JP4435307B2 - 化学プロセス・プラントのオンライン制御 - Google Patents

化学プロセス・プラントのオンライン制御 Download PDF

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JP4435307B2
JP4435307B2 JP53015698A JP53015698A JP4435307B2 JP 4435307 B2 JP4435307 B2 JP 4435307B2 JP 53015698 A JP53015698 A JP 53015698A JP 53015698 A JP53015698 A JP 53015698A JP 4435307 B2 JP4435307 B2 JP 4435307B2
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spectrum
polymer
value
corrected
group
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JP2001508354A (ja
JP2001508354A5 (enExample
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マクドナルド、マイケル・エフ
ロング、ロバート・エル
トマス、カール・ジェイ
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エクソンモービル・ケミカル・パテンツ・インク
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    • GPHYSICS
    • G05CONTROLLING; REGULATING
    • G05DSYSTEMS FOR CONTROLLING OR REGULATING NON-ELECTRIC VARIABLES
    • G05D21/00Control of chemical or physico-chemical variables, e.g. pH value
    • G05D21/02Control of chemical or physico-chemical variables, e.g. pH value characterised by the use of electric means
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F210/00Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F210/04Monomers containing three or four carbon atoms
    • C08F210/08Butenes
    • C08F210/10Isobutene
    • C08F210/12Isobutene with conjugated diolefins, e.g. butyl rubber
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J3/00Spectrometry; Spectrophotometry; Monochromators; Measuring colours
    • G01J3/28Investigating the spectrum
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01JMEASUREMENT OF INTENSITY, VELOCITY, SPECTRAL CONTENT, POLARISATION, PHASE OR PULSE CHARACTERISTICS OF INFRARED, VISIBLE OR ULTRAVIOLET LIGHT; COLORIMETRY; RADIATION PYROMETRY
    • G01J3/00Spectrometry; Spectrophotometry; Monochromators; Measuring colours
    • G01J3/28Investigating the spectrum
    • G01J3/45Interferometric spectrometry
    • G01J3/453Interferometric spectrometry by correlation of the amplitudes
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/3563Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light for analysing solids; Preparation of samples therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/359Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using near infrared light
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84Systems specially adapted for particular applications
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2400/00Characteristics for processes of polymerization
    • C08F2400/02Control or adjustment of polymerization parameters
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N2021/3595Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using FTIR
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84Systems specially adapted for particular applications
    • G01N2021/8411Application to online plant, process monitoring
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2201/00Features of devices classified in G01N21/00
    • G01N2201/12Circuits of general importance; Signal processing
    • G01N2201/129Using chemometrical methods

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  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • General Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Automation & Control Theory (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)
  • Control Of Non-Electrical Variables (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Polymerisation Methods In General (AREA)
  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)
JP53015698A 1996-12-31 1997-12-31 化学プロセス・プラントのオンライン制御 Expired - Lifetime JP4435307B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US3461496P 1996-12-31 1996-12-31
US60/034,614 1996-12-31
PCT/US1997/023734 WO1998029787A1 (en) 1996-12-31 1997-12-31 On-line control of a chemical process plant

Publications (3)

Publication Number Publication Date
JP2001508354A JP2001508354A (ja) 2001-06-26
JP2001508354A5 JP2001508354A5 (enExample) 2005-09-08
JP4435307B2 true JP4435307B2 (ja) 2010-03-17

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Application Number Title Priority Date Filing Date
JP53015698A Expired - Lifetime JP4435307B2 (ja) 1996-12-31 1997-12-31 化学プロセス・プラントのオンライン制御

Country Status (17)

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US (1) US6072576A (enExample)
EP (1) EP0948761B2 (enExample)
JP (1) JP4435307B2 (enExample)
KR (1) KR100500802B1 (enExample)
CN (1) CN1105956C (enExample)
AU (1) AU727750B2 (enExample)
BR (1) BR9714450A (enExample)
CA (1) CA2276624C (enExample)
DE (1) DE69705323T3 (enExample)
ES (1) ES2160983T5 (enExample)
IL (1) IL130731A (enExample)
MY (1) MY117038A (enExample)
NO (1) NO316346B1 (enExample)
PL (1) PL334397A1 (enExample)
RU (1) RU99116247A (enExample)
TW (2) TW558557B (enExample)
WO (1) WO1998029787A1 (enExample)

Families Citing this family (121)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19736310A1 (de) * 1997-08-21 1999-02-25 Bayer Ag Verfahren zur Herstellung von teilhydrierten Acrylnitril-Butadien-Kautschuken (HNBR) unter on-line-Anwendung der Raman-Spektroskopie
US6200134B1 (en) 1998-01-20 2001-03-13 Kerr Corporation Apparatus and method for curing materials with radiation
EP1094926B1 (en) * 1998-07-06 2002-04-10 ExxonMobil Chemical Patents Inc. Apparatus and method for dewatering an elastomeric polymer
US6635224B1 (en) * 1998-10-30 2003-10-21 General Electric Company Online monitor for polymer processes
FI991542L (fi) * 1999-07-06 2001-01-07 Neste Chemicals Oy Menetelmä moniarvoisten alkoholien valmistusprosessin ohjaamiseksi
US6748334B1 (en) * 1999-12-06 2004-06-08 Jorge E. Perez Specialty gas analysis system
WO2001082008A1 (en) 2000-04-27 2001-11-01 Bp Corporation North America Inc. Method for control of a chemical manufacturing process
WO2002012969A1 (en) * 2000-08-07 2002-02-14 Mitsui Chemicals, Inc. Production control method
US6632680B1 (en) * 2000-09-22 2003-10-14 Deslauriers Paul J. Measurement of short chain branching in olefin copolymers using chemometric analysis
GB0026173D0 (en) * 2000-10-26 2000-12-13 Imerys Minerals Ltd Processing of inorganic particulate materials
US7194369B2 (en) * 2001-07-23 2007-03-20 Cognis Corporation On-site analysis system with central processor and method of analyzing
KR100749589B1 (ko) * 2001-10-25 2007-08-14 에스케이에너지 주식회사 에틸렌 제조공정에 근적외선 분광분석 기술을 적용하는 방법
ATE389174T1 (de) * 2001-10-30 2008-03-15 Lanxess Deutschland Gmbh Bestimmung des reaktionsfortschritts von pfropfpolymerisationsreaktionen
CA2466318A1 (en) 2001-11-09 2003-05-22 Exxonmobil Chemical Patents Inc. On-line measurement and control of polymer properties by raman spectroscopy
US7307257B2 (en) * 2002-01-01 2007-12-11 Exxonmobil Chemical Patents Inc. Method and apparatus for on-line measurement of polymer properties
US6847899B2 (en) 2002-04-26 2005-01-25 Dean Allgeyer, M.D., Inc. Device and method for qualitative and quantitative determination of intravenous fluid components
CN100415779C (zh) * 2002-10-15 2008-09-03 埃克森美孚化学专利公司 通过喇曼光谱法在线测量和控制聚合物性能
CN1708352A (zh) * 2002-10-28 2005-12-14 Bp北美公司 采用在线仪器数据转换的化学制造工艺和方法
US7319040B2 (en) * 2002-10-28 2008-01-15 Ineos Usa Llc Process control using on-line instrumentation and process models
AU2003302739A1 (en) * 2003-01-06 2004-08-10 Exxonmobil Chemical Patents Inc. On-line measurement and control of polymer product properties by raman spectroscopy
DE10304615A1 (de) * 2003-02-05 2004-08-19 Bayer Ag Verfahren zur Überwachung und Führung von Nitrierprozessen mit Hilfe von Online-Spektrometern
DE10322439A1 (de) * 2003-05-19 2004-12-09 Bayer Ag Verfahren und Vorrichtung zur Bestimmung der Isomerenzusammensetzung bei Isocyanat-Herstellprozessen
PL1636272T5 (pl) * 2003-06-20 2012-01-31 Akzo Nobel Nv Sposób polimeryzacji z dozowaniem inicjatorów
US7402635B2 (en) * 2003-07-22 2008-07-22 Fina Technology, Inc. Process for preparing polyethylene
DE10336875A1 (de) * 2003-08-11 2005-03-17 Bayer Chemicals Ag Spektroskopische Konzentrationsbestimmung in einer Rektifikationskolonne
WO2005068516A2 (en) * 2004-01-14 2005-07-28 Chevron Phillips Chemical Company Lp Method and apparatus for monitoring polyolefin production
US7400941B2 (en) * 2004-01-14 2008-07-15 Chrevron Phillips Chemical Company Lp Method and apparatus for monitoring polyolefin production
CA2470887C (en) * 2004-06-14 2014-10-21 Nova Chemicals Corporation Detection of gels in a solution polymerization
WO2006020287A1 (en) * 2004-08-02 2006-02-23 Union Carbide Chemicals & Plastics Technology Corporation Stabilization of a hydroformylation process
US20060190137A1 (en) * 2005-02-18 2006-08-24 Steven W. Free Chemometric modeling software
JP4530040B2 (ja) 2005-03-31 2010-08-25 日立化成工業株式会社 ポリイミドの溶解速度評価方法、ポリイミドの製造方法、及びこれらの方法を用いて得られるポリイミド
DE102005020352A1 (de) * 2005-05-02 2007-08-16 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Steuerung eines technischen Produktionsprozesses für technische Bauteile oder chemische Produkte/Erzeugnisse als technische Produkte
US7505129B2 (en) 2005-07-22 2009-03-17 Exxonmobil Chemical Patents Inc. On-line analysis of polymer properties for control of a solution phase reaction system
US7505127B2 (en) * 2005-07-22 2009-03-17 Exxonmobil Chemical Patents Inc. On-line raman analysis and control of a high pressure reaction system
US7483129B2 (en) * 2005-07-22 2009-01-27 Exxonmobil Chemical Patents Inc. On-line properties analysis of a molten polymer by raman spectroscopy for control of a mixing device
CA2617100A1 (en) * 2005-07-29 2007-02-08 Exxonmobil Research And Engineering Company Method to determine predictive tests and device applying same to lubricant formulations
DE102005036643A1 (de) * 2005-08-04 2007-02-08 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Verfahren und Vorrichtung zur Ermittlung des Reifezustandes von Duroplast-Zusammensetzungen
US20070059838A1 (en) * 2005-09-13 2007-03-15 Pavilion Technologies, Inc. Dynamic constrained optimization of chemical manufacturing
US7764379B1 (en) 2005-12-20 2010-07-27 Axsun Technologies, Inc. Semiconductor laser natural gas analysis system and method
US7803629B2 (en) * 2006-06-27 2010-09-28 Chevron Phillips Chemical Company, Lp Method for employing SEC-FTIR data to predict mechanical properties of polyethylene
DE102006052673A1 (de) * 2006-11-07 2008-05-08 Thomas Schneider Verfahren und Vorrichtung zur Rekalibrierung von Herstellungsprozessen
US7756657B2 (en) * 2006-11-14 2010-07-13 Abb Inc. System for storing and presenting sensor and spectrum data for batch processes
KR100913232B1 (ko) * 2007-05-31 2009-08-24 학교법인 서강대학교 석유화학공정의 온라인 최적화 시스템 및 최적화 방법
EP2014641A3 (en) * 2007-06-06 2009-03-18 Huntsman International Llc Process for preparing mixtures of diphenylmethane diisocyanates and polyphenyl polymethylene polyisocyanates
CA2690078A1 (en) * 2007-06-15 2008-12-18 Bp Chemicals Limited A method for the online analysis of a vapour phase process stream
US20090060783A1 (en) * 2007-09-04 2009-03-05 Kenneth Charles Barrett Polymer concentration monitoring system and use thereof
US20090192340A1 (en) * 2007-11-01 2009-07-30 Robert Dielman Culp Alkylaromatic dehydrogenation system and method for monitoring and controlling the system
US9072572B2 (en) 2009-04-02 2015-07-07 Kerr Corporation Dental light device
US9066777B2 (en) 2009-04-02 2015-06-30 Kerr Corporation Curing light device
MY160821A (en) 2009-05-29 2017-03-31 Exxonmobil Chemical Patents Inc Feedback and feedforward closed loop purity and recovery control
EP2460017B1 (en) * 2009-07-30 2018-08-01 SGS North America Inc. Pvt analysis of pressurized fluids
US9223301B2 (en) * 2010-04-19 2015-12-29 Honeywell International Inc. Active cloud point controller for refining applications and related method
US8645082B2 (en) * 2010-09-13 2014-02-04 Mks Instruments, Inc. Monitoring, detecting and quantifying chemical compounds in a sample
US20120085151A1 (en) * 2010-10-07 2012-04-12 Bayer Materialscience Ag Method and apparatus for characterizing polymers
PL2625211T3 (pl) * 2010-10-08 2017-08-31 Arlanxeo Deutschland Gmbh Monitorowanie aktywności i kontrola sposobu polimeryzacji
US8843324B2 (en) 2011-02-03 2014-09-23 Nova Chemicals (International) S.A. Double derivative NIR process control
US8618226B2 (en) 2011-05-19 2013-12-31 Bridgestone Corporation Method for quantitative analysis of styrene microblock content
JP5845001B2 (ja) * 2011-06-01 2016-01-20 出光興産株式会社 水添石油樹脂の製造方法、および、水添石油樹脂ペレットの製造プラント
WO2013065035A1 (en) 2011-11-03 2013-05-10 Verifood Ltd. Low-cost spectrometry system for end-user food analysis
EP2791671A1 (en) * 2011-12-16 2014-10-22 Halliburton Energy Services, Inc. Methods of calibration transfer for a testing instrument
WO2013169809A1 (en) * 2012-05-08 2013-11-14 Panaridus, Llc System and apparatus for analysis of a guayule plant in situ
US9170155B2 (en) 2012-05-08 2015-10-27 Panaridus, Llc System and apparatus for analysis of a guayule plant in situ
CN104684875A (zh) * 2012-10-01 2015-06-03 巴斯夫欧洲公司 通过萃取蒸馏分离烃的混合物的方法
EP4006542B1 (en) 2013-08-02 2025-10-01 Verifood Ltd. Spectrometer comprising sample illuminator
JP2017505901A (ja) 2014-01-03 2017-02-23 ベリフード, リミテッドVerifood, Ltd. 分光システム、方法、および用途
CN104049624B (zh) * 2014-07-07 2017-07-11 蓝星(北京)技术中心有限公司 化工产品生产模式优化方法、装置和连续型化工系统
EP3201598A4 (en) * 2014-10-01 2018-02-28 Advanced Polymer Monitoring Technologies Inc. Systems and methods for control of polymer reactions and processing using automatic continuous online monitoring
WO2016063284A2 (en) 2014-10-23 2016-04-28 Verifood, Ltd. Accessories for handheld spectrometer
WO2016109554A1 (en) * 2014-12-29 2016-07-07 Bridgestone Corporation Methods for quantifying rubber content in a plant with nmr
WO2016118507A1 (en) * 2015-01-22 2016-07-28 Advanced Polymer Monitoring Technologies, Inc. Systems and methods for predicting and controlling the properties of a chemical species during a time-dependent process
WO2016125164A2 (en) 2015-02-05 2016-08-11 Verifood, Ltd. Spectrometry system applications
WO2016125165A2 (en) 2015-02-05 2016-08-11 Verifood, Ltd. Spectrometry system with visible aiming beam
WO2016162865A1 (en) 2015-04-07 2016-10-13 Verifood, Ltd. Detector for spectrometry system
CN104792725B (zh) * 2015-04-30 2018-01-23 西安近代化学研究所 乙醇胺脱水制备氮丙啶产物流的快速分析方法
US10066990B2 (en) 2015-07-09 2018-09-04 Verifood, Ltd. Spatially variable filter systems and methods
US20170097330A1 (en) * 2015-10-05 2017-04-06 Honeywell International Inc. Hybrid analyzer for fluid processing processes
DE102015223789A1 (de) * 2015-10-07 2017-04-13 Sms Group Gmbh Online Analytik mittels Nahinfrarotspektroskopie-Analytik NIR insbesondere zur Herstellung von Polyaluminiumchloridhydroxid
US10203246B2 (en) 2015-11-20 2019-02-12 Verifood, Ltd. Systems and methods for calibration of a handheld spectrometer
CN106892843A (zh) * 2015-12-17 2017-06-27 英尼奥斯欧洲股份公司 回收塔控制
EP3427031B1 (en) * 2016-03-07 2025-12-17 Yokogawa Fluence Analytics, Inc. Device and methods for simultaneous determination of intrinsic viscosity and non-newtonian behavior of polymers
US10254215B2 (en) 2016-04-07 2019-04-09 Verifood, Ltd. Spectrometry system applications
EP3488204A4 (en) 2016-07-20 2020-07-22 Verifood Ltd. ACCESSORIES FOR HANDLABLE SPECTROMETERS
US10791933B2 (en) 2016-07-27 2020-10-06 Verifood, Ltd. Spectrometry systems, methods, and applications
IT201600081868A1 (it) * 2016-08-03 2018-02-03 Versalis Spa Metodo e sistema per il controllo di un impianto di produzione in continuo di un polimero.
CN106290068A (zh) * 2016-08-25 2017-01-04 青岛励赫化工科技有限公司 一种胶料半部件表面粘性在线检测装置及其使用方法
GB201616787D0 (en) * 2016-10-03 2016-11-16 Renishaw Plc Measurement apparatus and methods
CN107957379B (zh) * 2016-10-18 2020-07-24 中国石油化工股份有限公司 在线连续检测设备和方法以及聚合反应系统和方法
CN106526653B (zh) * 2016-12-19 2023-02-28 桂林百锐光电技术有限公司 一种闪烁探测器
KR102153474B1 (ko) * 2017-06-20 2020-09-08 주식회사 엘지화학 에틸렌 비닐아세테이트 공중합 공정 제어 시스템 및 그 제어 방법
US10696906B2 (en) 2017-09-29 2020-06-30 Marathon Petroleum Company Lp Tower bottoms coke catching device
US11098139B2 (en) * 2018-02-28 2021-08-24 Chevron Phillips Chemical Company Lp Advanced quality control tools for manufacturing bimodal and multimodal polyethylene resins
JP7087468B2 (ja) * 2018-03-08 2022-06-21 東ソー株式会社 脂肪族-芳香族石油樹脂の製法
SG11202008576WA (en) 2018-03-28 2020-10-29 Dow Global Technologies Llc Method to monitor and control the polymerization of a polymer
CN110873699A (zh) * 2018-08-30 2020-03-10 广东生益科技股份有限公司 粘结片的在线质量控制方法、装置、系统和存储介质
US12000720B2 (en) 2018-09-10 2024-06-04 Marathon Petroleum Company Lp Product inventory monitoring
EP3864384A4 (en) 2018-10-08 2022-06-29 Verifood Ltd. Accessories for optical spectrometers
KR102479346B1 (ko) 2018-11-12 2022-12-19 주식회사 엘지화학 폴리올레핀 제조 공정에서의 파울링 예측 방법
EP3711852A1 (de) 2019-03-21 2020-09-23 Covestro Deutschland AG Verfahren und vorrichtung zur quantitativen überwachung der zusammensetzung einer oligomer-/monomermischung
US12031676B2 (en) 2019-03-25 2024-07-09 Marathon Petroleum Company Lp Insulation securement system and associated methods
US11975316B2 (en) 2019-05-09 2024-05-07 Marathon Petroleum Company Lp Methods and reforming systems for re-dispersing platinum on reforming catalyst
US11384174B2 (en) 2019-05-15 2022-07-12 Exxonmobil Chemical Patents Inc. Detection of polymer concentration in polymerization process using refractive index measurement
CA3081520C (en) 2019-05-30 2023-10-31 Marathon Petroleum Company Lp Methods and systems for minimizing nox and co emissions in natural draft heaters
CN112676193B (zh) * 2019-10-18 2022-08-09 李和伟 光谱检测在检测改性膜布质量中的应用及检测方法和检测设备
US11352577B2 (en) 2020-02-19 2022-06-07 Marathon Petroleum Company Lp Low sulfur fuel oil blends for paraffinic resid stability and associated methods
WO2022150743A1 (en) * 2021-01-11 2022-07-14 Avery Dennison Corporation Apparatus for polymerizing or devolatilizing a composition and method using the same
US11898109B2 (en) 2021-02-25 2024-02-13 Marathon Petroleum Company Lp Assemblies and methods for enhancing control of hydrotreating and fluid catalytic cracking (FCC) processes using spectroscopic analyzers
US12473500B2 (en) 2021-02-25 2025-11-18 Marathon Petroleum Company Lp Assemblies and methods for enhancing control of fluid catalytic cracking (FCC) processes using spectroscopic analyzers
US12461022B2 (en) 2021-02-25 2025-11-04 Marathon Petroleum Company Lp Methods and assemblies for determining and using standardized spectral responses for calibration of spectroscopic analyzers
US11702600B2 (en) 2021-02-25 2023-07-18 Marathon Petroleum Company Lp Assemblies and methods for enhancing fluid catalytic cracking (FCC) processes during the FCC process using spectroscopic analyzers
US11905468B2 (en) 2021-02-25 2024-02-20 Marathon Petroleum Company Lp Assemblies and methods for enhancing control of fluid catalytic cracking (FCC) processes using spectroscopic analyzers
KR102888496B1 (ko) 2021-04-28 2025-11-19 에스케이가스 주식회사 상업 화학 공정에서의 공정 핵심 인자 선별을 위한 시스템 및 방법
CN113390821B (zh) * 2021-05-21 2024-04-12 北京中医药大学 一种智能制造炼蜜过程质量的实时监测装备与方法
US11692141B2 (en) 2021-10-10 2023-07-04 Marathon Petroleum Company Lp Methods and systems for enhancing processing of hydrocarbons in a fluid catalytic cracking unit using a renewable additive
US11802257B2 (en) 2022-01-31 2023-10-31 Marathon Petroleum Company Lp Systems and methods for reducing rendered fats pour point
CN114752056B (zh) * 2022-03-02 2024-01-26 双驱智能科技(宁波)有限公司 一种可重复稳定生产窄分子量分布聚芳醚酮的装置及方法
CN115419892A (zh) * 2022-08-11 2022-12-02 陕西卡福纽恩新能源科技有限公司 一种氨气掺氢燃烧的锅炉系统
DE102022131690A1 (de) 2022-11-30 2024-06-06 Carl Freudenberg Kg Verfahren zur thermischen Behandlung eines vorvernetzten Elastomer-Bauteils
US12311305B2 (en) 2022-12-08 2025-05-27 Marathon Petroleum Company Lp Removable flue gas strainer and associated methods
CA3238046A1 (en) 2023-05-12 2025-07-07 Marathon Petroleum Company Lp Systems, apparatuses, and methods for sample cylinder inspection, pressurization, and sample disposal
US12415962B2 (en) 2023-11-10 2025-09-16 Marathon Petroleum Company Lp Systems and methods for producing aviation fuel
CN119354911A (zh) * 2024-12-26 2025-01-24 山东法恩新材料科技有限公司 基于红外光谱橡胶助剂成分分析与质量控制方法及其系统

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3553295A (en) * 1968-04-25 1971-01-05 Shell Oil Co Polymerization monitor
EP0120084A1 (en) * 1982-09-30 1984-10-03 Owens-Corning Fiberglas Corporation Methods and apparatus for measuring and controlling curing of polymeric materials
GB2152713B (en) * 1983-05-12 1987-07-15 Broken Hill Pty Co Ltd Characterizing and handling multi-component substances
US4830757A (en) * 1985-08-06 1989-05-16 The Mogul Corporation Telemetry system for water and energy monitoring
ATE146880T1 (de) 1987-08-18 1997-01-15 Bp Oil Int Verfahren zur direkten bestimmung der physikalischen eigenschaften von kohlenwasserstoffprodukten
ES2041801T3 (es) 1987-08-18 1993-12-01 Bp Oil International Limited Metodo para la determinacion directa de propiedades fisicas de productos hidrocarbonados.
US5116915A (en) * 1987-12-28 1992-05-26 Giprokautchuk Method of controlling polymerization process of olefinic hydrocarbons
FR2625506B1 (fr) 1987-12-31 1992-02-21 Bp Chimie Sa Procede et appareillage de fabrication de polymeres controlee a l'aide d'un systeme de regulation comprenant un spectrophotometre infrarouge
FR2626579B1 (fr) 1988-02-01 1990-06-15 Bp Chimie Sa Procede et appareillage de fabrication de polyoxyalcoylene controlee a l'aide d'un systeme de regulation comprenant un spectrophotometre infrarouge
FR2631957B1 (fr) 1988-05-30 1990-08-31 Bp Chimie Sa Procede et appareillage de fabrication d'olefines et de diolefines par reaction de vapocraquage d'hydrocarbures controlee a l'aide d'un systeme comprenant un spectrophotometre infrarouge
US5132916A (en) * 1990-05-21 1992-07-21 Elsag International B.V. Methodology for ph titration curve estimation for adaptive control
US5121337A (en) * 1990-10-15 1992-06-09 Exxon Research And Engineering Company Method for correcting spectral data for data due to the spectral measurement process itself and estimating unknown property and/or composition data of a sample using such method
MY107650A (en) * 1990-10-12 1996-05-30 Exxon Res & Engineering Company Method of estimating property and / or composition data of a test sample
US5243546A (en) * 1991-01-10 1993-09-07 Ashland Oil, Inc. Spectroscopic instrument calibration
DE4118232A1 (de) 1991-06-04 1992-12-10 Bayer Ag Kontinuierliche herstellung von polycarbonaten
DE4127512C2 (de) 1991-08-20 1995-02-23 Bayer Ag Verfahren zur Herstellung von Polycarbonat mit konstanter Viskosität
CH685003A5 (de) 1992-08-11 1995-02-28 Buehler Ag Verfahren zum kontinuierlichen Kristallisieren und Polymerisieren von Kunststoffmaterial und Vorrichtung hierfür.
EP0706049A1 (en) * 1994-10-07 1996-04-10 Bp Chemicals S.N.C. Cracking property determination
US5532487A (en) * 1994-11-23 1996-07-02 E. I. Du Pont De Nemours And Company Near-infrared measurement and control of polyamide processes

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CN1245570A (zh) 2000-02-23
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NO316346B1 (no) 2004-01-12
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