MY120567A - Method for producing acrylic acid and acrylic acid esters. - Google Patents
Method for producing acrylic acid and acrylic acid esters.Info
- Publication number
- MY120567A MY120567A MYPI99001164A MYPI9901164A MY120567A MY 120567 A MY120567 A MY 120567A MY PI99001164 A MYPI99001164 A MY PI99001164A MY PI9901164 A MYPI9901164 A MY PI9901164A MY 120567 A MY120567 A MY 120567A
- Authority
- MY
- Malaysia
- Prior art keywords
- acrylic acid
- give
- mixture
- esters
- acrylates
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
Abstract
A PROCESS FOR PREPARING ACRYLIC ACID AND/OR AN ACRYLATE COMPRISING THE FOLLOWING STAGE A AND, IF DESIRED, B AND, IF DESIRED, C: A: COOLING A GASEOUS REACTION MIXTURE WHICH COMPRISES ACRYLIC ACID AND IS OBTAINED IN THE GAS-PHASE OXIDATION TO PREPARE ACRYLIC ACID, USING AN ACRYLIC ACID CONTAINING NOT MORE THAN 5% BY WEIGHT OF WATER, TO GIVE A GASEOUS MIXTURE COMPRISING (METH)ACRYLIC ACID; B: SEPARATING THE GASEOUS MIXTURE COMPRISING ACRYLIC ACID TO GIVE A LOW-BOILING FRACTION AND A BOTTOM PRODUCT WHICH COMPRISES CRUDE ACRYLIC ACID, AND C: ESTERIFYING THE CRUDE ACRYLIC ACID OBTAINED IN STAGE B BY MEANS OF ONE OR MORE ALKANOLS, TO GIVE AN ESTERIFICATION MIXTURE COMPRISING ONE OR MORE ACRYLATES, ONE OR MORE ACETIC ESTERS, ONE OR MORE MALEIC ESTERS, AND OLIGOMERIC AND POLYMERIC ACRYLATES.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19814421A DE19814421A1 (en) | 1998-03-31 | 1998-03-31 | Process for the production of acrylic acid and acrylic acid esters |
Publications (1)
Publication Number | Publication Date |
---|---|
MY120567A true MY120567A (en) | 2005-11-30 |
Family
ID=7863128
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MYPI99001164A MY120567A (en) | 1998-03-31 | 1999-03-26 | Method for producing acrylic acid and acrylic acid esters. |
Country Status (7)
Country | Link |
---|---|
EP (1) | EP1068174B1 (en) |
JP (1) | JP5021116B2 (en) |
CN (1) | CN1137079C (en) |
BR (1) | BR9909312B1 (en) |
DE (2) | DE19814421A1 (en) |
MY (1) | MY120567A (en) |
WO (1) | WO1999050222A1 (en) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19851983A1 (en) | 1998-11-11 | 2000-05-18 | Basf Ag | Process for the continuous production of alkyl esters of (meth) acrylic acid |
ES2206197T3 (en) | 1999-03-06 | 2004-05-16 | Basf Aktiengesellschaft | PROCEDURE FOR OBTAINING ACRYLIC ACID. |
MY122671A (en) | 1999-03-06 | 2006-04-29 | Basf Ag | Fractional condensation of a product gas mixture containing acrylic acid |
JP3885486B2 (en) * | 2000-11-16 | 2007-02-21 | 東亞合成株式会社 | Polymerization inhibitor composition for vinyl monomer and method for producing high purity (meth) acrylic acid |
DE10063161A1 (en) * | 2000-12-18 | 2002-06-20 | Basf Ag | Process for quenching a hot gas mixture containing (meth) acrylic acid |
US8431743B2 (en) | 2004-07-01 | 2013-04-30 | Basf Aktiengesellschaft | Preparation of acrylic acid by heterogeneously catalyzed partial gas phase oxidation of propylene |
TWI306451B (en) * | 2004-08-02 | 2009-02-21 | Lg Chemical Ltd | Method for producing (meth) acrylic acid |
US7705181B2 (en) | 2005-03-01 | 2010-04-27 | Basf Akiengesellschaft | Process for removing methacrylic acid from liquid phase comprising acrylic acid as a main constituent and target product, and methacrylic acid as a secondary component |
JP2007191435A (en) * | 2006-01-19 | 2007-08-02 | Nippon Shokubai Co Ltd | Method for producing (meth)acrylic acid |
WO2008033687A2 (en) | 2006-09-15 | 2008-03-20 | Dow Global Technologies Inc. | Process for producing acrylic acid |
MY153094A (en) | 2008-07-28 | 2014-12-31 | Basf Se | Process for separating acrylic acid present as a main constituent and glyoxal present as a by-product in a product gas mixture of a partial heterogeneously catalyzed gas phase oxidation of a c3 precursor compound of acrylic acid |
DE102008040799A1 (en) | 2008-07-28 | 2008-12-11 | Basf Se | Separating a three carbon precursor compound of acrylic acid as main component containing acrylic acid and as byproduct containing glyoxal, in a product mixture of a heterogeneously catalyzed partial gas phase oxidation |
DE102008041573A1 (en) | 2008-08-26 | 2010-03-04 | Basf Se | Separating acrylic acid and glyoxal from gaseous product mixture of gas phase oxidation of a three carbon-precursor compound of acrylic acid comprises producing a liquid phase containing acrylic acid and glyoxal, and separating glyoxal |
JP5169899B2 (en) * | 2009-02-19 | 2013-03-27 | 東亞合成株式会社 | Method for producing alkyl acrylate ester |
DE102010042216A1 (en) | 2010-10-08 | 2011-06-09 | Basf Se | Inhibiting the unwanted radical polymerization of acrylic acid present in a liquid phase, comprises adding a chemical compound of copper to the liquid phase, and the liquid phase additionally contains propionic acid and glyoxal |
JP6856381B2 (en) * | 2014-06-23 | 2021-04-07 | ビーエイエスエフ・ソシエタス・エウロパエアBasf Se | A device for adding droplets of monomeric solution into a reactor |
JP6497454B2 (en) * | 2018-01-12 | 2019-04-10 | 三菱ケミカル株式会社 | Method for producing butyl acrylate |
WO2020020697A1 (en) | 2018-07-26 | 2020-01-30 | Basf Se | Method for inhibiting unwanted radical polymerisation of acrylic acid present in a liquid phase p |
US20230132285A1 (en) | 2020-03-26 | 2023-04-27 | Basf Se | Process for inhibiting the undesired free-radical polymerization of acrylic acid present in a liquid phase p |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3405172A (en) * | 1962-12-19 | 1968-10-08 | Distillers Co Yeast Ltd | Preparation of acrylic acid with the prevention of formation of acrylic polymers |
JPS57144237A (en) * | 1981-03-04 | 1982-09-06 | Japan Synthetic Rubber Co Ltd | Preparation of methacrylic acid |
US4554054A (en) * | 1983-12-09 | 1985-11-19 | Rohm And Haas Company | Methacrylic acid separation |
CA1316545C (en) * | 1987-06-27 | 1993-04-20 | Morimasa Kuragano | Quenching process of reaction product gas containing methacrylic acid and treatment method of quenched liquid |
-
1998
- 1998-03-31 DE DE19814421A patent/DE19814421A1/en not_active Withdrawn
-
1999
- 1999-03-25 CN CNB998047813A patent/CN1137079C/en not_active Expired - Lifetime
- 1999-03-25 WO PCT/EP1999/002036 patent/WO1999050222A1/en active IP Right Grant
- 1999-03-25 EP EP99919140A patent/EP1068174B1/en not_active Expired - Lifetime
- 1999-03-25 JP JP2000541132A patent/JP5021116B2/en not_active Expired - Lifetime
- 1999-03-25 DE DE59905752T patent/DE59905752D1/en not_active Expired - Lifetime
- 1999-03-25 BR BRPI9909312-0A patent/BR9909312B1/en not_active IP Right Cessation
- 1999-03-26 MY MYPI99001164A patent/MY120567A/en unknown
Also Published As
Publication number | Publication date |
---|---|
CN1137079C (en) | 2004-02-04 |
WO1999050222A1 (en) | 1999-10-07 |
EP1068174B1 (en) | 2003-05-28 |
DE19814421A1 (en) | 1999-10-07 |
BR9909312A (en) | 2000-11-21 |
CN1296470A (en) | 2001-05-23 |
JP5021116B2 (en) | 2012-09-05 |
DE59905752D1 (en) | 2003-07-03 |
JP2002509905A (en) | 2002-04-02 |
BR9909312B1 (en) | 2011-05-31 |
EP1068174A1 (en) | 2001-01-17 |
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