JP4541702B2 - 変性されたａｔｒｐコポリマー分散剤を有する顔料組成物 - Google Patents

変性されたａｔｒｐコポリマー分散剤を有する顔料組成物 Download PDF

Info

Publication number
JP4541702B2
JP4541702B2 JP2003547476A JP2003547476A JP4541702B2 JP 4541702 B2 JP4541702 B2 JP 4541702B2 JP 2003547476 A JP2003547476 A JP 2003547476A JP 2003547476 A JP2003547476 A JP 2003547476A JP 4541702 B2 JP4541702 B2 JP 4541702B2
Authority
JP
Japan
Prior art keywords
group
copolymer
acid
alkyl
salt
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2003547476A
Other languages
English (en)
Japanese (ja)
Other versions
JP2005510595A5 (enExample
JP2005510595A (ja
Inventor
アウシュラ，クレメンス
エックシュタイン，エルンスト
ザンク，マリー−オディール
ミューレバッハ，アンドレアス
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF Schweiz AG
Original Assignee
Ciba Holding AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ciba Holding AG filed Critical Ciba Holding AG
Publication of JP2005510595A publication Critical patent/JP2005510595A/ja
Publication of JP2005510595A5 publication Critical patent/JP2005510595A5/ja
Application granted granted Critical
Publication of JP4541702B2 publication Critical patent/JP4541702B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B3/00—Dyes with an anthracene nucleus condensed with one or more carbocyclic rings
    • C09B3/02—Benzathrones
    • C09B3/06—Preparation from starting materials already containing the benzanthrone nucleus
    • C09B3/10—Amino derivatives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F293/00—Macromolecular compounds obtained by polymerisation on to a macromolecule having groups capable of inducing the formation of new polymer chains bound exclusively at one or both ends of the starting macromolecule
    • C08F293/005—Macromolecular compounds obtained by polymerisation on to a macromolecule having groups capable of inducing the formation of new polymer chains bound exclusively at one or both ends of the starting macromolecule using free radical "living" or "controlled" polymerisation, e.g. using a complexing agent
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F293/00—Macromolecular compounds obtained by polymerisation on to a macromolecule having groups capable of inducing the formation of new polymer chains bound exclusively at one or both ends of the starting macromolecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00—Use of organic ingredients
    • C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
    • C08K5/0041—Optical brightening agents, organic pigments
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L53/00—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D153/00—Coating compositions based on block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Coating compositions based on derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2438/00—Living radical polymerisation
    • C08F2438/01—Atom Transfer Radical Polymerization [ATRP] or reverse ATRP

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Polymers & Plastics (AREA)
  • Medicinal Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Paints Or Removers (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Graft Or Block Polymers (AREA)
  • Pigments, Carbon Blacks, Or Wood Stains (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
JP2003547476A 2001-11-29 2002-11-21 変性されたａｔｒｐコポリマー分散剤を有する顔料組成物 Expired - Fee Related JP4541702B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP01811158 2001-11-29
PCT/EP2002/013064 WO2003046029A1 (en) 2001-11-29 2002-11-21 Pigment compositions with modified atrp copolymer dispersants

Publications (3)

Publication Number Publication Date
JP2005510595A JP2005510595A (ja) 2005-04-21
JP2005510595A5 JP2005510595A5 (enExample) 2006-01-05
JP4541702B2 true JP4541702B2 (ja) 2010-09-08

Family

ID=8184277

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2003547476A Expired - Fee Related JP4541702B2 (ja) 2001-11-29 2002-11-21 変性されたａｔｒｐコポリマー分散剤を有する顔料組成物

Country Status (11)

Country Link
US (2) US20050004317A1 (enExample)
EP (1) EP1465935B1 (enExample)
JP (1) JP4541702B2 (enExample)
KR (1) KR100918576B1 (enExample)
CN (1) CN100408606C (enExample)
AU (1) AU2002352086A1 (enExample)
BR (1) BR0214616B1 (enExample)
CA (1) CA2465291A1 (enExample)
MX (1) MXPA04004693A (enExample)
TW (1) TW200407363A (enExample)
WO (1) WO2003046029A1 (enExample)

Families Citing this family (54)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1802409A (zh) * 2003-04-08 2006-07-12 西巴特殊化学品控股有限公司 颜料分散体中的光稳定聚合物分散剂
JP2006526678A (ja) * 2003-06-03 2006-11-24 チバ　スペシャルティ　ケミカルズ　ホールディング　インコーポレーテッド 放射線硬化性コーティングにおいて用いるための顔料濃厚物の製造方法
TW200604223A (en) * 2004-01-19 2006-02-01 Dainichiseika Color Chem Graft copolymers having excellent pigment-dispersing ability, production process of the graft copolymers, production method of emulsions by use of the graft copolymers, and pigment dispersions making use of the graft copolymers or emulsions
US7402624B2 (en) 2004-11-08 2008-07-22 E.I. Du Pont De Nemours & Company Graft copolymers with segmented arms and their preparation and use
JP2006167674A (ja) * 2004-12-20 2006-06-29 Toyo Ink Mfg Co Ltd 顔料分散剤
FR2885367B1 (fr) * 2005-05-03 2007-07-27 Rhodia Chimie Sa Organosol stabilise par des polymeres sequences amphiphiles
TW200730547A (en) * 2006-01-03 2007-08-16 Byk Chemie Gmbh Copolymers comprising three segments of different ion density, processes for preparing them and use thereof
CN101421360A (zh) * 2006-04-11 2009-04-29 西巴控股有限公司 制造金属氧化物薄片的方法
CN101426861B (zh) * 2006-04-21 2011-12-28 日本板硝子株式会社 光辉性颜料及其制造方法以及含有该光辉性颜料的水性树脂组合物
EP2038701B1 (en) 2006-07-06 2017-04-12 Basf Se Encapsulated dispersions comprising electrophoretically mobile organic colorants
EP2038704B9 (en) * 2006-07-11 2019-03-27 Basf Se Color filter composition
DE102006035726A1 (de) * 2006-07-28 2008-01-31 Evonik Röhm Gmbh Verfahren zur Herstellung von ABA-Triblockcopolymeren auf (Meth)acrylatbasis
JP5123189B2 (ja) * 2006-08-29 2013-01-16 日本板硝子株式会社 真珠光沢顔料
DE102006048144A1 (de) * 2006-10-10 2008-04-17 Byk-Chemie Gmbh Netz- und Dispergiermittel basierend auf Mischungen von strukturierten Copolymeren
DE102006062441A1 (de) 2006-12-27 2008-07-03 Byk-Chemie Gmbh Modifizierte Kammcopolymere
US8519026B2 (en) * 2006-12-28 2013-08-27 Nuplex Resins B.V. Waterborne polymeric dispersions
CN101675120B (zh) * 2007-04-18 2012-12-05 日本板硝子株式会社 光辉性颜料以及使用了该颜料的化妆用组合物
US20080264303A1 (en) 2007-04-24 2008-10-30 The Diller Corporation Solid surface product containing oriented reflective particles and method of making same
WO2008136471A1 (ja) * 2007-04-27 2008-11-13 Nippon Sheet Glass Company, Limited 光輝性顔料と、それを含有する光輝性塗料組成物および自動車外板コート物
ZA200804693B (en) * 2007-05-30 2009-02-25 Oreal Cosmetic hair compositions containing metal-oxide layered pigments and functionalized metal-oxide layered pigments and methods of use
JP5479343B2 (ja) 2007-09-07 2014-04-23 ビーエーエスエフ ソシエタス・ヨーロピア 電気泳動型移動性有機着色剤を含むカプセル化分散液
CN101827898B (zh) * 2007-10-18 2013-03-27 日本板硝子株式会社 发光性颜料
JP5104478B2 (ja) * 2008-03-31 2012-12-19 大日本印刷株式会社 ナノ微粒子複合体の製造方法
JP5374903B2 (ja) * 2008-03-31 2013-12-25 大日本印刷株式会社 カラーフィルタ用ネガ型レジスト組成物、カラーフィルタ及び液晶表示装置
US8664324B2 (en) 2008-06-23 2014-03-04 Basf Se Pigment dispersants with modified copolymers
US20090137172A1 (en) * 2008-12-04 2009-05-28 Lei Huang Colorant media and articles having photo-stable and surface-functionalizable colorant particles
WO2010089295A1 (de) * 2009-02-03 2010-08-12 Bühler PARTEC GmbH Mit phosphonocarbonsäure modifizierte zinkoxid-partikel und verwendung von zinkoxid-partikeln
EP2241602A1 (de) * 2009-04-17 2010-10-20 Bühler PARTEC GmbH Mit Phosphonocarbonsäure modifizierte Zinkoxid-Partikel und Verwendung von Zinkoxid-Partikeln
ES2423054T3 (es) 2009-03-25 2013-09-17 Byk-Chemie Gmbh Composición que comprende mezclas estables de polioles
JP5463712B2 (ja) * 2009-03-31 2014-04-09 大日本印刷株式会社 カラーフィルタ用顔料分散液及びその製造方法、カラーフィルタ用ネガ型レジスト組成物及びその製造方法、カラーフィルタ、並びに、液晶表示装置
US8753708B2 (en) * 2009-09-02 2014-06-17 Cardiac Pacemakers, Inc. Solventless method for forming a coating on a medical electrical lead body
EP2516495B1 (de) 2009-12-22 2015-07-29 BYK-Chemie GmbH Zusammensetzung umfassend stabile polyolmischungen
CN103080248B (zh) * 2010-09-27 2014-12-24 巴斯夫应用化工有限公司 水性白色色浆及其制备方法
DE102011014250A1 (de) * 2011-03-17 2012-09-20 Clariant International Ltd. Pulverlackzusammensetzung zum Strukturieren und Texturieren von Lackoberflächen
JP5779072B2 (ja) * 2011-10-20 2015-09-16 理想科学工業株式会社 非水系顔料インク及び非水系顔料インク用顔料分散剤
KR101127959B1 (ko) 2011-11-18 2012-04-04 (재)한국섬유소재연구소 분산제 및 그 제조방법
EP2817358B1 (en) 2012-02-24 2019-08-21 Basf Se Novel polymer dispersants
WO2013191707A1 (en) * 2012-06-22 2013-12-27 Hewlett-Packard Development Company, L.P. Inks including colorant particles with covalently attached dispersants
CN103205202A (zh) * 2013-04-03 2013-07-17 中山职业技术学院 一种表面张力梯度性变化的梯度功能涂料及其制备方法
JP2016523290A (ja) 2013-06-07 2016-08-08 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 新規のポリマー分散剤
JP2016525154A (ja) 2013-06-24 2016-08-22 ベーイプシロンカー ヘミー ゲゼルシャフト ミット ベシュレンクター ハフトゥング 接着強化添加剤およびそれを含むコーティング組成物
EP3024874B1 (en) 2013-07-22 2017-09-06 Basf Se Novel polymers and use of these as dispersants
EP3052701B1 (en) * 2013-10-04 2017-06-28 Basf Se High gloss metal effect papers
CN103924459A (zh) * 2014-04-30 2014-07-16 江南大学 用于纺织品涂料染色的双亲性核壳乳液粘合剂及其制备方法
TWI516520B (zh) 2014-10-31 2016-01-11 財團法人工業技術研究院 波長轉換聚合物、其製法及包含其之波長轉換裝置
WO2016071386A1 (en) 2014-11-05 2016-05-12 Basf Se Novel polymer compositions and use of these polymer compositions as dispersants
MX2019008010A (es) 2017-01-03 2019-08-29 Byk Chemie Gmbh Copolimeros (met)acrilicos como aditivos reologicos en fluidos de perforacion y fluidos de perforacion que comprenden dichos copolimeros.
WO2020035300A1 (en) 2018-08-16 2020-02-20 Basf Se Polymer composition
US12365762B2 (en) 2018-08-16 2025-07-22 Basf Se Dispersant for coating system
MX2021002384A (es) 2018-08-29 2021-04-29 Basf Coatings Gmbh Dispersante de pigmentos.
WO2021009351A1 (en) 2019-07-18 2021-01-21 Basf Se Allophanate based dispersing agent
CN111039270B (zh) * 2019-12-27 2021-10-08 天津科技大学 一种花状磷酸锌纳米颗粒抑菌材料及其制备方法与用途
CN114369212B (zh) * 2021-12-10 2024-06-28 复旦大学 颜料用高分子分散剂及其一锅多步合成方法和应用
EP4457261A1 (en) 2021-12-28 2024-11-06 BASF Coatings GmbH Dispersant

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4656226A (en) * 1985-09-30 1987-04-07 E. I. Du Pont De Nemours And Company Acrylic pigment dispersants made by group transfer polymerization
DE3875105T2 (de) * 1988-02-23 1993-03-18 Du Pont Blockmischpolymerisat-dispergiermittel.
US5763548A (en) * 1995-03-31 1998-06-09 Carnegie-Mellon University (Co)polymers and a novel polymerization process based on atom (or group) transfer radical polymerization
US5859113A (en) * 1997-07-17 1999-01-12 E. I. Du Pont De Nemours And Company Pigment dispersions containing hydroxylated AB-block polymer dispersant
US6265489B1 (en) * 1998-08-31 2001-07-24 Ppg Industries Ohio, Inc. Thermosetting compositions containing carboxylic acid functional polymers prepared by atom transfer radical polymerization
CN1333790A (zh) * 1998-12-31 2002-01-30 西巴特殊化学品控股有限公司 含atrp聚合物的颜料组合物
FR2791987A1 (fr) * 1999-04-06 2000-10-13 Oreal Composition notamment cosmetique comprenant des polymeres ayant une structure en etoiles, lesdits polymeres et leur utilisation
FR2791989A1 (fr) * 1999-04-06 2000-10-13 Oreal Composition notamment cosmetique comprenant des polymeres ayant une structure en etoiles, lesdits polymeres et leur utilisation
US6462125B1 (en) * 1999-12-16 2002-10-08 Ppg Industries Ohio, Inc. Pigment dispersions containing dispersants prepared by controlled radical polymerization having hydrophilic and hydrophobic segments
US6376597B1 (en) * 1999-12-16 2002-04-23 Ppg Industries Ohio, Inc. Pigment dispersions containing dispersants having pendent hydrophilic polymeric segments prepared by controlled radical polymerization
EP1254185A1 (en) * 2000-01-11 2002-11-06 Ciba SC Holding AG Comb polymers from atrp macromonomers
AU6744401A (en) * 2000-05-31 2001-12-11 Creavis Gesellschaft Fur Technologie Und Innovation Mbh Polymerically micro-encapsulated pigments
US6849679B2 (en) * 2001-05-21 2005-02-01 Ciba Specialty Chemicals Corporation Pigment compositions with modified block copolymer dispersants

Also Published As

Publication number Publication date
EP1465935B1 (en) 2016-09-07
BR0214616B1 (pt) 2012-08-07
CA2465291A1 (en) 2003-06-05
US20060160950A1 (en) 2006-07-20
US7723425B2 (en) 2010-05-25
US20050004317A1 (en) 2005-01-06
CN100408606C (zh) 2008-08-06
CN1639216A (zh) 2005-07-13
KR20040070197A (ko) 2004-08-06
WO2003046029A1 (en) 2003-06-05
KR100918576B1 (ko) 2009-09-24
AU2002352086A1 (en) 2003-06-10
EP1465935A1 (en) 2004-10-13
TW200407363A (en) 2004-05-16
MXPA04004693A (es) 2004-08-19
BR0214616A (pt) 2004-09-14
JP2005510595A (ja) 2005-04-21

Similar Documents

Publication Publication Date Title
JP4541702B2 (ja) 変性されたａｔｒｐコポリマー分散剤を有する顔料組成物
EP1275689B1 (en) Pigment compositions with modified block copolymer dispersants
JP4758336B2 (ja) 顔料分散体における光安定化ポリマー分散剤
JP5035938B2 (ja) Ａｔｒｐポリマー含有の顔料組成物
JP5290485B2 (ja) Ａｔｒｐマクロモノマーからのクシ型ポリマー

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20051108

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20051108

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20080806

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20090217

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20090512

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20091027

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20100126

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20100202

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20100225

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20100304

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20100325

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20100401

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20100422

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20100608

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20100624

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20130702

Year of fee payment: 3

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees