JP4744080B2 - ポリシロキサン及びそれらの調製 - Google Patents

ポリシロキサン及びそれらの調製 Download PDF

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Publication number
JP4744080B2
JP4744080B2 JP2003521702A JP2003521702A JP4744080B2 JP 4744080 B2 JP4744080 B2 JP 4744080B2 JP 2003521702 A JP2003521702 A JP 2003521702A JP 2003521702 A JP2003521702 A JP 2003521702A JP 4744080 B2 JP4744080 B2 JP 4744080B2
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JP
Japan
Prior art keywords
group
silanol
groups
carboxylic acid
aminosilane
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP2003521702A
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English (en)
Japanese (ja)
Other versions
JP2005523342A (ja
JP2005523342A5 (OSRAM
Inventor
ウェストール、スティーヴン
サージェナー、エイヴリル
ハップフィールド、ピーター・チェシャー
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Silicones Corp
Original Assignee
Dow Corning Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=9920561&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JP4744080(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Dow Corning Corp filed Critical Dow Corning Corp
Publication of JP2005523342A publication Critical patent/JP2005523342A/ja
Publication of JP2005523342A5 publication Critical patent/JP2005523342A5/ja
Application granted granted Critical
Publication of JP4744080B2 publication Critical patent/JP4744080B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C08G77/08—Preparatory processes characterised by the catalysts used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/38—Polysiloxanes modified by chemical after-treatment
    • C08G77/382—Polysiloxanes modified by chemical after-treatment containing atoms other than carbon, hydrogen, oxygen or silicon
    • C08G77/388—Polysiloxanes modified by chemical after-treatment containing atoms other than carbon, hydrogen, oxygen or silicon containing nitrogen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
    • C08L83/04—Polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/14—Polysiloxanes containing silicon bound to oxygen-containing groups
    • C08G77/16—Polysiloxanes containing silicon bound to oxygen-containing groups to hydroxyl groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Silicon Polymers (AREA)
  • Cosmetics (AREA)
JP2003521702A 2001-08-17 2002-08-12 ポリシロキサン及びそれらの調製 Expired - Lifetime JP4744080B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB0120058.3 2001-08-17
GBGB0120058.3A GB0120058D0 (en) 2001-08-17 2001-08-17 Polysiloxanes and their preparation
PCT/EP2002/009821 WO2003016380A2 (en) 2001-08-17 2002-08-12 Polysiloxanes and their preparation

Publications (3)

Publication Number Publication Date
JP2005523342A JP2005523342A (ja) 2005-08-04
JP2005523342A5 JP2005523342A5 (OSRAM) 2006-01-05
JP4744080B2 true JP4744080B2 (ja) 2011-08-10

Family

ID=9920561

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2003521702A Expired - Lifetime JP4744080B2 (ja) 2001-08-17 2002-08-12 ポリシロキサン及びそれらの調製

Country Status (9)

Country Link
US (2) US20040210074A1 (OSRAM)
EP (1) EP1432753B2 (OSRAM)
JP (1) JP4744080B2 (OSRAM)
CN (1) CN100415804C (OSRAM)
AT (1) ATE473253T1 (OSRAM)
AU (1) AU2002333788A1 (OSRAM)
DE (1) DE60236946D1 (OSRAM)
GB (1) GB0120058D0 (OSRAM)
WO (1) WO2003016380A2 (OSRAM)

Families Citing this family (57)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0327067D0 (en) * 2003-11-21 2003-12-24 Dow Corning Polymeric products useful as oil repellents
DE102004014218A1 (de) * 2004-03-23 2005-10-13 Wacker-Chemie Gmbh Verfahren zur Herstellung von aminofunktionellen Organopolysiloxanen
GB0407433D0 (en) 2004-04-01 2004-05-05 Dow Corning Substituted aminosiloxanes and polymeric products
US7097785B2 (en) * 2004-04-12 2006-08-29 Dow Corning Corporation Fluoropolymer—amino terminated polydiorganosiloxane compositions for textile treatments
GB0415001D0 (en) 2004-07-03 2004-08-04 Dow Corning Process of stabilising siloxane polymers
DE102005022099A1 (de) * 2005-05-12 2006-11-16 Wacker Chemie Ag Verfahren zur Herstellung von Dispersionen von vernetzten Organopolysiloxanen
US7687121B2 (en) * 2006-01-20 2010-03-30 Momentive Performance Materials Inc. Insulated glass unit with sealant composition having reduced permeability to gas
US7531613B2 (en) * 2006-01-20 2009-05-12 Momentive Performance Materials Inc. Inorganic-organic nanocomposite
EP2061828B1 (en) * 2006-10-10 2018-11-21 Dow Silicones Corporation Silicone polymer emulsions
US9694214B2 (en) * 2008-04-16 2017-07-04 Dow Corning Corporation Preparation of silicone microemulsions
DE102008001867A1 (de) * 2008-05-19 2009-11-26 Wacker Chemie Ag Verfahren zur Herstellung von quartäre Ammoniumgruppen aufweisenden Organopolysiloxanen
US8734767B2 (en) 2008-10-22 2014-05-27 Dow Corning Corporation Aminofunctional endblocked silicone polyether copolymers in personal care compositions
WO2010104186A2 (en) 2009-03-10 2010-09-16 Dow Corning Toray Co., Ltd. Oil-in-water silicone emulsion composition
GB0905507D0 (en) 2009-03-31 2009-05-13 Dow Corning Organopol Ysiloxane Compositions Containing An Active Material
GB0905502D0 (en) 2009-03-31 2009-05-13 Dow Corning Organopolysiloxane emulsions and their production
DE102010002178A1 (de) 2010-02-22 2011-08-25 Evonik Goldschmidt GmbH, 45127 Verfahren zur Herstellung von Amin-Amid-funktionellen Siloxanen
EP2556103B1 (en) * 2010-04-06 2018-10-03 Dow Silicones Corporation Reactive amine-functional silicone-polyether block copolymers
JP5826826B2 (ja) * 2010-04-23 2015-12-02 ヘンケル アイピー アンド ホールディング ゲゼルシャフト ミット ベシュレンクテル ハフツング シリコーン−アクリルコポリマー
DE102010028182A1 (de) * 2010-04-26 2011-10-27 Momentive Performance Materials Gmbh Hydrophile Polyorganosiloxane
WO2012002571A1 (ja) 2010-07-02 2012-01-05 東レ・ダウコーニング株式会社 水中油型シリコーンエマルジョン組成物
DE102010062156A1 (de) 2010-10-25 2012-04-26 Evonik Goldschmidt Gmbh Polysiloxane mit stickstoffhaltigen Gruppen
DE102010062676A1 (de) 2010-12-09 2012-06-14 Evonik Goldschmidt Gmbh Zubereitungen enthaltend Polysiloxane mit stickstoffhaltigen Gruppen
EP2468759A1 (de) * 2010-12-17 2012-06-27 Sika Technology AG Sekundäre Aminosilane
CN102898883B (zh) * 2011-07-29 2016-08-24 道康宁(中国)投资有限公司 涂料组合物、使用其涂覆材料表面的方法、以及具有其的表面处理的材料
DE102011110100A1 (de) 2011-08-12 2013-02-14 Evonik Goldschmidt Gmbh Verfahren zu Herstellungen von Polysiloxanen mit stickstoffhaltigen Gruppen
EP2785908A1 (en) 2011-11-29 2014-10-08 Dow Corning Corporation Aminofunctional silicone emulsions for fiber treatments
WO2013082112A1 (en) 2011-11-29 2013-06-06 Dow Corning Corporation Aminofunctional silicone emulsions
DE102012201167A1 (de) 2012-01-27 2013-08-01 Evonik Industries Ag Mischungszusammensetzung enthaltend aminofunktionelle Siloxane, hydrophobePartikel und hochmolekulare Silicone sowie dessen Verwendung zur Lederbehandlung
CN102613904B (zh) * 2012-03-30 2014-07-30 广东新宝电器股份有限公司 咖啡机的防滴漏结构
DE102012207062A1 (de) 2012-04-27 2013-10-31 Wacker Chemie Ag Verfahren zur Herstellung von Aminogruppen aufweisenden Organosiliciumverbindungen
DE102014200106B4 (de) 2013-02-13 2018-04-26 Evonik Degussa Gmbh Härtbare organomodifizierte Siloxane hergestellt durch Kondensation
US9717676B2 (en) * 2013-07-26 2017-08-01 The Procter & Gamble Company Amino silicone nanoemulsion
US9175139B2 (en) * 2014-03-18 2015-11-03 Wacker Chemical Corporation Alkoxy group-containing silicones with reactive functional groups of defined reactivity
KR20170133490A (ko) 2015-04-08 2017-12-05 다우 코닝 코포레이션 유체 조성물 및 개인 케어
DE102015207673A1 (de) 2015-04-27 2016-10-27 Wacker Chemie Ag Verfahren zur Herstellung von Aminogruppen aufweisenden Organosiliciumverbindungen
US12275862B2 (en) * 2017-01-17 2025-04-15 Akzo Nobel Coatings International B.V. Foul release coating composition
WO2019231557A1 (en) 2018-05-31 2019-12-05 Dow Silicones Corporation Method for making an amino-functional polydiorganosiloxane using a removable acid catalysit
US11028233B2 (en) 2018-05-31 2021-06-08 Dow Silicones Corporation Method for making an amino-functional polydiorganosiloxane using a removable solid catalyst
CN112469769B (zh) 2018-08-24 2022-07-08 美国陶氏有机硅公司 用于羟基封端的聚二有机硅氧烷的缩合聚合的方法
MY208159A (en) 2018-08-24 2025-04-19 Dow Global Technologies Llc Method for condensation polymerization of hydroxyl-terminated polydiorganosiloxanes
US20220169803A1 (en) 2019-05-09 2022-06-02 Dow Silicones Corporation Method for mechanically preparing an emulsion of an amino-functional polyorganosiloxane
EP4028452A1 (en) * 2019-09-09 2022-07-20 Dow Silicones Corporation Method of preparing alkoxy-functional organosiloxane compounds
EP4028405A1 (en) 2019-09-09 2022-07-20 Dow Silicones Corporation Method of preparing alkoxy-functional organosilicon compounds
WO2021055272A1 (en) 2019-09-16 2021-03-25 Chevron Phillips Chemical Company Lp Chromium-catalyzed production of diols from olefins
WO2021065737A1 (ja) * 2019-09-30 2021-04-08 株式会社朝日Ｆｒ研究所 摺動性部材、及びその製造方法
CN114630857A (zh) 2019-11-26 2022-06-14 美国陶氏有机硅公司 用于制备聚环氧硅氮烷和使用聚环氧硅氮烷生成氨基官能化聚有机硅氧烷的方法
US20230287624A1 (en) * 2020-09-09 2023-09-14 Wacker Chemie Ag Use of low-cyclen derivatized amino-functional silicone polymers for treating fibrous substrates
US20240124653A1 (en) 2021-05-18 2024-04-18 Dow Silicones Corporation Processes for making polysiloxazanes and using same for producing amino-functional polyorganosiloxanes
CN117545795A (zh) 2021-06-28 2024-02-09 美国陶氏有机硅公司 氨基硅氧烷酯共聚物以及所述共聚物的制备方法和用途
EP4366841A1 (en) 2021-07-07 2024-05-15 Dow Silicones Corporation Foam stabilizing composition including a siloxane cationic surfactant and colloidal silica
EP4399249B1 (en) 2021-09-07 2025-11-19 Dow Silicones Corporation Amino-functional polyorganosiloxane additive for aqueous coating compositions
CN114409904A (zh) * 2022-01-19 2022-04-29 杭州一川新材料有限公司 一种缩合型透明硅橡胶的制备方法与应用
CN118922500A (zh) 2022-03-29 2024-11-08 美国陶氏有机硅公司 氨基官能聚有机硅氧烷乳液的制备
WO2025144523A1 (en) * 2023-12-26 2025-07-03 Dow Global Technologies Llc The use of aminosiloxane ester copolymers for the treatment of textiles
WO2025184162A1 (en) 2024-03-01 2025-09-04 Dow Global Technologies Llc Hydroxyl – functional aminosiloxane ester copolymer and methods for its preparation
WO2025254797A1 (en) 2024-06-04 2025-12-11 Dow Global Technologies Llc Aldehyde – diamine curable polyorganosiloxane composition and methods for the preparation and use thereof
WO2025254798A1 (en) 2024-06-04 2025-12-11 Dow Global Technologies Llc Aldehyde – amine curable polyorganosiloxane composition and methods for the preparation and use thereof

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS6022018B2 (ja) * 1981-11-27 1985-05-30 信越化学工業株式会社 シリコ−ン水性エマルジヨン組成物
US4508887A (en) * 1983-08-01 1985-04-02 Dow Corning Corporation Method and novel catalyst compositions for preparing polyorganosiloxanes
US4525567A (en) * 1984-01-04 1985-06-25 General Electric Company Ionically cross-linked siloxane polymers
US4523002A (en) * 1984-01-04 1985-06-11 General Electric Company Ionically cross-linked siloxane polymers
US4496705A (en) * 1984-01-04 1985-01-29 General Electric Company Synthesis of zwitterionic siloxane polymers
US4496795A (en) † 1984-05-16 1985-01-29 Harvey Hubbell Incorporated Electrical cable splicing system
US4633002A (en) * 1984-08-21 1986-12-30 Charles Piskoti Aminofunctional polysiloxane compounds and method of preparation therefor
US4699988A (en) * 1985-07-18 1987-10-13 General Electric Company Novel aminofunctional silicone compositions
US4785067A (en) * 1986-04-16 1988-11-15 Genesee Polymers Corporation Protective coating and method of making the same
US4950770A (en) * 1987-06-16 1990-08-21 Elder Pharmaceuticals, Inc. Psoralens aminomethylation
US4915938A (en) * 1987-11-13 1990-04-10 Zawadzki Mary E Hair treating composition
US4950506A (en) * 1989-01-05 1990-08-21 Dow Corning Corporation Water sheeting zwitterionomeric aminofunctional siloxanes
DE4026029A1 (de) † 1989-09-07 1992-02-20 Sandoz Ag Waessrige aminopolysiloxanmikroemulsionen, deren herstellung und verwendung
US5164522A (en) * 1990-06-29 1992-11-17 Karlshamns Ab Cationic silicones
US5115049A (en) * 1991-02-19 1992-05-19 Siltech Inc. Fatty carboxylic silicone amine salts
GB9218841D0 (en) 1992-09-05 1992-10-21 Dow Corning Process for producing organosiloxanes
GB9311509D0 (en) * 1993-06-03 1993-07-21 Dow Corning Process for the preparation of organopolysiloxanes
JP3350334B2 (ja) * 1996-01-12 2002-11-25 信越化学工業株式会社 新規なオルガノポリシロキサンおよびそれを主成分とする繊維処理剤組成物
GB9702234D0 (en) * 1997-02-04 1997-03-26 Dow Corning Process for stabilising siloxane polymers
DE19733168A1 (de) * 1997-07-31 1999-02-04 Wacker Chemie Gmbh Unter Abspaltung von Alkoholen zu Elastomeren vernetzbare Organopolysiloxanmassen
DE19739964A1 (de) † 1997-09-11 1999-03-18 Wacker Chemie Gmbh Einfach herstellbare Aminosiliconzusammensetzung
GB9826394D0 (en) * 1998-12-02 1999-01-27 Dow Corning Sa Method of making silicone-in-water emulsions
US6605123B1 (en) * 1999-04-16 2003-08-12 General Electric Company Silicone finishing compositions and processes
US6124490A (en) * 1999-10-26 2000-09-26 Mona Industries, Inc. Zwitterionic siloxane polymers and ionically cross-linked polymers formed therefrom
US6548465B2 (en) * 2000-03-10 2003-04-15 General Electric Company Siloxane dry cleaning composition and process

Also Published As

Publication number Publication date
CN1798792A (zh) 2006-07-05
CN100415804C (zh) 2008-09-03
AU2002333788A1 (en) 2003-03-03
EP1432753A2 (en) 2004-06-30
WO2003016380A2 (en) 2003-02-27
DE60236946D1 (de) 2010-08-19
JP2005523342A (ja) 2005-08-04
ATE473253T1 (de) 2010-07-15
EP1432753B1 (en) 2010-07-07
WO2003016380A3 (en) 2003-08-28
US20040210074A1 (en) 2004-10-21
GB0120058D0 (en) 2001-10-10
US20070073028A1 (en) 2007-03-29
EP1432753B2 (en) 2017-10-04
US7238768B2 (en) 2007-07-03

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