JP4743204B2 - 変性ポリウレタン樹脂及びこれを用いた接着剤組成物、並びに回路部材の接続方法及び回路部材の接続構造 - Google Patents
変性ポリウレタン樹脂及びこれを用いた接着剤組成物、並びに回路部材の接続方法及び回路部材の接続構造 Download PDFInfo
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Images
Classifications
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- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/67—Unsaturated compounds having active hydrogen
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
- C09J175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L24/00—Arrangements for connecting or disconnecting semiconductor or solid-state bodies; Methods or apparatus related thereto
- H01L24/01—Means for bonding being attached to, or being formed on, the surface to be connected, e.g. chip-to-package, die-attach, "first-level" interconnects; Manufacturing methods related thereto
- H01L24/26—Layer connectors, e.g. plate connectors, solder or adhesive layers; Manufacturing methods related thereto
- H01L24/28—Structure, shape, material or disposition of the layer connectors prior to the connecting process
- H01L24/29—Structure, shape, material or disposition of the layer connectors prior to the connecting process of an individual layer connector
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- H—ELECTRICITY
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- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
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- H01L24/80—Methods for connecting semiconductor or other solid state bodies using means for bonding being attached to, or being formed on, the surface to be connected
- H01L24/83—Methods for connecting semiconductor or other solid state bodies using means for bonding being attached to, or being formed on, the surface to be connected using a layer connector
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- H—ELECTRICITY
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Description
-CH2-CH2-CH2-CH2-O-、
-CH2-CH(CH3)-O-、
-CH2-CH2-O-、
-CH2-CH2-CH2-CH2-O-、
-(CH2-CH(CH3)-O)a-(CH2-CH2-O)b- (ただし、a/b=9〜1/1〜9mol%の共重合体)、
-CO-(CH2)4-CO-O-(CH2)2-O-、
-CO-(CH2)4-CO-O-(CH2)2-O-(CH2)2-O-、
-CO-(CH2)4-CO-O-CH2-CH(CH3)-O-、
-CO-(CH2)4-CO-O-(CH2)4-O-、
-CO-(CH2)4-CO-O-(CH2)6-O-、
-CO-(CH2)4-CO-O-CH2-C(CH3)2-CH2-O-、
-CO-(CH2)8-CO-O-(CH2)6-O-、
-CO-(CH2)5-O-、
-CO-O-(CH2)6-O-、及び
-R4-(Si(CH3)2-O)-R4- (ただし、R4は炭素数1〜10の有機基を示す。)
等の繰り返し単位を有するものが挙げられる。Yは、一般に、変性ポリウレタン樹脂の合成に用いられるジオールに由来するジオール残基である。式(I)中の複数のYは同一でも異なっていてもよい。言い換えると、変性ポリウレタン樹脂は1種類又は2種類以上を組み合わせたジオールを原料として用いて得られるものであってもよい。この場合、ジオールの平均分子量は100〜10000であることが好ましく、500〜5000であればより好ましい。
(A):下記一般式(VI)で表される化合物、下記一般式(VII)で表される化合物及び下記一般式(VIII)で表される化合物の混合物
オキシジフタル酸二無水物(1.0mol)、2−ヒドロキシエチルメタクリレート(0.2mol)、トリエチルアミン(0.01mol)及びヒドロキノン(0.01mol)をγ―ブチロラクトン中で窒素雰囲気下、80℃で5時間攪拌し、オキシジフタル酸二無水物の一部に2−ヒドロキシエチルメタクリレートが付加したオキシジフタル酸二無水物混合液を得た。
平均分子量2000のポリテトラメチレングリコール(0.8mol)を平均分子量2000のポリ(ヘキサメチレンカーボネート)(0.8mol)に代えた他はPU−1と同様にして、一般式(I)において−Z(R)r−の部分が下記化学式(IIa)、(IIIa)又は(IVa)で表される2価の基である分子鎖を含む変性ポリウレタン樹脂PU−2を得た。変性ポリウレタン樹脂PU−2のGPCを測定したところ、ポリスチレン換算でMw=25000、Mn=12000であった。
PU−1をメチルエチルケトンに固形分濃度40質量%で溶解し、硬化剤として1,1−ビス(t−ヘキシルパーオキシ)−3,3,5−トリメチルシクロヘキサン(パーヘキサTMH、日本油脂株式会社製商品名)を固形重量比でPU−1の量100重量部に対して2重量部加え、更に導電粒子を1.5体積%加えてこれを分散した。導電性子は、ポリスチレンを核とする粒子の表面に厚み0.2μmのニッケル層を設け、このニッケル層の外側に厚み0.02μmの金層を設けた平均粒径5μm、比重2.5のものを用いた。導電粒子を分散した溶液を厚み80μmのフッ素樹脂フィルムに塗工装置を用いて塗布し、70℃、10分の熱風乾燥によって接着剤層の厚みが20μmのフィルム状回路接続用異方導電接着剤(フィルム状接着剤)を得た。
PU−1に代えてPU−2を用いた他は実施例1と同様にしてフィルム状接着剤を作製し、これを用いて実施例1と同様に接続体を作製し、その接着強度を測定した。
80重量部のPU−1、硬化性樹脂としての20重量部のイソシアヌル酸EO変性ジアクリレート(東亞合成製、アロニックスM215)、及び硬化剤としての2重量部の1,1−ビス(t−ヘキシルパーオキシ)−3,3,5−トリメチルシクロヘキサン(パーヘキサTMH、日本油脂株式会社製商品名)を混合した。得られた混合物に実施例1と同様の導電粒子を1.5体積%加えてこれを分散して接着剤組成物を調製した。この接着剤を用いて実施例1と同様にフィルム状接着剤を作製した。そして、得られたフィルム状接着剤を用いて実施例1と同様にして接続体を作製し、その接着強度を測定した。
PU−1に代えてウレタンアクリレート(UA−511、新中村化学工業株式会社製)を用いた他は実施例1と同様にして、接続体の接着強度を測定した。
PU−1に代えてジフェニルメタン−4,4’−ジイソシアネート(0.5mol)、ジフェニルメタン−2,4’−ジイソシアネート(0.5mol)及び平均分子量2000のポリテトラメチレングリコール(1.0mol)から得られるポリウレタン(平均分子量Mw=57000、Mn=35000)を用いて実施例3と同様にして接続体の接着強度を測定した。
Claims (8)
- 下記一般式(I)で表される分子鎖を含む変性ポリウレタン樹脂。
- (a)、(b)及び(c)の合計量を基準として、(a)の割合が10〜90mol%、(b)の割合が0〜90mol%、(c)の割合が0〜90mol%である、請求項1記載の変性ポリウレタン樹脂。
- 請求項1又は2記載の変性ポリウレタン樹脂を含有する接着剤組成物。
- 硬化性樹脂を更に含有する、請求項3記載の接着剤組成物。
- 前記硬化性樹脂がラジカル重合により硬化する樹脂であり、
光照射又は加熱により遊離ラジカルを発生する硬化剤を含有している、請求項4記載の接着剤組成物。 - 導電粒子を更に含有する、請求項3〜5のいずれか一項に記載の接着剤組成物。
- 第一の基板及びこれの主面上に形成された第一の回路電極を有する第一の回路部材と、
第二の基板及びこれの主面上に形成された第二の回路電極を有する第二の回路部材とを請求項3〜6のいずれか一項に記載の接着剤組成物で接着することにより、前記第一の回路電極と前記第二の回路電極とを電気的に接続する、回路部材の接続方法。 - 第一の基板及びこれの主面上に形成された第一の回路電極を有する第一の回路部材と、第二の基板及びこれの主面上に形成された第二の回路電極を有する第二の回路部材と、を備え、
前記第一の回路電極と前記第二の回路電極とが電気的に接続されるように前記第一の回路部材と前記第二の回路部材とが請求項3〜6のいずれか一項に記載の接着剤組成物で接着されている、回路部材の接続構造。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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JP2007517724A JP4743204B2 (ja) | 2005-05-27 | 2006-01-27 | 変性ポリウレタン樹脂及びこれを用いた接着剤組成物、並びに回路部材の接続方法及び回路部材の接続構造 |
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JP2005155405 | 2005-05-27 | ||
JP2005155405 | 2005-05-27 | ||
JP2007517724A JP4743204B2 (ja) | 2005-05-27 | 2006-01-27 | 変性ポリウレタン樹脂及びこれを用いた接着剤組成物、並びに回路部材の接続方法及び回路部材の接続構造 |
PCT/JP2006/301356 WO2006126305A1 (ja) | 2005-05-27 | 2006-01-27 | 変性ポリウレタン樹脂及びこれを用いた接着剤組成物、並びに回路部材の接続方法及び回路部材の接続構造 |
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JPWO2006126305A1 JPWO2006126305A1 (ja) | 2008-12-25 |
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KR (1) | KR100934802B1 (ja) |
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JP2013206765A (ja) * | 2012-03-29 | 2013-10-07 | Tanaka Kikinzoku Kogyo Kk | ダイボンド用導電性ペースト及び該導電性ペーストによるダイボンド方法 |
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KR101293481B1 (ko) | 2013-07-08 | 2013-08-06 | 주식회사 비츠로테크 | 차단기와 단로기/접지개폐기 간의 인터록 연동장치 |
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JPS4947278B1 (ja) * | 1970-03-30 | 1974-12-14 | ||
JPH07113004A (ja) * | 1993-10-18 | 1995-05-02 | Regurusu:Kk | 熱可塑性ポリウレタンエラストマー及びその製造方法 |
JPH11199669A (ja) * | 1998-01-14 | 1999-07-27 | Ajinomoto Co Inc | 変成ポリイミド樹脂及びこれを含有する熱硬化性樹脂組成物 |
JP2000053744A (ja) * | 1998-08-07 | 2000-02-22 | Hitachi Chem Co Ltd | 樹脂組成物、接着剤、接着フィルム、これを用いたリードフレーム及び半導体装置 |
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GB1415155A (en) * | 1971-10-28 | 1975-11-26 | Johnson Matthey Co Ltd | Catalysis |
US4786657A (en) * | 1987-07-02 | 1988-11-22 | Minnesota Mining And Manufacturing Company | Polyurethanes and polyurethane/polyureas crosslinked using 2-glyceryl acrylate or 2-glyceryl methacrylate |
JPH01159824A (ja) * | 1987-12-16 | 1989-06-22 | Toyobo Co Ltd | 磁気記録媒体 |
US7320830B2 (en) * | 2001-09-05 | 2008-01-22 | Hitachi Chemical Co., Ltd. | Flame-retardant heat-resistant resin composition and adhesive film comprising the same |
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JPS4947278B1 (ja) * | 1970-03-30 | 1974-12-14 | ||
JPH07113004A (ja) * | 1993-10-18 | 1995-05-02 | Regurusu:Kk | 熱可塑性ポリウレタンエラストマー及びその製造方法 |
JPH11199669A (ja) * | 1998-01-14 | 1999-07-27 | Ajinomoto Co Inc | 変成ポリイミド樹脂及びこれを含有する熱硬化性樹脂組成物 |
JP2000053744A (ja) * | 1998-08-07 | 2000-02-22 | Hitachi Chem Co Ltd | 樹脂組成物、接着剤、接着フィルム、これを用いたリードフレーム及び半導体装置 |
Cited By (1)
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JP2013206765A (ja) * | 2012-03-29 | 2013-10-07 | Tanaka Kikinzoku Kogyo Kk | ダイボンド用導電性ペースト及び該導電性ペーストによるダイボンド方法 |
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TWI399405B (zh) | 2013-06-21 |
WO2006126305A1 (ja) | 2006-11-30 |
CN101180335A (zh) | 2008-05-14 |
KR100934802B1 (ko) | 2009-12-31 |
JPWO2006126305A1 (ja) | 2008-12-25 |
TW200641046A (en) | 2006-12-01 |
KR20080022121A (ko) | 2008-03-10 |
CN101180335B (zh) | 2010-12-15 |
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