JP6108397B2 - プロセス材料から金属を回収する方法およびその方法を実施するための反応器 - Google Patents
プロセス材料から金属を回収する方法およびその方法を実施するための反応器 Download PDFInfo
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- JP6108397B2 JP6108397B2 JP2013508330A JP2013508330A JP6108397B2 JP 6108397 B2 JP6108397 B2 JP 6108397B2 JP 2013508330 A JP2013508330 A JP 2013508330A JP 2013508330 A JP2013508330 A JP 2013508330A JP 6108397 B2 JP6108397 B2 JP 6108397B2
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D7/00—Sublimation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
- B01D1/24—Evaporating by bringing a thin layer of the liquid into contact with a heated surface to obtain dry solids
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- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
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- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1263—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction
- C22B34/1268—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams
- C22B34/1272—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds, e.g. by reduction using alkali or alkaline-earth metals or amalgams reduction of titanium halides, e.g. Kroll process
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/129—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08 obtaining metallic titanium from titanium compounds by dissociation, e.g. thermic dissociation of titanium tetraiodide, or by electrolysis or with the use of an electric arc
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/12—Obtaining titanium or titanium compounds from ores or scrap by metallurgical processing; preparation of titanium compounds from other titanium compounds see C01G23/00 - C01G23/08
- C22B34/1295—Refining, melting, remelting, working up of titanium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/10—Obtaining titanium, zirconium or hafnium
- C22B34/14—Obtaining zirconium or hafnium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/02—Refining by liquating, filtering, centrifuging, distilling, or supersonic wave action including acoustic waves
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
- C22B9/04—Refining by applying a vacuum
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/40—Alkaline earth metal or magnesium compounds
- B01D2251/402—Alkaline earth metal or magnesium compounds of magnesium
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- General Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Acoustics & Sound (AREA)
- Physics & Mathematics (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Furnace Charging Or Discharging (AREA)
- Muffle Furnaces And Rotary Kilns (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Description
炉に設けられたレトルト内にプロセス材料を輸送するステップであって、レトルトが真空下でかつプロセス材料からの成分の昇華を引き起こす程度に十分な温度で操作され、これによって精製金属を製造するステップと、
昇華した成分を低温の表面に堆積するステップと、
精製金属をレトルトから取り出すステップと、
堆積した成分を低温の表面から取り出すステップと
を含む方法を提供する。
炉と、
炉内にまた炉を通して延びるレトルトであって、プロセス材料をレトルト内に送出するための入口と、プロセス材料から揮発物を昇華した後にレトルトから金属を取り出すための出口とを備えるレトルトと、
プロセス材料から昇華した揮発物を堆積するための表面であって、レトルトから揮発物を受容するための入口と、堆積された揮発物を表面から取り出すための出口とを備える表面と、を備える。
Claims (5)
- 金属と、金属よりも揮発性である成分とを含むプロセス材料から金属を回収する方法において、
炉に設けられたレトルトにおいて前記プロセス材料を輸送するステップであって、焼結を制御しつつ、前記レトルトが真空下でかつプロセス材料からの成分の昇華を引き起こす程度に十分な温度で操作され、これによって精製金属を製造するステップと、
昇華された前記成分を低温の表面に堆積するステップと、
精製金属を前記レトルトから取り出すステップと、
堆積した成分を前記低温の表面から取り出すステップと、を含み、
当該方法が連続的に操作され、新鮮なプロセス材料が前記レトルト及び炉に連続的に供給され、精製金属及び堆積された揮発性成分が連続的に取り出され、
前記金属がチタンであり、前記プロセス材料が、マグネシウムによる四塩化チタンの還元によって製造されることを特徴とする方法。 - 請求項1に記載の方法において、揮発性成分が昇華ステップで昇華するように、前記方法を、温度及び圧力の条件下で、選択された金属含有プロセス材料に実施することを特徴とする方法。
- 請求項1に記載の方法において、前記プロセス材料が、回転するスクリューを使用して前記レトルトにおいて輸送されることを特徴とする方法。
- 請求項1の方法を実施するための反応器において、
炉と、
前記炉内にまた前記炉を通して延びるレトルトであって、プロセス材料を前記レトルト内に連続的に送出するための入口と、前記プロセス材料から揮発物を昇華した後に前記レトルトから金属を連続的に取り出すための出口とを備えるレトルトと、
前記プロセス材料から昇華した揮発物を堆積するための表面であって、前記レトルトから揮発物を受容するための入口と、堆積された揮発物を前記表面から取り出すための出口とを備える表面と、
前記入口から前記レトルトに沿って前記反応器の高温ゾーン内にプロセス材料を連続的に輸送するための機構と、揮発物が昇華したプロセス材料を前記レトルトの出口に連続的に輸送するための機構と
を備えることを特徴とする反応器。 - 請求項4に記載の反応器において、前記レトルトが、昇華スクリューを含む昇華レトルトの形態をとり、揮発物を堆積するための前記表面が、堆積スクリューを含む堆積レトルトの形態をとることを特徴とする反応器。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
AU2010901904A AU2010901904A0 (en) | 2010-05-04 | Separation method | |
AU2010901904 | 2010-05-04 | ||
PCT/AU2011/000516 WO2011137489A1 (en) | 2010-05-04 | 2011-05-04 | Separation method |
Publications (2)
Publication Number | Publication Date |
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JP2013529252A JP2013529252A (ja) | 2013-07-18 |
JP6108397B2 true JP6108397B2 (ja) | 2017-04-05 |
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JP2013508330A Expired - Fee Related JP6108397B2 (ja) | 2010-05-04 | 2011-05-04 | プロセス材料から金属を回収する方法およびその方法を実施するための反応器 |
Country Status (11)
Country | Link |
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US (1) | US10035078B2 (ja) |
EP (1) | EP2569068B1 (ja) |
JP (1) | JP6108397B2 (ja) |
KR (1) | KR20130058707A (ja) |
CN (1) | CN102985148B (ja) |
AU (1) | AU2011250655B2 (ja) |
CA (1) | CA2798262A1 (ja) |
EA (1) | EA027761B1 (ja) |
NZ (1) | NZ603297A (ja) |
WO (1) | WO2011137489A1 (ja) |
ZA (1) | ZA201209070B (ja) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102560152B (zh) * | 2012-01-18 | 2014-03-26 | 深圳市新星轻合金材料股份有限公司 | 一种用于海绵钛生产的反应设备 |
WO2017027914A1 (en) | 2015-08-14 | 2017-02-23 | Coogee Titanium Pty Ltd | Method for recovery of metal-containing material from a composite material |
WO2017027915A1 (en) | 2015-08-14 | 2017-02-23 | Coogee Titanium Pty Ltd | Method for production of a composite material using excess oxidant |
US10960469B2 (en) | 2015-08-14 | 2021-03-30 | Coogee Titanium Pty Ltd | Methods using high surface area per volume reactive particulate |
AU2017280091A1 (en) | 2016-06-20 | 2018-11-22 | Othrys Technologies Pty Ltd | Coating of particulate substrates |
CN114829037A (zh) * | 2019-12-04 | 2022-07-29 | 曼特尔公司 | 炉系统及使用方法 |
CN110938799B (zh) * | 2019-12-17 | 2022-07-29 | 宁波海秀丰科技有限公司 | 一种高纯高均匀性金靶材及其制备方法与应用 |
Family Cites Families (22)
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US2734244A (en) * | 1956-02-14 | herres | ||
US1594344A (en) * | 1922-11-01 | 1926-08-03 | American Magnesium Corp | Production of magnesium |
US1814072A (en) * | 1926-01-11 | 1931-07-14 | American Magnesium Corp | Separating volatile metals by sublimation |
US2878008A (en) * | 1955-07-22 | 1959-03-17 | Ishizuka Hiroshi | Apparatus for continuous vacuum refining of sponge metallic titanium |
DE1071350B (ja) * | 1956-03-20 | |||
US3356491A (en) * | 1966-07-26 | 1967-12-05 | Oregon Metallurgical Corp | Purification of contaminated reactive metal products |
GB1321374A (en) * | 1971-03-01 | 1973-06-27 | Vni Pi Aljuminievoi Magnievoi | Apparatus for metal production |
JPS58210128A (ja) * | 1982-05-31 | 1983-12-07 | Hiroshi Ishizuka | 金属塩化物の還元及び精製のための装置及び方法 |
GB2140141B (en) | 1983-05-20 | 1986-10-01 | British Petroleum Co Plc | Process and vacuum sublimation furnace for treatment of ores |
US4749409A (en) | 1987-08-31 | 1988-06-07 | Hiroshi Ishizuka | Method of purifying refractory metal |
JPH0772289B2 (ja) * | 1990-04-23 | 1995-08-02 | 川崎製鉄株式会社 | 溶銑予備処理ダストの再利用方法および装置 |
US5078789A (en) | 1990-10-31 | 1992-01-07 | Westinghouse Electric Corp. | Continuous vacuum distillation and furnace therefor |
US5100465A (en) * | 1990-12-24 | 1992-03-31 | Westinghouse Electric Corp. | Process for purifying zirconium sponge |
JP2619314B2 (ja) * | 1991-11-26 | 1997-06-11 | トヨタ自動車株式会社 | 付着金属の蒸発除去装置 |
JPH0570855A (ja) * | 1991-07-30 | 1993-03-23 | Ishikawajima Harima Heavy Ind Co Ltd | 脱亜鉛処理システム |
DE19823908A1 (de) * | 1998-05-28 | 1999-12-02 | Kempten Elektroschmelz Gmbh | Elliptischer keramischer Verdampfer |
FR2782932B1 (fr) | 1998-09-07 | 2000-11-24 | Serge Medvedieff | Appareil pour la purificaiton, en phase gazeuse de substances inorganiques simples et composees |
JP3987373B2 (ja) * | 2002-04-26 | 2007-10-10 | 東芝機械株式会社 | 金属溶解加熱装置 |
RU2273674C1 (ru) * | 2004-09-16 | 2006-04-10 | Открытое Акционерное Общество"Корпорация ВСМПО-АВИСМА" | Способ вакуумной сепарации губчатого титана и устройство для его осуществления |
RU2273675C1 (ru) * | 2004-09-22 | 2006-04-10 | Открытое Акционерное Общество "Корпорация ВСМПО -АВИСМА" | Способ вакуумной сепарации губчатого титана и устройство для его осуществления |
CN101454467B (zh) * | 2006-03-27 | 2014-01-08 | 联邦科学及工业研究组织 | 生产金属化合物的设备和方法 |
CN201088871Y (zh) * | 2007-06-21 | 2008-07-23 | 中国矿业大学 | 真空升华提纯炉 |
-
2011
- 2011-05-04 AU AU2011250655A patent/AU2011250655B2/en not_active Ceased
- 2011-05-04 KR KR1020127031206A patent/KR20130058707A/ko not_active Application Discontinuation
- 2011-05-04 EA EA201291080A patent/EA027761B1/ru not_active IP Right Cessation
- 2011-05-04 US US13/695,993 patent/US10035078B2/en active Active
- 2011-05-04 WO PCT/AU2011/000516 patent/WO2011137489A1/en active Application Filing
- 2011-05-04 CN CN201180030392.0A patent/CN102985148B/zh not_active Expired - Fee Related
- 2011-05-04 JP JP2013508330A patent/JP6108397B2/ja not_active Expired - Fee Related
- 2011-05-04 NZ NZ603297A patent/NZ603297A/xx not_active IP Right Cessation
- 2011-05-04 CA CA2798262A patent/CA2798262A1/en not_active Abandoned
- 2011-05-04 EP EP11777029.7A patent/EP2569068B1/en active Active
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2012
- 2012-11-30 ZA ZA2012/09070A patent/ZA201209070B/en unknown
Also Published As
Publication number | Publication date |
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EP2569068A1 (en) | 2013-03-20 |
AU2011250655A1 (en) | 2012-11-22 |
AU2011250655B2 (en) | 2015-07-09 |
EA027761B1 (ru) | 2017-08-31 |
ZA201209070B (en) | 2018-07-25 |
EA201291080A1 (ru) | 2013-05-30 |
CN102985148A (zh) | 2013-03-20 |
CN102985148B (zh) | 2016-01-20 |
EP2569068A4 (en) | 2017-04-12 |
US20130052076A1 (en) | 2013-02-28 |
NZ603297A (en) | 2013-07-26 |
JP2013529252A (ja) | 2013-07-18 |
WO2011137489A1 (en) | 2011-11-10 |
KR20130058707A (ko) | 2013-06-04 |
US10035078B2 (en) | 2018-07-31 |
CA2798262A1 (en) | 2011-11-10 |
EP2569068B1 (en) | 2020-11-18 |
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