JP5626217B2 - ニッケル微粉及びその製造方法 - Google Patents
ニッケル微粉及びその製造方法 Download PDFInfo
- Publication number
- JP5626217B2 JP5626217B2 JP2011533011A JP2011533011A JP5626217B2 JP 5626217 B2 JP5626217 B2 JP 5626217B2 JP 2011533011 A JP2011533011 A JP 2011533011A JP 2011533011 A JP2011533011 A JP 2011533011A JP 5626217 B2 JP5626217 B2 JP 5626217B2
- Authority
- JP
- Japan
- Prior art keywords
- nickel
- fine powder
- sulfur
- oxygen
- coating layer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims description 566
- 229910052759 nickel Inorganic materials 0.000 title claims description 263
- 239000000843 powder Substances 0.000 title claims description 156
- 238000004519 manufacturing process Methods 0.000 title claims description 30
- 229910052717 sulfur Inorganic materials 0.000 claims description 101
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 100
- 239000011593 sulfur Substances 0.000 claims description 100
- WWNBZGLDODTKEM-UHFFFAOYSA-N sulfanylidenenickel Chemical compound [Ni]=S WWNBZGLDODTKEM-UHFFFAOYSA-N 0.000 claims description 84
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 82
- 229910052760 oxygen Inorganic materials 0.000 claims description 82
- 239000001301 oxygen Substances 0.000 claims description 82
- 239000011247 coating layer Substances 0.000 claims description 63
- 239000002994 raw material Substances 0.000 claims description 57
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 claims description 51
- 239000010410 layer Substances 0.000 claims description 50
- 229910000480 nickel oxide Inorganic materials 0.000 claims description 28
- 239000002245 particle Substances 0.000 claims description 28
- LGQLOGILCSXPEA-UHFFFAOYSA-L nickel sulfate Chemical compound [Ni+2].[O-]S([O-])(=O)=O LGQLOGILCSXPEA-UHFFFAOYSA-L 0.000 claims description 23
- 229910000363 nickel(II) sulfate Inorganic materials 0.000 claims description 23
- 238000004458 analytical method Methods 0.000 claims description 21
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 18
- 239000011261 inert gas Substances 0.000 claims description 14
- 238000011084 recovery Methods 0.000 claims description 14
- 238000002360 preparation method Methods 0.000 claims description 13
- 230000001590 oxidative effect Effects 0.000 claims description 12
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 11
- 238000010298 pulverizing process Methods 0.000 claims description 11
- 238000001816 cooling Methods 0.000 claims description 10
- BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 claims description 8
- 238000009826 distribution Methods 0.000 claims description 6
- 230000000930 thermomechanical effect Effects 0.000 claims description 5
- 230000008016 vaporization Effects 0.000 claims description 4
- 230000006698 induction Effects 0.000 claims description 2
- 238000013329 compounding Methods 0.000 claims 1
- 239000001856 Ethyl cellulose Substances 0.000 description 40
- ZZSNKZQZMQGXPY-UHFFFAOYSA-N Ethyl cellulose Chemical compound CCOCC1OC(OC)C(OCC)C(OCC)C1OC1C(O)C(O)C(OC)C(CO)O1 ZZSNKZQZMQGXPY-UHFFFAOYSA-N 0.000 description 40
- 229920001249 ethyl cellulose Polymers 0.000 description 40
- 235000019325 ethyl cellulose Nutrition 0.000 description 40
- 239000011230 binding agent Substances 0.000 description 30
- 230000003647 oxidation Effects 0.000 description 29
- 238000007254 oxidation reaction Methods 0.000 description 29
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 28
- 238000000034 method Methods 0.000 description 25
- 238000010304 firing Methods 0.000 description 24
- 238000005979 thermal decomposition reaction Methods 0.000 description 24
- 239000007789 gas Substances 0.000 description 21
- 230000000694 effects Effects 0.000 description 20
- 238000011156 evaluation Methods 0.000 description 20
- 239000011347 resin Substances 0.000 description 20
- 229920005989 resin Polymers 0.000 description 20
- 238000000354 decomposition reaction Methods 0.000 description 17
- 230000003197 catalytic effect Effects 0.000 description 15
- 229910052786 argon Inorganic materials 0.000 description 14
- 238000005245 sintering Methods 0.000 description 14
- 239000001257 hydrogen Substances 0.000 description 13
- 229910052739 hydrogen Inorganic materials 0.000 description 13
- 230000000052 comparative effect Effects 0.000 description 12
- 238000005259 measurement Methods 0.000 description 10
- 230000008569 process Effects 0.000 description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 239000000919 ceramic Substances 0.000 description 8
- 239000007772 electrode material Substances 0.000 description 7
- 230000008859 change Effects 0.000 description 6
- 230000008602 contraction Effects 0.000 description 6
- 238000006722 reduction reaction Methods 0.000 description 6
- 238000000682 scanning probe acoustic microscopy Methods 0.000 description 6
- 239000000126 substance Substances 0.000 description 6
- 150000003464 sulfur compounds Chemical class 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 description 5
- 239000012159 carrier gas Substances 0.000 description 5
- 239000003985 ceramic capacitor Substances 0.000 description 5
- 239000013078 crystal Substances 0.000 description 5
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 description 5
- 230000009467 reduction Effects 0.000 description 5
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 4
- 238000004220 aggregation Methods 0.000 description 4
- 230000002776 aggregation Effects 0.000 description 4
- 125000004429 atom Chemical group 0.000 description 4
- 239000000460 chlorine Substances 0.000 description 4
- 229910052801 chlorine Inorganic materials 0.000 description 4
- 150000001875 compounds Chemical class 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 238000002003 electron diffraction Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000002345 surface coating layer Substances 0.000 description 4
- 239000012808 vapor phase Substances 0.000 description 4
- 238000005169 Debye-Scherrer Methods 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 3
- 239000003990 capacitor Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 230000020169 heat generation Effects 0.000 description 3
- 239000012798 spherical particle Substances 0.000 description 3
- 230000007847 structural defect Effects 0.000 description 3
- 239000002344 surface layer Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 238000011109 contamination Methods 0.000 description 2
- 238000005260 corrosion Methods 0.000 description 2
- 230000007797 corrosion Effects 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000032798 delamination Effects 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- XONPDZSGENTBNJ-UHFFFAOYSA-N molecular hydrogen;sodium Chemical compound [Na].[H][H] XONPDZSGENTBNJ-UHFFFAOYSA-N 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 238000000197 pyrolysis Methods 0.000 description 2
- 230000006798 recombination Effects 0.000 description 2
- 238000005215 recombination Methods 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L sulfate group Chemical group S(=O)(=O)([O-])[O-] QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 241000080590 Niso Species 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 description 1
- 239000012491 analyte Substances 0.000 description 1
- JRPBQTZRNDNNOP-UHFFFAOYSA-N barium titanate Chemical compound [Ba+2].[Ba+2].[O-][Ti]([O-])([O-])[O-] JRPBQTZRNDNNOP-UHFFFAOYSA-N 0.000 description 1
- 229910002113 barium titanate Inorganic materials 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000011362 coarse particle Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000003111 delayed effect Effects 0.000 description 1
- SQIFACVGCPWBQZ-UHFFFAOYSA-N delta-terpineol Natural products CC(C)(O)C1CCC(=C)CC1 SQIFACVGCPWBQZ-UHFFFAOYSA-N 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- -1 for example Chemical compound 0.000 description 1
- 230000008014 freezing Effects 0.000 description 1
- 238000007710 freezing Methods 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 150000002815 nickel Chemical group 0.000 description 1
- AIBQNUOBCRIENU-UHFFFAOYSA-N nickel;dihydrate Chemical compound O.O.[Ni] AIBQNUOBCRIENU-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 238000007650 screen-printing Methods 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 238000000992 sputter etching Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 125000004434 sulfur atom Chemical group 0.000 description 1
- 230000001629 suppression Effects 0.000 description 1
- 238000005211 surface analysis Methods 0.000 description 1
- 238000010301 surface-oxidation reaction Methods 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 229940116411 terpineol Drugs 0.000 description 1
- WLTSUBTXQJEURO-UHFFFAOYSA-N thorium tungsten Chemical compound [W].[Th] WLTSUBTXQJEURO-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C19/00—Alloys based on nickel or cobalt
- C22C19/03—Alloys based on nickel or cobalt based on nickel
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/16—Metallic particles coated with a non-metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F9/00—Making metallic powder or suspensions thereof
- B22F9/02—Making metallic powder or suspensions thereof using physical processes
- B22F9/12—Making metallic powder or suspensions thereof using physical processes starting from gaseous material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2301/00—Metallic composition of the powder or its coating
- B22F2301/15—Nickel or cobalt
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Powder Metallurgy (AREA)
- Manufacture Of Metal Powder And Suspensions Thereof (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2011533011A JP5626217B2 (ja) | 2009-09-24 | 2010-09-22 | ニッケル微粉及びその製造方法 |
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2009219286 | 2009-09-24 | ||
| JP2009219286 | 2009-09-24 | ||
| JP2011533011A JP5626217B2 (ja) | 2009-09-24 | 2010-09-22 | ニッケル微粉及びその製造方法 |
| PCT/JP2010/066448 WO2011037150A1 (ja) | 2009-09-24 | 2010-09-22 | ニッケル微粉及びその製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPWO2011037150A1 JPWO2011037150A1 (ja) | 2013-02-21 |
| JP5626217B2 true JP5626217B2 (ja) | 2014-11-19 |
Family
ID=43795896
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011533011A Active JP5626217B2 (ja) | 2009-09-24 | 2010-09-22 | ニッケル微粉及びその製造方法 |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JP5626217B2 (zh) |
| KR (1) | KR101745030B1 (zh) |
| CN (1) | CN102665969B (zh) |
| TW (1) | TWI517914B (zh) |
| WO (1) | WO2011037150A1 (zh) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2013231230A (ja) * | 2012-04-04 | 2013-11-14 | Nippon Steel & Sumikin Chemical Co Ltd | 複合ニッケル粒子 |
| JP5962562B2 (ja) * | 2013-03-22 | 2016-08-03 | 住友金属鉱山株式会社 | ニッケル粉末とその製造方法 |
| JP2014189884A (ja) * | 2013-03-28 | 2014-10-06 | Sumitomo Metal Mining Co Ltd | ニッケル粉末の製造方法 |
| JP6083295B2 (ja) * | 2013-03-29 | 2017-02-22 | 住友金属鉱山株式会社 | ニッケル粉末の製造方法 |
| KR102248526B1 (ko) * | 2013-07-23 | 2021-05-06 | 삼성전기주식회사 | 내부 전극용 니켈 분말, 이를 포함하는 적층 세라믹 커패시터 및 전자부품이 실장된 회로기판 |
| JP6213301B2 (ja) * | 2014-02-26 | 2017-10-18 | 住友金属鉱山株式会社 | ニッケル粉末の製造方法 |
| JP2015197303A (ja) * | 2014-03-31 | 2015-11-09 | 住友金属鉱山株式会社 | 金属粉末表面の評価方法及びニッケル粉末 |
| JP2015197302A (ja) * | 2014-03-31 | 2015-11-09 | 住友金属鉱山株式会社 | 金属粉末表面の評価方法及び金属粉末製造条件の決定方法 |
| CN106457379B (zh) * | 2014-04-08 | 2020-12-08 | 东邦钛株式会社 | 镍粉 |
| JP2017025400A (ja) * | 2015-07-28 | 2017-02-02 | 住友金属鉱山株式会社 | 積層セラミックコンデンサ用ニッケル粉末および導電ペースト |
| WO2017122689A1 (ja) * | 2016-01-12 | 2017-07-20 | 東邦チタニウム株式会社 | ニッケル粉末 |
| JP6573563B2 (ja) * | 2016-03-18 | 2019-09-11 | 住友金属鉱山株式会社 | ニッケル粉末、ニッケル粉末の製造方法、およびニッケル粉末を用いた内部電極ペーストならびに電子部品 |
| JP6649840B2 (ja) * | 2016-04-18 | 2020-02-19 | 株式会社ノリタケカンパニーリミテド | 導体形成用ペースト |
| KR102484793B1 (ko) * | 2018-06-28 | 2023-01-05 | 도호 티타늄 가부시키가이샤 | 금속 분말과 그 제조 방법, 및 소결 온도의 예측 방법 |
| CN112872349A (zh) * | 2021-01-12 | 2021-06-01 | 杭州新川新材料有限公司 | 一种核壳结构的纳米镍粉 |
| CN113948235B (zh) * | 2021-12-20 | 2022-03-29 | 西安宏星电子浆料科技股份有限公司 | 一种高分散性、低收缩率的镍内电极浆料及其制备方法 |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05156325A (ja) * | 1991-12-09 | 1993-06-22 | Mitsubishi Gas Chem Co Inc | 微細金属粉の製造法 |
| JP2000045001A (ja) * | 1998-07-27 | 2000-02-15 | Toho Titanium Co Ltd | 導電ペースト用ニッケル粉末 |
| JP2000096110A (ja) * | 1998-09-22 | 2000-04-04 | Sumitomo Metal Mining Co Ltd | 金属粉の製造方法 |
| JP2002146401A (ja) * | 2000-11-09 | 2002-05-22 | Mitsui Mining & Smelting Co Ltd | ニッケル粉及びその製造方法 |
| JP2002348603A (ja) * | 2001-05-24 | 2002-12-04 | Murata Mfg Co Ltd | 金属粉末の製造方法、金属粉末、導電性ペーストおよび積層セラミック電子部品 |
| JP2008223068A (ja) * | 2007-03-12 | 2008-09-25 | Shoei Chem Ind Co | ニッケル粉末、その製造方法、導体ペーストおよびそれを用いた積層セラミック電子部品 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5250101A (en) * | 1991-04-08 | 1993-10-05 | Mitsubishi Gas Chemical Company, Inc. | Process for the production of fine powder |
-
2010
- 2010-09-22 JP JP2011533011A patent/JP5626217B2/ja active Active
- 2010-09-22 CN CN201080052922.7A patent/CN102665969B/zh active Active
- 2010-09-22 KR KR1020127009139A patent/KR101745030B1/ko active IP Right Grant
- 2010-09-22 WO PCT/JP2010/066448 patent/WO2011037150A1/ja active Application Filing
- 2010-09-23 TW TW099132243A patent/TWI517914B/zh active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH05156325A (ja) * | 1991-12-09 | 1993-06-22 | Mitsubishi Gas Chem Co Inc | 微細金属粉の製造法 |
| JP2000045001A (ja) * | 1998-07-27 | 2000-02-15 | Toho Titanium Co Ltd | 導電ペースト用ニッケル粉末 |
| JP2000096110A (ja) * | 1998-09-22 | 2000-04-04 | Sumitomo Metal Mining Co Ltd | 金属粉の製造方法 |
| JP2002146401A (ja) * | 2000-11-09 | 2002-05-22 | Mitsui Mining & Smelting Co Ltd | ニッケル粉及びその製造方法 |
| JP2002348603A (ja) * | 2001-05-24 | 2002-12-04 | Murata Mfg Co Ltd | 金属粉末の製造方法、金属粉末、導電性ペーストおよび積層セラミック電子部品 |
| JP2008223068A (ja) * | 2007-03-12 | 2008-09-25 | Shoei Chem Ind Co | ニッケル粉末、その製造方法、導体ペーストおよびそれを用いた積層セラミック電子部品 |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2011037150A1 (ja) | 2011-03-31 |
| TW201129434A (en) | 2011-09-01 |
| KR20120084730A (ko) | 2012-07-30 |
| KR101745030B1 (ko) | 2017-06-08 |
| JPWO2011037150A1 (ja) | 2013-02-21 |
| TWI517914B (zh) | 2016-01-21 |
| CN102665969A (zh) | 2012-09-12 |
| CN102665969B (zh) | 2015-03-04 |
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