JP4856070B2 - 鏡像関係にある純粋な1,1’−スピロビインダン−6,6’−ジオール誘導体の製造方法 - Google Patents
鏡像関係にある純粋な1,1’−スピロビインダン−6,6’−ジオール誘導体の製造方法 Download PDFInfo
- Publication number
- JP4856070B2 JP4856070B2 JP2007522543A JP2007522543A JP4856070B2 JP 4856070 B2 JP4856070 B2 JP 4856070B2 JP 2007522543 A JP2007522543 A JP 2007522543A JP 2007522543 A JP2007522543 A JP 2007522543A JP 4856070 B2 JP4856070 B2 JP 4856070B2
- Authority
- JP
- Japan
- Prior art keywords
- spirobiindane
- racemic
- mixture
- diol
- chiral
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
- C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
- C07C37/86—Purification; separation; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
- C07C41/01—Preparation of ethers
- C07C41/34—Separation; Purification; Stabilisation; Use of additives
- C07C41/44—Separation; Purification; Stabilisation; Use of additives by treatments giving rise to a chemical modification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
- C07B2200/00—Indexing scheme relating to specific properties of organic compounds
- C07B2200/07—Optical isomers
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2603/00—Systems containing at least three condensed rings
- C07C2603/93—Spiro compounds
- C07C2603/94—Spiro compounds containing "free" spiro atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10/895,160 US7214834B2 (en) | 2004-07-20 | 2004-07-20 | Process for preparing enantiomerically pure 1,1′-spirobiindane-6,6′-diol derivatives |
| US10/895,160 | 2004-07-20 | ||
| PCT/US2005/024452 WO2006019663A1 (en) | 2004-07-20 | 2005-07-07 | Process for preparing enantiomerically pure 1,1'-spirobiindane-6,6'-diol derivatives |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2008507516A JP2008507516A (ja) | 2008-03-13 |
| JP2008507516A5 JP2008507516A5 (OSRAM) | 2008-09-04 |
| JP4856070B2 true JP4856070B2 (ja) | 2012-01-18 |
Family
ID=35336314
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2007522543A Expired - Fee Related JP4856070B2 (ja) | 2004-07-20 | 2005-07-07 | 鏡像関係にある純粋な1,1’−スピロビインダン−6,6’−ジオール誘導体の製造方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US7214834B2 (OSRAM) |
| EP (1) | EP1768943B1 (OSRAM) |
| JP (1) | JP4856070B2 (OSRAM) |
| CN (1) | CN1989093A (OSRAM) |
| DE (1) | DE602005011814D1 (OSRAM) |
| WO (1) | WO2006019663A1 (OSRAM) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7470376B2 (en) * | 2004-10-29 | 2008-12-30 | Industrial Technology Research Institute | Photochemically active chiral compounds and compositions containing the same |
| US7452482B2 (en) * | 2004-12-15 | 2008-11-18 | Industrial Technology Research Institute | Photochemically active chiral compounds and compositions containing the same |
| US7329368B2 (en) * | 2005-12-08 | 2008-02-12 | Industrial Technology Research Institute | Temperature compensating chiral dopants |
| TWI449772B (zh) | 2011-11-25 | 2014-08-21 | Ind Tech Res Inst | 液晶化合物及包括該化合物之液晶顯示器及光變色指示材料 |
| JP6167868B2 (ja) * | 2012-11-16 | 2017-07-26 | 三菱ケミカル株式会社 | スピロビインダン類の製造方法 |
| JP6309083B2 (ja) * | 2013-05-14 | 2018-04-11 | スリーエム イノベイティブ プロパティズ カンパニー | 堅固でかつ制御されたジビニル架橋剤によるアミノ含有ポリマー材料 |
| CN108250008B (zh) * | 2018-02-05 | 2020-07-28 | 浙江大学 | 3,3,3’,3’-四甲基-1,1’-螺二氢茚-6,6’-二醇衍生物手性拆分方法 |
| CN109020788B (zh) * | 2018-07-04 | 2020-09-04 | 浙江大学 | 光学纯的1,1’-螺二氢茚-6,6’-二醇衍生物的制备方法 |
| CN116375562B (zh) * | 2023-03-31 | 2024-05-31 | 福州大学 | 一种莰烯水合制异龙脑的精制方法 |
| CN117362729B (zh) * | 2023-10-24 | 2024-03-29 | 新航涂布科技(苏州)有限公司 | 一种板材耐候抗形变炫彩膜及其制备方法 |
| WO2025160090A1 (en) * | 2024-01-22 | 2025-07-31 | Wave Life Sciences Ltd. | Technol. ogies useful for oligonucleotide preparation |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6190155A (ja) * | 1984-10-09 | 1986-05-08 | Konishiroku Photo Ind Co Ltd | ハロゲン化銀カラ−写真感光材料 |
| JPS63146837A (ja) * | 1986-10-10 | 1988-06-18 | ゼネラル・エレクトリック・カンパニイ | 実質的に純粋なスピロビインダンビスフェノール類の製造方法 |
| JPH04273835A (ja) * | 1991-02-28 | 1992-09-30 | Tokyo Kasei Kogyo Kk | 光学活性アルコールの製造法 |
| JPH06298690A (ja) * | 1993-04-19 | 1994-10-25 | Mitsui Toatsu Chem Inc | 6,6’−ジヒドロキシ−3,3,3’,3’−テトラメチル−1,1’−スピロビインダンの製造方法 |
| JP2004189696A (ja) * | 2002-12-13 | 2004-07-08 | Mitsubishi Chemicals Corp | 光学活性6,6’−ジメチル−1,1’−ビフェニル−2,2’−ジオール誘導体の製造方法 |
| JP2005281215A (ja) * | 2004-03-30 | 2005-10-13 | Sumitomo Chemical Co Ltd | 光学活性スピロ化合物からなる光学分割試薬 |
| JP2007518849A (ja) * | 2003-12-16 | 2007-07-12 | イーストマン コダック カンパニー | キラル化合物を含む液晶組成物 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2645020A1 (de) | 1976-10-06 | 1978-04-13 | Bayer Ag | Verfahren zur herstellung von dihydroxyspirobisindanen |
| AU594348B2 (en) | 1985-06-28 | 1990-03-08 | Mitsui Toatsu Chemicals Inc. | Process for producing 6,6'-dihydroxy-3,3,3',3'-tetramethyl- 1,1'-spirobiidane |
| US4701566A (en) | 1986-10-10 | 1987-10-20 | General Electric Company | Method for preparing spirobiindane bisphenols |
| DE4027385A1 (de) | 1989-09-05 | 1991-03-07 | Basf Ag | Hitzehaertbare bismaleinimid-formmassen |
| WO1997020877A2 (de) | 1995-12-01 | 1997-06-12 | Ciba Specialty Chemicals Holding Inc. | Poly(9,9'-spirobisfluorene), deren herstellung und deren verwendung |
| US5856422A (en) | 1997-10-24 | 1999-01-05 | Molecular Optoelectronics Corporation | Optically active poly(aryl)ethers containing optically pure spirobindane and indane moieties |
| US6288206B1 (en) | 1999-03-08 | 2001-09-11 | Molecular Optoelectronics Corporation | Chiral polymer compositions exhibiting nonlinear optical properties |
-
2004
- 2004-07-20 US US10/895,160 patent/US7214834B2/en not_active Expired - Fee Related
-
2005
- 2005-07-07 JP JP2007522543A patent/JP4856070B2/ja not_active Expired - Fee Related
- 2005-07-07 EP EP05769287A patent/EP1768943B1/en not_active Expired - Lifetime
- 2005-07-07 DE DE602005011814T patent/DE602005011814D1/de not_active Expired - Lifetime
- 2005-07-07 CN CNA2005800242724A patent/CN1989093A/zh active Pending
- 2005-07-07 WO PCT/US2005/024452 patent/WO2006019663A1/en not_active Ceased
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6190155A (ja) * | 1984-10-09 | 1986-05-08 | Konishiroku Photo Ind Co Ltd | ハロゲン化銀カラ−写真感光材料 |
| JPS63146837A (ja) * | 1986-10-10 | 1988-06-18 | ゼネラル・エレクトリック・カンパニイ | 実質的に純粋なスピロビインダンビスフェノール類の製造方法 |
| JPH04273835A (ja) * | 1991-02-28 | 1992-09-30 | Tokyo Kasei Kogyo Kk | 光学活性アルコールの製造法 |
| JPH06298690A (ja) * | 1993-04-19 | 1994-10-25 | Mitsui Toatsu Chem Inc | 6,6’−ジヒドロキシ−3,3,3’,3’−テトラメチル−1,1’−スピロビインダンの製造方法 |
| JP2004189696A (ja) * | 2002-12-13 | 2004-07-08 | Mitsubishi Chemicals Corp | 光学活性6,6’−ジメチル−1,1’−ビフェニル−2,2’−ジオール誘導体の製造方法 |
| JP2007518849A (ja) * | 2003-12-16 | 2007-07-12 | イーストマン コダック カンパニー | キラル化合物を含む液晶組成物 |
| JP2005281215A (ja) * | 2004-03-30 | 2005-10-13 | Sumitomo Chemical Co Ltd | 光学活性スピロ化合物からなる光学分割試薬 |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2006019663A1 (en) | 2006-02-23 |
| CN1989093A (zh) | 2007-06-27 |
| JP2008507516A (ja) | 2008-03-13 |
| DE602005011814D1 (de) | 2009-01-29 |
| EP1768943B1 (en) | 2008-12-17 |
| EP1768943A1 (en) | 2007-04-04 |
| US20060020150A1 (en) | 2006-01-26 |
| US7214834B2 (en) | 2007-05-08 |
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