JP4515094B2 - 飼料用酵素含有顆粒 - Google Patents
飼料用酵素含有顆粒 Download PDFInfo
- Publication number
- JP4515094B2 JP4515094B2 JP2003559260A JP2003559260A JP4515094B2 JP 4515094 B2 JP4515094 B2 JP 4515094B2 JP 2003559260 A JP2003559260 A JP 2003559260A JP 2003559260 A JP2003559260 A JP 2003559260A JP 4515094 B2 JP4515094 B2 JP 4515094B2
- Authority
- JP
- Japan
- Prior art keywords
- enzyme
- polyolefin
- granules
- feed
- granule
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
- A23K40/10—Shaping or working-up of animal feeding-stuffs by agglomeration; by granulation, e.g. making powders
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/105—Aliphatic or alicyclic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/189—Enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
- A23K40/30—Shaping or working-up of animal feeding-stuffs by encapsulating; by coating
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Polymers & Plastics (AREA)
- Zoology (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Animal Husbandry (AREA)
- Fodder In General (AREA)
- Enzymes And Modification Thereof (AREA)
- General Preparation And Processing Of Foods (AREA)
- Seeds, Soups, And Other Foods (AREA)
Description
フィターゼ含有顆粒の製造
フィターゼ含有顆粒は、国際公開WO98/54980に記載される方法にしたがって製造する。
50グラムの顆粒を10 kgの選択した飼料のプレミックスと混合し、試験直前に240 kgの同じレシピのものと混合した。この250 kg の混合物を、ミキサー/コンディショナー中で600 kg/時の速度の混合スクリューによって混合した。この際約80℃の直接蒸気により加熱した。滞留時間の約30〜40秒間が経過した時、この熱い混合物をペレット圧縮機中に入れた。型から出てきたペレットは80〜82℃の温度を示し、冷却ベルト上に置いた。このベルトから、安定性測定のためにサンプルを回収した。
トウモロコシ(50%)、豆類(5%)、大豆ミール(28%)、タピオカ(1.98%)、フィッシュミール(2.5%)、フェザーミール(1.5%)、大豆油(1.75%)、動物性脂肪(3.5%)、Mervit (Premervo, Utrecht, オランダ) 100 (1%)、ライムストーン(1.1%)、リン酸モノカルシウム(1.22%)、塩(0.3%)、Mervit 394 (0.65%)、Mervit 393 (1.5%)、全量 100%。
フィターゼ活性は、"ISL法 61696" (マニュアル モリブデン酸-バナジウム酸アッセイ)の手順にしたがって測定した。
300グラムの非コーティング顆粒(バッチNPHG 498)を、NIRO-AEROMATIC製のSTREA流動床装置中に入れた。
フィターゼ含有顆粒のペレット化安定性に及ぼすコーティング剤Dispersion1205の影響を大規模製造において調べた。
Glatt製 流動床型コーティング装置GPCG1.1中、一般的方法の項において記載したようにして製造した非コーティング顆粒1 kgを、表3に記載したように様々なコーティングでコーティングした。
Dispersion 1205の濃度の違い(2〜24%, サンプルS〜V)が、ペレット化安定性に及ぼす影響と顆粒の溶解時間に及ぼす影響について試験した。非コーティング顆粒は、一般的方法の項において記載したようにして製造した。該顆粒は、表4に示したようにコーティングし、一般的方法の項において記載したペレット化試験を行った。
本実施例においては、異なる供給業者から入手したポリプロピレン(PP)分散物およびポリエチレン(PE)分散物の影響について調べた。非コーティング顆粒は、一般的方法の項に記載したようにして製造した。次いで、表5に示すように顆粒をコーティングし、一般的方法において記載したようにしてペレット化試験を行った。
本実施例においては、異なる供給業者から入手したポリプロピレン(PP)分散物およびポリエチレン(PE)分散物の影響について別の比較を行った。非コーティング顆粒は、一般的方法の項に記載したようにして製造した。次いで、表6に示すように顆粒をコーティングし、一般的方法において記載したようにしてペレット化試験を行った。
Claims (16)
- 動物用飼料中で使用するのに適した酵素含有顆粒の製造方法であって、乾燥酵素含有顆粒を取得する工程と、ポリオレフィンを用いて該顆粒をコーティングする工程と、を含んでなり、該ポリオレフィンがポリエチレン、ポリプロピレン、ポリブチレンおよびポリブタジエンからなる群より選択され、該ポリオレフィンが適切な溶媒中のポリオレフィン粒子の分散物として顆粒に適用され、かつポリオレフィンが、アミンによって安定化された酸性基を含むことを特徴とする、上記方法。
- 該ポリオレフィンを、顆粒の重量あたりのポリオレフィンの重量が0.1〜20%の割合で適用する、請求項1記載の方法。
- 該ポリオレフィンが、100〜200℃(境界値含む)の範囲の温度に溶融温度の境界値を有する、請求項1または2記載の方法。
- 溶媒が水である、請求項1〜3のいずれか1項記載の方法。
- ポリオレフィン粒子が、10〜1000 nm (境界値含む)の範囲の粒径を有する、請求項1〜4のいずれか1項記載の方法。
- ポリオレフィン分散物が、10〜60 % (w/w)のポリオレフィンを含有する、請求項1〜5のいずれか1項記載の方法。
- 酸性基がカルボキシル基である、請求項1〜6のいずれか1項記載の方法。
- アミンがアンモニアである、請求項1〜7のいずれか1項記載の方法。
- 酵素が、フィターゼ、キシラナーゼ、β-グルカナーゼ、プロテアーゼ、ホスホリパーゼ、アミラーゼおよび/またはグルコースオキシダーゼである、請求項1〜8のいずれか1項記載の方法。
- 請求項1〜9のいずれか1項記載の方法によって取得することができるポリオレフィンによってコーティングされている酵素含有顆粒であって、該ポリオレフィンがポリエチレン、ポリプロピレン、ポリブチレンおよびポリブタジエンからなる群より選択され、かつポリオレフィンが、アミンによって安定化された酸性基を含むことを特徴とする、上記酵素含有顆粒。
- 動物用飼料または動物用飼料のプレミックスもしくは前駆物質の製造方法であって、請求項10記載の顆粒と、1種以上の動物用飼料物質または動物用飼料成分とを混合する工程を含んでなる、上記方法。
- 飼料用物質と顆粒との混合物を蒸気処理し、ペレット化し、冷却する、請求項11記載の方法。
- 請求項10記載の顆粒を含んでなる飼料組成物。
- 動物の成長を促進させる方法であって、請求項10記載の顆粒または請求項13記載の組成物を含む食餌を動物に与えることを含んでなる、上記方法。
- 動物用飼料中でのまたは動物用食餌中の成分としての、請求項10記載の顆粒の使用。
- 酵素のペレット化安定性を向上させるための、請求項10記載の顆粒の使用。
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP02075016 | 2002-01-15 | ||
PCT/EP2003/000342 WO2003059087A1 (en) | 2002-01-15 | 2003-01-14 | Granulates containing feed-enzymes |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2005514050A JP2005514050A (ja) | 2005-05-19 |
JP4515094B2 true JP4515094B2 (ja) | 2010-07-28 |
Family
ID=8185493
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2003559260A Expired - Lifetime JP4515094B2 (ja) | 2002-01-15 | 2003-01-14 | 飼料用酵素含有顆粒 |
Country Status (16)
Country | Link |
---|---|
US (1) | US7501269B2 (ja) |
EP (1) | EP1467630B2 (ja) |
JP (1) | JP4515094B2 (ja) |
KR (1) | KR100906838B1 (ja) |
CN (1) | CN100345494C (ja) |
AT (1) | ATE369043T1 (ja) |
BR (1) | BR0306917A (ja) |
CA (1) | CA2471475C (ja) |
DE (1) | DE60315412T3 (ja) |
DK (1) | DK1467630T4 (ja) |
MX (1) | MXPA04006218A (ja) |
NO (1) | NO20043343L (ja) |
PL (1) | PL207550B1 (ja) |
RU (1) | RU2348175C9 (ja) |
WO (1) | WO2003059087A1 (ja) |
ZA (1) | ZA200406443B (ja) |
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AU755302B2 (en) * | 1998-04-02 | 2002-12-12 | Genencor International, Inc. | Modified starch coating |
DE19859385A1 (de) * | 1998-12-22 | 2000-06-29 | Basf Ag | Verfahren zur Herstellung von enzymhaltigen Granulaten |
EP1069832B1 (en) * | 1999-02-10 | 2004-05-06 | Basf Aktiengesellschaft | Granulates containing feed-enzymes |
DE19929257A1 (de) | 1999-06-25 | 2000-12-28 | Basf Ag | Polymerbeschichtete, granulierte enzymhaltige Futtermittelzusätze und Verfahren zu deren Herstellung |
AU7405400A (en) | 1999-10-01 | 2001-05-10 | Novozymes A/S | Enzyme granulate |
US20020094367A1 (en) | 2000-09-08 | 2002-07-18 | Novozymes A/S | Dough composition |
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2003
- 2003-01-14 US US10/500,144 patent/US7501269B2/en not_active Expired - Lifetime
- 2003-01-14 AT AT03701512T patent/ATE369043T1/de not_active IP Right Cessation
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- 2003-01-14 WO PCT/EP2003/000342 patent/WO2003059087A1/en active IP Right Grant
- 2003-01-14 CN CNB038022699A patent/CN100345494C/zh not_active Expired - Lifetime
- 2003-01-14 MX MXPA04006218A patent/MXPA04006218A/es active IP Right Grant
- 2003-01-14 PL PL369759A patent/PL207550B1/pl unknown
- 2003-01-14 BR BR0306917-6A patent/BR0306917A/pt not_active Application Discontinuation
- 2003-01-14 DK DK03701512.0T patent/DK1467630T4/da active
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Also Published As
Publication number | Publication date |
---|---|
KR100906838B1 (ko) | 2009-07-08 |
DE60315412T3 (de) | 2012-09-20 |
JP2005514050A (ja) | 2005-05-19 |
DK1467630T3 (da) | 2007-11-05 |
RU2348175C9 (ru) | 2011-12-20 |
CN100345494C (zh) | 2007-10-31 |
PL207550B1 (pl) | 2010-12-31 |
AU2003202563A1 (en) | 2003-07-30 |
DK1467630T4 (da) | 2011-07-25 |
EP1467630A1 (en) | 2004-10-20 |
US20050163765A1 (en) | 2005-07-28 |
BR0306917A (pt) | 2004-11-09 |
CA2471475C (en) | 2011-01-04 |
US7501269B2 (en) | 2009-03-10 |
NO20043343L (no) | 2004-08-11 |
KR20040078665A (ko) | 2004-09-10 |
RU2004124941A (ru) | 2005-05-10 |
ATE369043T1 (de) | 2007-08-15 |
ZA200406443B (en) | 2005-10-26 |
MXPA04006218A (es) | 2004-11-01 |
EP1467630B1 (en) | 2007-08-08 |
PL369759A1 (en) | 2005-05-02 |
WO2003059087A1 (en) | 2003-07-24 |
DE60315412D1 (de) | 2007-09-20 |
RU2348175C2 (ru) | 2009-03-10 |
EP1467630B2 (en) | 2011-04-20 |
CA2471475A1 (en) | 2003-07-24 |
CN1615085A (zh) | 2005-05-11 |
DE60315412T2 (de) | 2008-04-30 |
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