造方法
DE10016106A1 (de) * 2000-03-31 2001-10-04 Merck Patent Gmbh Verfahren zur Beckmann-Umlagerung organischer Oxime
US6871982B2 (en) * 2003-01-24 2005-03-29 Digital Optics International Corporation High-density illumination system
EP1775875A1 (en) 2004-08-04 2007-04-18 Matsushita Electric Industrial Co., Ltd. Radio communication device, radio communication system, and radio communication method
DE102005003966A1 (de) * 2005-01-27 2006-08-10 Ehrfeld Mikrotechnik Bts Gmbh Vorrichtung zur kontinuierlichen Durchführung photochemischer Prozesse mit geringen optischen Schichtdicken, enger Verweilzeitverteilung und hohen Durchsätzen
FR2887250B1 (fr) * 2005-06-21 2009-10-02 Arkema Sa Procede de synthese du lauryllactame (l12) par rearrangement catalytique en phase gazeuse de la cyclododecanone oxime
JP5110779B2 (ja) * 2005-07-21 2012-12-26 日東電工株式会社 光反応生成物シート類の製造方法及び装置
JP5083205B2 (ja) 2006-03-10 2012-11-28 日亜化学工業株式会社 発光装置
KR20090019871A (ko) * 2006-05-31 2009-02-25 크리 엘이디 라이팅 솔루션즈, 인크. 조명 장치 및 조명 방법
JP5030222B2 (ja) 2006-09-08 2012-09-19 国立大学法人東京工業大学 光触媒系マイクロ反応装置
JP2009235365A (ja) 2008-03-28 2009-10-15 Toyota Motor Corp ポリ乳酸複合成形体、ポリ乳酸複合成形体の製造方法及び自動車内装材用表面部材
FR2931478B1 (fr) * 2008-05-26 2012-08-03 Arkema France Prodece de preparation de lactames comprenant une etape de photonitrosation suivie d'une etape de transposition de beckmann
JP5359063B2 (ja) * 2008-06-30 2013-12-04 東レ株式会社 シクロアルカノンオキシムの製造方法
JP5359064B2 (ja) * 2008-06-30 2013-12-04 東レ株式会社 シクロアルカノンオキシムの製造方法および光化学反応装置

Also Published As

Publication number Publication date
US9499481B2 (en) 2016-11-22
US20110137027A1 (en) 2011-06-09
JP6235769B2 (ja) 2017-11-22
CN103588706A (zh) 2014-02-19
FR2931478A1 (fr) 2009-11-27
CN102046604B (zh) 2015-02-25
JP2019055999A (ja) 2019-04-11
EP2291357B1 (fr) 2016-07-13
JP2015157871A (ja) 2015-09-03
JP6567332B2 (ja) 2019-08-28
US20140246303A1 (en) 2014-09-04
JP2017132797A (ja) 2017-08-03
PL2291357T3 (pl) 2016-12-30
CN102046604A (zh) 2011-05-04
EP2291357A1 (fr) 2011-03-09
JP2011521004A (ja) 2011-07-21
PL3101011T3 (pl) 2018-09-28
JP2017081987A (ja) 2017-05-18
CN103588706B (zh) 2016-08-24
WO2009153470A1 (fr) 2009-12-23
EP3101011B1 (fr) 2018-06-20
EP3101011A1 (fr) 2016-12-07

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