JP5204651B2 - 触媒および無水マレイン酸の製造法 - Google Patents

触媒および無水マレイン酸の製造法 Download PDF

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Publication number
JP5204651B2
JP5204651B2 JP2008523339A JP2008523339A JP5204651B2 JP 5204651 B2 JP5204651 B2 JP 5204651B2 JP 2008523339 A JP2008523339 A JP 2008523339A JP 2008523339 A JP2008523339 A JP 2008523339A JP 5204651 B2 JP5204651 B2 JP 5204651B2
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Prior art keywords
iron
catalyst
vanadium
maleic anhydride
vpo
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Expired - Fee Related
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JP2008523339A
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Japanese (ja)
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JP2009502465A5 (enExample
JP2009502465A (ja
Inventor
ドブナー コーネリア
ドゥーダ マーク
ライヒレ アンドレアス
ヴィルマー ハーゲン
ロゾフスキー フランク
ヘルツレ マルクス
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BASF SE
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BASF SE
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/847—Vanadium, niobium or tantalum or polonium
    • B01J23/8472—Vanadium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/195—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with vanadium, niobium or tantalum
    • B01J27/198—Vanadium
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • B01J37/031—Precipitation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/16—Reducing

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Furan Compounds (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
JP2008523339A 2005-07-28 2006-07-21 触媒および無水マレイン酸の製造法 Expired - Fee Related JP5204651B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102005035978A DE102005035978A1 (de) 2005-07-28 2005-07-28 Katalysator und Verfahren zur Herstellung von Maleinsäureanhydrid
DE102005035978.7 2005-07-28
PCT/EP2006/064551 WO2007012620A1 (de) 2005-07-28 2006-07-21 Katalysator und verfahren zur herstellung von maleinsäureanhydrid

Publications (3)

Publication Number Publication Date
JP2009502465A JP2009502465A (ja) 2009-01-29
JP2009502465A5 JP2009502465A5 (enExample) 2012-05-17
JP5204651B2 true JP5204651B2 (ja) 2013-06-05

Family

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Application Number Title Priority Date Filing Date
JP2008523339A Expired - Fee Related JP5204651B2 (ja) 2005-07-28 2006-07-21 触媒および無水マレイン酸の製造法

Country Status (7)

Country Link
US (1) US20080227992A1 (enExample)
EP (1) EP1915210A1 (enExample)
JP (1) JP5204651B2 (enExample)
CN (1) CN101227974B (enExample)
DE (1) DE102005035978A1 (enExample)
TW (1) TW200718468A (enExample)
WO (1) WO2007012620A1 (enExample)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW200719968A (en) 2005-10-31 2007-06-01 Sued Chemie Ag Catalyst molding for partial oxidation reactions
DE102007003076A1 (de) * 2007-01-16 2008-07-17 Basf Se Verfahren zur Herstellung einer das Element Eisen in oxidischer Form enthaltenden Multielementoxidmasse
DE102007004961A1 (de) 2007-01-26 2008-07-31 Basf Se Verfahren zur Herstellung von Katalysatorformkörpern, deren Aktivmasse ein Multielementoxid ist
EP2114562B1 (de) 2007-01-19 2017-11-01 Basf Se Verfahren zur herstellung von katalysatorformkörpern, deren aktivmasse ein multielementoxid ist
DE102007012725A1 (de) * 2007-03-16 2008-09-18 Basf Se Polynäres Metalloxidphosphat
DE102007012723A1 (de) * 2007-03-16 2008-09-18 Basf Se Polynäres Vanadylpyrophosphat
DE102007012722A1 (de) * 2007-03-16 2008-09-18 Basf Se Polynäres Metall-Vanadiumoxidphosphat
DE102007012724A1 (de) * 2007-03-16 2008-09-18 Basf Se Polynäres Metalloxidphosphat
DE102007017080A1 (de) 2007-04-10 2008-10-16 Basf Se Verfahren zur Beschickung eines Längsabschnitts eines Kontaktrohres
DE102007025869A1 (de) 2007-06-01 2008-07-03 Basf Se Verfahren der Wiederbeschickung der Reaktionsrohre eines Rohrbündelreaktors mit einem neuen Katalysatorfestbett
DE102007028332A1 (de) 2007-06-15 2008-12-18 Basf Se Verfahren zum Beschicken eines Reaktors mit einem Katalysatorfestbett, das wenigstens ringförmige Katalysatorformkörper K umfasst
DE102008040094A1 (de) 2008-07-02 2009-01-29 Basf Se Verfahren zur Herstellung eines oxidischen geometrischen Formkörpers
DE102008040093A1 (de) 2008-07-02 2008-12-18 Basf Se Verfahren zur Herstellung eines ringähnlichen oxidischen Formkörpers
DE102008054586A1 (de) 2008-12-12 2010-06-17 Basf Se Verfahren zur kontinuierlichen Herstellung von geometrischen Katalysatorformkörpern K
DE102010040921A1 (de) 2010-09-16 2012-03-22 Basf Se Verfahren zur Herstellung von Acrylsäure aus Methanol und Essigsäure
DE102010040923A1 (de) 2010-09-16 2012-03-22 Basf Se Verfahren zur Herstellung von Acrylsäure aus Ethanol und Formaldehyd
DE112013001034T5 (de) * 2012-02-20 2015-02-05 Basf Se Gasphasenoxidationskatalysator mit einer niedrigen Aktivierungsenergie für den Ladungstransport
DE102012012510B4 (de) 2012-06-22 2018-12-06 Clariant International Ltd. Graphithaltiger Katalysatorformkörper, dessen Herstellverfahren sowie Verwendung
DE102013008206A1 (de) 2013-05-14 2014-11-20 Basf Se Verfahren zur Herstellung von Vinylidencarbonsäure(ester)n durch Umsetzung von Formaldehyd mit Alkylcarbonsäure(estern)n
DE102013008207A1 (de) 2013-05-14 2014-11-20 Basf Se Verfahren zur Herstellung von Acrylsäure mit hoher Raum-Zeit-Ausbeute
US9073846B2 (en) 2013-06-05 2015-07-07 Celanese International Corporation Integrated process for the production of acrylic acids and acrylates
US9120743B2 (en) 2013-06-27 2015-09-01 Celanese International Corporation Integrated process for the production of acrylic acids and acrylates
US11289700B2 (en) 2016-06-28 2022-03-29 The Research Foundation For The State University Of New York KVOPO4 cathode for sodium ion batteries
CN106311258A (zh) * 2016-09-23 2017-01-11 上海应用技术大学 一种钒酸铁光催化剂的制备方法
CN111097465B (zh) * 2018-10-25 2022-10-11 中国石油化工股份有限公司 钒磷氧化物催化剂的制备方法
CN111097467B (zh) * 2018-10-25 2022-10-11 中国石油化工股份有限公司 低碳烃选择氧化的钒磷催化剂前驱体的活化方法
JP2022154004A (ja) * 2021-03-30 2022-10-13 三菱ケミカル株式会社 無水マレイン酸製造用触媒及び無水マレイン酸の製造方法

Family Cites Families (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1146844B (de) * 1960-12-14 1963-04-11 Thyssensche Gas Und Wasserwerk Verfahren zum Verkoken von gasreichen backenden Kohlen zur Erzeugung von Erzkoks
US3856824A (en) * 1971-12-27 1974-12-24 Monsanto Co Modified p-v-fe catalyst for production of maleic anhydride from saturated aliphatic hydrocarbons
US3888886A (en) * 1972-06-08 1975-06-10 Mobil Oil Corp Oxidation of alkanes to maleic anhydride using promoted vanadium-phosphorus catalyst
CA1049540A (en) * 1972-06-08 1979-02-27 Mobil Oil Corporation Oxidation of alkanes to dicarboxylic acid anhydrides using promoted vanadium-phosphorus catalyst
US4064070A (en) * 1974-12-23 1977-12-20 Chevron Research Company Catalyst for producing maleic anhydride
US4244878A (en) * 1978-08-04 1981-01-13 Halcon Research And Development Corporation Preparation of maleic anhydride
US4251390A (en) * 1979-06-11 1981-02-17 Denka Chemical Corporation Partial oxidation catalyst
US4337173A (en) * 1980-09-22 1982-06-29 Mitsubishi Chemical Industries, Ltd. Solid-solution type crystalline oxides and their precursors
DE3130343A1 (de) * 1981-07-31 1983-02-17 Bayer Ag, 5090 Leverkusen Vanadium/phosphor-mischoxid-katalysator, verfahren zu dessen herstellung sowie dessen verwendung
US4442226A (en) * 1982-02-16 1984-04-10 E. I. Du Pont De Nemours And Company Catalyst for vapor phase oxidation of n-butane to maleic anhydride
IN164007B (enExample) * 1984-09-04 1988-12-24 Halcon Sd Group Inc
US4699985A (en) * 1985-07-15 1987-10-13 E. I. Du Pont De Nemours And Company Process for oxidation of N-butane to maleic anhydride
ES2000042B3 (es) * 1985-10-28 1990-05-01 Monsanto Co Hierro/litio-catalizadores activos para la produccion de anhidrido maleico y descripcion del proceso de preparacion de anh. maleico
US4632915A (en) * 1985-10-28 1986-12-30 Monsanto Company Iron/lithium--promoted catalysts for the production of maleic anhydride
US5158923A (en) * 1990-05-21 1992-10-27 Scientific Design Company, Inc. Phosphorous/vanadium oxidation catalyst
US5137860A (en) * 1991-06-27 1992-08-11 Monsanto Company Process for the transformation of vanadium/phosphorus mixed oxide catalyst precursors into active catalysts for the production of maleic anhydride
US5185455A (en) * 1992-02-18 1993-02-09 Monsanto Company Method for improving the performance of VPO catalysts
JPH06145160A (ja) * 1992-11-06 1994-05-24 Maruzen Petrochem Co Ltd 無水マレイン酸の製造方法
JPH05262754A (ja) * 1992-03-17 1993-10-12 Maruzen Petrochem Co Ltd 無水マレイン酸の製造方法
US5364824A (en) * 1992-12-08 1994-11-15 Huntsman Specialty Chemicals Corporation Catalysis for the production of maleic anhydride containing vanadium-phosphorus oxide with selected promoter elements
US5506187A (en) * 1992-12-18 1996-04-09 Amoco Corporation Catalysts for the production of maleic anhydride by the oxidation of butane
US5296436A (en) * 1993-01-08 1994-03-22 Scientific Design Company, Inc. Phosphorous/vanadium oxidation catalyst
US5348927A (en) * 1993-03-01 1994-09-20 Scientific Design Company, Inc. Treatment for virgin phosphorous/vanadium oxidation catalysts
JP3555205B2 (ja) * 1993-12-22 2004-08-18 三菱化学株式会社 リン−バナジウム酸化物触媒前駆体の製造方法
US5543532A (en) * 1994-03-31 1996-08-06 E. I. Du Pont De Nemours And Company Catalyst and method for vapor phase oxidation of alkane hydrocarbons
US5641722A (en) * 1994-09-15 1997-06-24 Huntsman Petrochemical Corporation High performance VPO catalyst and process of preparation thereof
US5922637A (en) * 1997-03-28 1999-07-13 Scientific Design Company, Inc. Phosphorus/vanadium catalyst preparation
WO2001052983A1 (en) * 2000-01-20 2001-07-26 E.I. Dupont De Nemours And Company Vanadium-phosphorus oxide catalysts with promoter reagents
DE10011307A1 (de) * 2000-03-10 2001-09-13 Basf Ag Katalysator und Verfahren zur Herstellung von Maleinsäureanhydrid
DE10015365C2 (de) * 2000-03-23 2002-09-19 Inst Angewandte Chemie Berlin Mischkatalysator aus Oxovanadiumdiphosphat und weiteren Komponenten
DE10211447A1 (de) * 2002-03-15 2003-10-02 Basf Ag Katalysator und Verfahren zur Herstellung von Maleinsäureanhydrid
DE10211449A1 (de) * 2002-03-15 2003-09-25 Basf Ag Katalysator-Precursor für die Herstellung von Maleinsäureanhydrid und Verfahren zu dessen Herstellung
DE10235355A1 (de) * 2002-08-02 2004-02-19 Basf Ag Verfahren zur Herstellung von Maleinsäureanhydrid

Also Published As

Publication number Publication date
TW200718468A (en) 2007-05-16
US20080227992A1 (en) 2008-09-18
EP1915210A1 (de) 2008-04-30
CN101227974B (zh) 2014-12-10
JP2009502465A (ja) 2009-01-29
CN101227974A (zh) 2008-07-23
DE102005035978A1 (de) 2007-02-01
WO2007012620A1 (de) 2007-02-01

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