TW200407363A - Pigment compositions with modified ATRP copolymer dispersants - Google Patents

Info

Publication number

TW200407363A

TW200407363A TW091133302A TW91133302A TW200407363A TW 200407363 A TW200407363 A TW 200407363A TW 091133302 A TW091133302 A TW 091133302A TW 91133302 A TW91133302 A TW 91133302A TW 200407363 A TW200407363 A TW 200407363A

Authority

TW

Taiwan

Prior art keywords

group

alkyl

acid

substituted

scope

Prior art date

2001-11-29

Links

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• 239000000203 mixture Substances 0.000 title claims abstract description 95
• 239000000049 pigment Substances 0.000 title claims abstract description 66
• 239000002270 dispersing agent Substances 0.000 title claims abstract description 23
• 229920001577 copolymer Polymers 0.000 title claims description 76
• 238000010560 atom transfer radical polymerization reaction Methods 0.000 title claims description 28
• 101710141544 Allatotropin-related peptide Proteins 0.000 title 1
• 150000003839 salts Chemical class 0.000 claims abstract description 24
• 229920001400 block copolymer Polymers 0.000 claims abstract description 23
• 239000000976 ink Substances 0.000 claims abstract description 10
• 239000012860 organic pigment Substances 0.000 claims abstract description 10
• 239000001023 inorganic pigment Substances 0.000 claims abstract description 9
• -1 aralkyl halides Chemical class 0.000 claims description 150
• 229920000642 polymer Polymers 0.000 claims description 101
• 239000000178 monomer Substances 0.000 claims description 65
• 125000000217 alkyl group Chemical group 0.000 claims description 63
• 150000001875 compounds Chemical class 0.000 claims description 55
• 238000000034 method Methods 0.000 claims description 55
• 239000002253 acid Substances 0.000 claims description 47
• 238000000576 coating method Methods 0.000 claims description 45
• 229910052757 nitrogen Inorganic materials 0.000 claims description 44
• 239000006185 dispersion Substances 0.000 claims description 37
• 238000006116 polymerization reaction Methods 0.000 claims description 34
• LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 31
• 238000006243 chemical reaction Methods 0.000 claims description 30
• QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 30
• 239000003999 initiator Substances 0.000 claims description 28
• 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 28
• 125000002950 monocyclic group Chemical group 0.000 claims description 27
• 125000003367 polycyclic group Chemical group 0.000 claims description 25
• 229920005989 resin Polymers 0.000 claims description 25
• 239000011347 resin Substances 0.000 claims description 25
• PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 23
• NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 23
• 125000005907 alkyl ester group Chemical group 0.000 claims description 23
• 125000003545 alkoxy group Chemical group 0.000 claims description 22
• 239000003054 catalyst Substances 0.000 claims description 22
• 239000002245 particle Substances 0.000 claims description 22
• 239000000126 substance Substances 0.000 claims description 22
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
• 239000000654 additive Substances 0.000 claims description 19
• 150000001412 amines Chemical class 0.000 claims description 19
• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 18
• 239000011230 binding agent Substances 0.000 claims description 17
• ABLZXFCXXLZCGV-UHFFFAOYSA-N phosphonic acid group Chemical group P(O)(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 claims description 16
• JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 claims description 16
• 229910052736 halogen Inorganic materials 0.000 claims description 15
• 150000002367 halogens Chemical group 0.000 claims description 15
• 239000000463 material Substances 0.000 claims description 15
• LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 claims description 14
• 125000003277 amino group Chemical group 0.000 claims description 14
• 239000012634 fragment Substances 0.000 claims description 14
• 239000007788 liquid Substances 0.000 claims description 14
• NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 13
• 125000001931 aliphatic group Chemical group 0.000 claims description 13
• 239000000853 adhesive Substances 0.000 claims description 12
• 230000001070 adhesive effect Effects 0.000 claims description 12
• 125000003118 aryl group Chemical group 0.000 claims description 12
• 239000003795 chemical substances by application Substances 0.000 claims description 12
• 150000002148 esters Chemical class 0.000 claims description 12
• 229920006395 saturated elastomer Polymers 0.000 claims description 12
• 125000001424 substituent group Chemical group 0.000 claims description 12
• 230000009471 action Effects 0.000 claims description 11
• 239000003505 polymerization initiator Substances 0.000 claims description 11
• 238000001035 drying Methods 0.000 claims description 10
• WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 10
• SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 9
• 150000001252 acrylic acid derivatives Chemical class 0.000 claims description 9
• 150000001732 carboxylic acid derivatives Chemical group 0.000 claims description 9
• 239000000945 filler Substances 0.000 claims description 9
• 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 9
• 238000010526 radical polymerization reaction Methods 0.000 claims description 9
• 235000021419 vinegar Nutrition 0.000 claims description 9
• YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 8
• 150000001350 alkyl halides Chemical class 0.000 claims description 8
• 125000002947 alkylene group Chemical group 0.000 claims description 8
• 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 claims description 8
• 238000007334 copolymerization reaction Methods 0.000 claims description 8
• 229920003023 plastic Polymers 0.000 claims description 8
• 239000004033 plastic Substances 0.000 claims description 8
• 150000003440 styrenes Chemical class 0.000 claims description 8
• 239000000052 vinegar Substances 0.000 claims description 8
• VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 7
• 229910052739 hydrogen Inorganic materials 0.000 claims description 7
• XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 6
• 239000006096 absorbing agent Substances 0.000 claims description 6
• 230000002378 acidificating effect Effects 0.000 claims description 6
• 125000005395 methacrylic acid group Chemical group 0.000 claims description 6
• HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 claims description 5
• 125000004185 ester group Chemical group 0.000 claims description 5
• 108010069898 fibrinogen fragment X Proteins 0.000 claims description 5
• 239000001257 hydrogen Substances 0.000 claims description 5
• 125000004178 (C1-C4) alkyl group Chemical group 0.000 claims description 4
• OSSNTDFYBPYIEC-UHFFFAOYSA-N 1-ethenylimidazole Chemical group C=CN1C=CN=C1 OSSNTDFYBPYIEC-UHFFFAOYSA-N 0.000 claims description 4
• KGIGUEBEKRSTEW-UHFFFAOYSA-N 2-vinylpyridine Chemical compound C=CC1=CC=CC=N1 KGIGUEBEKRSTEW-UHFFFAOYSA-N 0.000 claims description 4
• OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
• UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical compound C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 claims description 4
• GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 4
• 230000003213 activating effect Effects 0.000 claims description 4
• 230000015572 biosynthetic process Effects 0.000 claims description 4
• 239000002131 composite material Substances 0.000 claims description 4
• 150000002576 ketones Chemical class 0.000 claims description 4
• 230000004048 modification Effects 0.000 claims description 4
• 238000012986 modification Methods 0.000 claims description 4
• 150000007524 organic acids Chemical class 0.000 claims description 4
• 239000003973 paint Substances 0.000 claims description 4
• 230000036961 partial effect Effects 0.000 claims description 4
• 239000004014 plasticizer Substances 0.000 claims description 4
• WGYKZJWCGVVSQN-UHFFFAOYSA-N propylamine Chemical compound CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 claims description 4
• 125000000542 sulfonic acid group Chemical group 0.000 claims description 4
• VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 4
• KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 claims description 3
• NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims description 3
• VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical group C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 3
• 239000005977 Ethylene Substances 0.000 claims description 3
• UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 3
• 150000001335 aliphatic alkanes Chemical class 0.000 claims description 3
• 229910052782 aluminium Inorganic materials 0.000 claims description 3
• XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 3
• 125000000751 azo group Chemical group [*]N=N[*] 0.000 claims description 3
• 239000006229 carbon black Substances 0.000 claims description 3
• 239000000975 dye Substances 0.000 claims description 3
• 239000003365 glass fiber Substances 0.000 claims description 3
• 239000010439 graphite Substances 0.000 claims description 3
• 229910002804 graphite Inorganic materials 0.000 claims description 3
• 150000004820 halides Chemical class 0.000 claims description 3
• 125000004435 hydrogen atom Chemical class [H]* 0.000 claims description 3
• 239000004611 light stabiliser Substances 0.000 claims description 3
• 150000003009 phosphonic acids Chemical group 0.000 claims description 3
• 238000005956 quaternization reaction Methods 0.000 claims description 3
• 239000007921 spray Substances 0.000 claims description 3
• 239000004094 surface-active agent Substances 0.000 claims description 3
• 239000013008 thixotropic agent Substances 0.000 claims description 3
• 239000011787 zinc oxide Substances 0.000 claims description 3
• BDKSYBXVYUGXIG-UHFFFAOYSA-N 2-(ethylamino)ethyl prop-2-enoate Chemical compound CCNCCOC(=O)C=C BDKSYBXVYUGXIG-UHFFFAOYSA-N 0.000 claims description 2
• ULEVTQHCVWIDPC-UHFFFAOYSA-N 2-(methylamino)ethyl prop-2-enoate Chemical compound CNCCOC(=O)C=C ULEVTQHCVWIDPC-UHFFFAOYSA-N 0.000 claims description 2
• LBSXSAXOLABXMF-UHFFFAOYSA-N 4-Vinylaniline Chemical compound NC1=CC=C(C=C)C=C1 LBSXSAXOLABXMF-UHFFFAOYSA-N 0.000 claims description 2
• UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 2
• BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 claims description 2
• WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 claims description 2
• 239000004568 cement Substances 0.000 claims description 2
• ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical group [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 claims description 2
• 229910000423 chromium oxide Inorganic materials 0.000 claims description 2
• 238000009833 condensation Methods 0.000 claims description 2
• 239000004035 construction material Substances 0.000 claims description 2
• 150000004696 coordination complex Chemical class 0.000 claims description 2
• 239000013078 crystal Chemical group 0.000 claims description 2
• 125000000664 diazo group Chemical group [N-]=[N+]=[*] 0.000 claims description 2
• 125000004494 ethyl ester group Chemical group 0.000 claims description 2
• 235000011087 fumaric acid Nutrition 0.000 claims description 2
• 239000010440 gypsum Substances 0.000 claims description 2
• 229910052602 gypsum Inorganic materials 0.000 claims description 2
• 235000003642 hunger Nutrition 0.000 claims description 2
• 238000003384 imaging method Methods 0.000 claims description 2
• 235000019239 indanthrene blue RS Nutrition 0.000 claims description 2
• UHOKSCJSTAHBSO-UHFFFAOYSA-N indanthrone blue Chemical compound C1=CC=C2C(=O)C3=CC=C4NC5=C6C(=O)C7=CC=CC=C7C(=O)C6=CC=C5NC4=C3C(=O)C2=C1 UHOKSCJSTAHBSO-UHFFFAOYSA-N 0.000 claims description 2
• VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 2
• 235000013336 milk Nutrition 0.000 claims description 2
• 239000008267 milk Substances 0.000 claims description 2
• 210000004080 milk Anatomy 0.000 claims description 2
• 229910003455 mixed metal oxide Inorganic materials 0.000 claims description 2
• MEFBJEMVZONFCJ-UHFFFAOYSA-N molybdate Chemical group [O-][Mo]([O-])(=O)=O MEFBJEMVZONFCJ-UHFFFAOYSA-N 0.000 claims description 2
• 229910052814 silicon oxide Inorganic materials 0.000 claims description 2
• 239000012265 solid product Substances 0.000 claims description 2
• OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims description 2
• 229910052727 yttrium Inorganic materials 0.000 claims description 2
• MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 claims 4
• WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 3
• UCRIXEWTILHNCG-UHFFFAOYSA-N 1-ethyl-2h-pyridine Chemical compound CCN1CC=CC=C1 UCRIXEWTILHNCG-UHFFFAOYSA-N 0.000 claims 1
• GSQIVVSEVORPJF-UHFFFAOYSA-N 2-(butylamino)ethyl prop-2-enoate Chemical group CCCCNCCOC(=O)C=C GSQIVVSEVORPJF-UHFFFAOYSA-N 0.000 claims 1
• GOJUJUVQIVIZAV-UHFFFAOYSA-N 2-amino-4,6-dichloropyrimidine-5-carbaldehyde Chemical group NC1=NC(Cl)=C(C=O)C(Cl)=N1 GOJUJUVQIVIZAV-UHFFFAOYSA-N 0.000 claims 1
• 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims 1
• MLMQPDHYNJCQAO-UHFFFAOYSA-N 3,3-dimethylbutyric acid Chemical compound CC(C)(C)CC(O)=O MLMQPDHYNJCQAO-UHFFFAOYSA-N 0.000 claims 1
• GQWAOUOHRMHSHL-UHFFFAOYSA-N 4-ethenyl-n,n-dimethylaniline Chemical compound CN(C)C1=CC=C(C=C)C=C1 GQWAOUOHRMHSHL-UHFFFAOYSA-N 0.000 claims 1
• KFDVPJUYSDEJTH-UHFFFAOYSA-N 4-ethenylpyridine Chemical compound C=CC1=CC=NC=C1 KFDVPJUYSDEJTH-UHFFFAOYSA-N 0.000 claims 1
• OCLHNLMDZIPHBE-UHFFFAOYSA-N C(C=C)(=O)N(CCCN(C)C)C1=CC=CC=2C3=CC=CC=C3CC12 Chemical compound C(C=C)(=O)N(CCCN(C)C)C1=CC=CC=2C3=CC=CC=C3CC12 OCLHNLMDZIPHBE-UHFFFAOYSA-N 0.000 claims 1
• 235000000177 Indigofera tinctoria Nutrition 0.000 claims 1
• NRCMAYZCPIVABH-UHFFFAOYSA-N Quinacridone Chemical compound N1C2=CC=CC=C2C(=O)C2=C1C=C1C(=O)C3=CC=CC=C3NC1=C2 NRCMAYZCPIVABH-UHFFFAOYSA-N 0.000 claims 1
• 240000004534 Scutellaria baicalensis Species 0.000 claims 1
• 235000017089 Scutellaria baicalensis Nutrition 0.000 claims 1
• 239000005083 Zinc sulfide Substances 0.000 claims 1
• CQBLUJRVOKGWCF-UHFFFAOYSA-N [O].[AlH3] Chemical compound [O].[AlH3] CQBLUJRVOKGWCF-UHFFFAOYSA-N 0.000 claims 1
• 238000010669 acid-base reaction Methods 0.000 claims 1
• 125000003418 alkyl amino alkoxy group Chemical group 0.000 claims 1
• 239000003963 antioxidant agent Substances 0.000 claims 1
• IFVTZJHWGZSXFD-UHFFFAOYSA-N biphenylene Chemical group C1=CC=C2C3=CC=CC=C3C2=C1 IFVTZJHWGZSXFD-UHFFFAOYSA-N 0.000 claims 1
• 239000011449 brick Substances 0.000 claims 1
• 238000010586 diagram Methods 0.000 claims 1
• ZOOODBUHSVUZEM-UHFFFAOYSA-N ethoxymethanedithioic acid Chemical compound CCOC(S)=S ZOOODBUHSVUZEM-UHFFFAOYSA-N 0.000 claims 1
• 125000003827 glycol group Chemical group 0.000 claims 1
• 125000004051 hexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims 1
• 229940097275 indigo Drugs 0.000 claims 1
• COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 claims 1
• GWVMLCQWXVFZCN-UHFFFAOYSA-N isoindoline Chemical compound C1=CC=C2CNCC2=C1 GWVMLCQWXVFZCN-UHFFFAOYSA-N 0.000 claims 1
• 150000002596 lactones Chemical class 0.000 claims 1
• 230000005291 magnetic effect Effects 0.000 claims 1
• 150000004702 methyl esters Chemical class 0.000 claims 1
• CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 claims 1
• 125000002347 octyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims 1
• IEQIEDJGQAUEQZ-UHFFFAOYSA-N phthalocyanine Chemical compound N1C(N=C2C3=CC=CC=C3C(N=C3C4=CC=CC=C4C(=N4)N3)=N2)=C(C=CC=C2)C2=C1N=C1C2=CC=CC=C2C4=N1 IEQIEDJGQAUEQZ-UHFFFAOYSA-N 0.000 claims 1
• MZBILCSYBHTKQX-UHFFFAOYSA-N pyrene-4,9-dione Chemical compound C=1C=CC2=CC(C3=CC=CC4=CC(C1C2=C34)=O)=O MZBILCSYBHTKQX-UHFFFAOYSA-N 0.000 claims 1
• 238000000926 separation method Methods 0.000 claims 1
• 238000005987 sulfurization reaction Methods 0.000 claims 1
• JOUDBUYBGJYFFP-FOCLMDBBSA-N thioindigo Chemical compound S\1C2=CC=CC=C2C(=O)C/1=C1/C(=O)C2=CC=CC=C2S1 JOUDBUYBGJYFFP-FOCLMDBBSA-N 0.000 claims 1
• NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 claims 1
• 239000012991 xanthate Substances 0.000 claims 1
• LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 claims 1
• 229910000165 zinc phosphate Inorganic materials 0.000 claims 1
• 229910052984 zinc sulfide Inorganic materials 0.000 claims 1
• DRDVZXDWVBGGMH-UHFFFAOYSA-N zinc;sulfide Chemical compound [S-2].[Zn+2] DRDVZXDWVBGGMH-UHFFFAOYSA-N 0.000 claims 1
• 239000008199 coating composition Substances 0.000 abstract description 21
• 238000012546 transfer Methods 0.000 abstract description 4
• 239000004922 lacquer Substances 0.000 abstract 1
• 239000011248 coating agent Substances 0.000 description 26
• 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 21
• IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 20
• 239000002904 solvent Substances 0.000 description 19
• 239000000243 solution Substances 0.000 description 18
• QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 16
• 238000002360 preparation method Methods 0.000 description 16
• 239000007787 solid Substances 0.000 description 16
• 238000007792 addition Methods 0.000 description 15
• 239000012964 benzotriazole Substances 0.000 description 14
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 13
• XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical group CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 13
• 229940048053 acrylate Drugs 0.000 description 13
• JROGBPMEKVAPEH-GXGBFOEMSA-N emetine dihydrochloride Chemical compound Cl.Cl.N1CCC2=CC(OC)=C(OC)C=C2[C@H]1C[C@H]1C[C@H]2C3=CC(OC)=C(OC)C=C3CCN2C[C@@H]1CC JROGBPMEKVAPEH-GXGBFOEMSA-N 0.000 description 13
• 239000003960 organic solvent Substances 0.000 description 13
• 238000003756 stirring Methods 0.000 description 13
• QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 description 12
• 239000007789 gas Substances 0.000 description 12
• 239000003446 ligand Substances 0.000 description 12
• 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 11
• JAXFJECJQZDFJS-XHEPKHHKSA-N gtpl8555 Chemical compound OC(=O)C[C@H](N)C(=O)N[C@@H](CCC(O)=O)C(=O)N[C@@H](C(C)C)C(=O)N[C@@H](C(C)C)C(=O)N1CCC[C@@H]1C(=O)N[C@H](B1O[C@@]2(C)[C@H]3C[C@H](C3(C)C)C[C@H]2O1)CCC1=CC=C(F)C=C1 JAXFJECJQZDFJS-XHEPKHHKSA-N 0.000 description 11
• 239000000460 chlorine Substances 0.000 description 10
• 238000003801 milling Methods 0.000 description 10
• PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 9
• OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
• DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 9
• 238000004458 analytical method Methods 0.000 description 9
• OBNCKNCVKJNDBV-UHFFFAOYSA-N butanoic acid ethyl ester Natural products CCCC(=O)OCC OBNCKNCVKJNDBV-UHFFFAOYSA-N 0.000 description 9
• 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 9
• 235000019441 ethanol Nutrition 0.000 description 9
• 229910052751 metal Inorganic materials 0.000 description 9
• 239000002184 metal Substances 0.000 description 9
• 239000011541 reaction mixture Substances 0.000 description 9
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