JP5021116B2 - アクリル酸およびアクリル酸エステルの製造方法 - Google Patents

アクリル酸およびアクリル酸エステルの製造方法 Download PDF

Info

Publication number
JP5021116B2
JP5021116B2 JP2000541132A JP2000541132A JP5021116B2 JP 5021116 B2 JP5021116 B2 JP 5021116B2 JP 2000541132 A JP2000541132 A JP 2000541132A JP 2000541132 A JP2000541132 A JP 2000541132A JP 5021116 B2 JP5021116 B2 JP 5021116B2
Authority
JP
Japan
Prior art keywords
acrylic acid
mixture
mass
esters
separation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP2000541132A
Other languages
English (en)
Japanese (ja)
Other versions
JP2002509905A (ja
JP2002509905A5 (https=
Inventor
ボルツ ゲアハルト
ネストラー ゲアハルト
シュレーダー ユルゲン
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2002509905A publication Critical patent/JP2002509905A/ja
Publication of JP2002509905A5 publication Critical patent/JP2002509905A5/ja
Application granted granted Critical
Publication of JP5021116B2 publication Critical patent/JP5021116B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2000541132A 1998-03-31 1999-03-25 アクリル酸およびアクリル酸エステルの製造方法 Expired - Lifetime JP5021116B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19814421.0 1998-03-31
DE19814421A DE19814421A1 (de) 1998-03-31 1998-03-31 Verfahren zur Herstellung von Acrylsäure und Acrylsäureestern
PCT/EP1999/002036 WO1999050222A1 (de) 1998-03-31 1999-03-25 Verfahren zur herstellung von acrylsäure und acrylsäureestern

Publications (3)

Publication Number Publication Date
JP2002509905A JP2002509905A (ja) 2002-04-02
JP2002509905A5 JP2002509905A5 (https=) 2006-01-19
JP5021116B2 true JP5021116B2 (ja) 2012-09-05

Family

ID=7863128

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2000541132A Expired - Lifetime JP5021116B2 (ja) 1998-03-31 1999-03-25 アクリル酸およびアクリル酸エステルの製造方法

Country Status (7)

Country Link
EP (1) EP1068174B1 (https=)
JP (1) JP5021116B2 (https=)
CN (1) CN1137079C (https=)
BR (1) BR9909312B1 (https=)
DE (2) DE19814421A1 (https=)
MY (1) MY120567A (https=)
WO (1) WO1999050222A1 (https=)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19851983A1 (de) 1998-11-11 2000-05-18 Basf Ag Verfahren zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure
JP4673483B2 (ja) 1999-03-06 2011-04-20 ビーエーエスエフ ソシエタス・ヨーロピア アクリル酸の製造法
MY122671A (en) 1999-03-06 2006-04-29 Basf Ag Fractional condensation of a product gas mixture containing acrylic acid
JP3885486B2 (ja) * 2000-11-16 2007-02-21 東亞合成株式会社 ビニル単量体用重合防止剤組成物及び高純度（メタ）アクリル酸の製造方法
DE10063161A1 (de) * 2000-12-18 2002-06-20 Basf Ag Verfahren zum Abschrecken eines heißen (Meth)acrylsäure enthaltenden Gasgemisches
US7592483B2 (en) 2004-07-01 2009-09-22 Basf Aktiengesellschaft Preparation of acrolein or acrylic acid or a mixture thereof by heterogeneously catalyzed partial gas phase oxidation of propylene
JP4732366B2 (ja) 2004-08-02 2011-07-27 エルジー・ケム・リミテッド （メタ）アクリル酸の製造法
US7705181B2 (en) 2005-03-01 2010-04-27 Basf Akiengesellschaft Process for removing methacrylic acid from liquid phase comprising acrylic acid as a main constituent and target product, and methacrylic acid as a secondary component
JP2007191435A (ja) * 2006-01-19 2007-08-02 Nippon Shokubai Co Ltd （メタ）アクリル酸の製造方法
KR101477491B1 (ko) 2006-09-15 2014-12-31 알케마 인코포레이티드 아크릴산의 제조방법
DE102008041573A1 (de) 2008-08-26 2010-03-04 Basf Se Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enhaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal
CN102112429B (zh) 2008-07-28 2015-09-16 巴斯夫欧洲公司 从丙烯酸c3前体化合物的气态产物混合物中分离作为主成份含有的丙烯酸和作为副产物含有的乙二醛的方法
DE102008040799A1 (de) 2008-07-28 2008-12-11 Basf Se Verfahren zur Auftrennung von in einem Produktgasgemisch einer partiellen heterogen katalysierten Gasphasenoxidation einer C3-Vorläuferverbindung der Acrylsäure als Hauptbestandteil enthaltener Acrylsäure und als Nebenprodukt enthaltenem Glyoxal
JP5169899B2 (ja) * 2009-02-19 2013-03-27 東亞合成株式会社 アクリル酸アルキルエステルの製造方法
DE102010042216A1 (de) 2010-10-08 2011-06-09 Basf Se Verfahren zur Hemmung der unerwünschten radikalischen Polymerisation von in einer flüssigen Phase P befindlicher Acrylsäure
JP6856381B2 (ja) * 2014-06-23 2021-04-07 ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ モノマー溶液の液滴を反応器中に添加するための装置
JP6497454B2 (ja) * 2018-01-12 2019-04-10 三菱ケミカル株式会社 アクリル酸ブチルの製造方法
KR102893876B1 (ko) 2018-07-26 2025-12-03 바스프 에스이 액상 p 중 존재하는 아크릴산의 원치않는 라디칼 중합의 억제 방법
CN115335354A (zh) 2020-03-26 2022-11-11 巴斯夫欧洲公司 抑制存在于液相p中的丙烯酸的不期望的自由基聚合的方法
WO2026032892A1 (de) 2024-08-05 2026-02-12 Basf Se Verfahren zur herstellung von (meth)acrylsäurealkylester ausgehend von (meth)acrylsäure
WO2026032891A1 (de) 2024-08-05 2026-02-12 Basf Se Verfahren zur abtrennung von (meth)acrylsäure

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3405172A (en) * 1962-12-19 1968-10-08 Distillers Co Yeast Ltd Preparation of acrylic acid with the prevention of formation of acrylic polymers
JPS57144237A (en) * 1981-03-04 1982-09-06 Japan Synthetic Rubber Co Ltd Preparation of methacrylic acid
US4554054A (en) * 1983-12-09 1985-11-19 Rohm And Haas Company Methacrylic acid separation
CA1316545C (en) * 1987-06-27 1993-04-20 Morimasa Kuragano Quenching process of reaction product gas containing methacrylic acid and treatment method of quenched liquid

Also Published As

Publication number Publication date
EP1068174A1 (de) 2001-01-17
JP2002509905A (ja) 2002-04-02
EP1068174B1 (de) 2003-05-28
BR9909312B1 (pt) 2011-05-31
BR9909312A (pt) 2000-11-21
WO1999050222A1 (de) 1999-10-07
DE59905752D1 (de) 2003-07-03
CN1137079C (zh) 2004-02-04
MY120567A (en) 2005-11-30
CN1296470A (zh) 2001-05-23
DE19814421A1 (de) 1999-10-07

Similar Documents

Publication Publication Date Title
JP5021116B2 (ja) アクリル酸およびアクリル酸エステルの製造方法
JP4410935B2 (ja) アクリル酸およびアクリル酸エステルを製造する方法
JP4410934B2 (ja) アクリル酸及びアクリル酸エステルの製造法
KR102263549B1 (ko) 개선된 (메트)아크릴산 제조 방법
CN1318378C (zh) (甲基)丙烯酸酯的制备方法
JP4555473B2 (ja) （メタ）アクリル酸および（メタ）アクリル酸エステルの製造方法
JP2010503692A (ja) アクリル酸の生成方法
KR19990013692A (ko) 메틸 메타크릴레이트의 제조 방법
SG178084A1 (en) Method for producing bioresourced acrylic acid from glycerol
JP3681285B2 (ja) メタクリル酸メチルの製造方法
CN1902154B (zh) 通过氧化气体底物得到的(甲基)丙烯酸的纯化方法
KR20020026389A (ko) 프로필렌 및/또는 아크롤레인의 산화로 수득한 아크릴산의정제 방법
CN100473636C (zh) 通过氧化气体基质得到(甲基)丙烯酸的纯化方法
CN105980343B (zh) 用于制备生物来源的丙烯酸的方法
JPS6212776B2 (https=)
US20240034709A1 (en) Novel process for continuous preparation of methacrylic acid by catalytic hydrolysis of methyl methacrylate
JP4651175B2 (ja) メタクリル酸の精製方法およびメタクリル酸メチルの製造方法
JP2003176253A (ja) （メタ）アクリル酸類の蒸留方法
JP2023520711A (ja) （メタ）アクリル酸を精製するための方法

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20051116

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20051116

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20081128

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20090226

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20090805

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20091207

A911 Transfer to examiner for re-examination before appeal (zenchi)

Free format text: JAPANESE INTERMEDIATE CODE: A911

Effective date: 20091215

A912 Re-examination (zenchi) completed and case transferred to appeal board

Free format text: JAPANESE INTERMEDIATE CODE: A912

Effective date: 20100205

RD04 Notification of resignation of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7424

Effective date: 20101227

RD04 Notification of resignation of power of attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7424

Effective date: 20101228

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20111117

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20111128

RD13 Notification of appointment of power of sub attorney

Free format text: JAPANESE INTERMEDIATE CODE: A7433

Effective date: 20120314

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A821

Effective date: 20120314

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20120417

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20120614

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20150622

Year of fee payment: 3

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term