JP2015500313A5 - - Google Patents
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- Publication number
- JP2015500313A5 JP2015500313A5 JP2014546456A JP2014546456A JP2015500313A5 JP 2015500313 A5 JP2015500313 A5 JP 2015500313A5 JP 2014546456 A JP2014546456 A JP 2014546456A JP 2014546456 A JP2014546456 A JP 2014546456A JP 2015500313 A5 JP2015500313 A5 JP 2015500313A5
- Authority
- JP
- Japan
- Prior art keywords
- hmf
- starting solution
- solution
- steam
- producing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 21
- 239000000243 solution Substances 0.000 claims 13
- NOEGNKMFWQHSLB-UHFFFAOYSA-N 5-hydroxymethylfurfural Chemical compound OCC1=CC=C(C=O)O1 NOEGNKMFWQHSLB-UHFFFAOYSA-N 0.000 claims 11
- RJGBSYZFOCAGQY-UHFFFAOYSA-N hydroxymethylfurfural Natural products COC1=CC=C(C=O)O1 RJGBSYZFOCAGQY-UHFFFAOYSA-N 0.000 claims 11
- 238000006243 chemical reaction Methods 0.000 claims 7
- DSLRVRBSNLHVBH-UHFFFAOYSA-N 2,5-furandimethanol Chemical compound OCC1=CC=C(CO)O1 DSLRVRBSNLHVBH-UHFFFAOYSA-N 0.000 claims 6
- CHTHALBTIRVDBM-UHFFFAOYSA-N furan-2,5-dicarboxylic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)O1 CHTHALBTIRVDBM-UHFFFAOYSA-N 0.000 claims 6
- 238000009835 boiling Methods 0.000 claims 4
- 150000002402 hexoses Chemical class 0.000 claims 3
- 229930091371 Fructose Natural products 0.000 claims 2
- 239000005715 Fructose Substances 0.000 claims 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims 2
- 239000004721 Polyphenylene oxide Substances 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- 239000007864 aqueous solution Substances 0.000 claims 2
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims 2
- 239000008103 glucose Substances 0.000 claims 2
- 229920000570 polyether Polymers 0.000 claims 2
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 claims 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 claims 1
- 238000004821 distillation Methods 0.000 claims 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 1
- BJHIKXHVCXFQLS-UYFOZJQFSA-N fructose group Chemical group OCC(=O)[C@@H](O)[C@H](O)[C@H](O)CO BJHIKXHVCXFQLS-UYFOZJQFSA-N 0.000 claims 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 239000010409 thin film Substances 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP11193157 | 2011-12-13 | ||
| EP11193157.2 | 2011-12-13 | ||
| PCT/EP2012/075055 WO2013087613A1 (de) | 2011-12-13 | 2012-12-11 | Herstellung von 5-hydroxymethylfurfural (hmf) aus hexoselösungen in gegenwart von wasserdampf |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015500313A JP2015500313A (ja) | 2015-01-05 |
| JP2015500313A5 true JP2015500313A5 (enExample) | 2015-02-12 |
| JP6073363B2 JP6073363B2 (ja) | 2017-02-01 |
Family
ID=47458896
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014546456A Expired - Fee Related JP6073363B2 (ja) | 2011-12-13 | 2012-12-11 | スチームの存在下におけるヘキソース溶液からの５−ヒドロキシメチルフルフラール（ｈｍｆ）の調製 |
Country Status (10)
| Country | Link |
|---|---|
| EP (1) | EP2791126B1 (enExample) |
| JP (1) | JP6073363B2 (enExample) |
| KR (1) | KR101970853B1 (enExample) |
| CN (1) | CN104169263B (enExample) |
| BR (1) | BR112014014054B1 (enExample) |
| CA (1) | CA2856864C (enExample) |
| ES (1) | ES2626835T3 (enExample) |
| HU (1) | HUE033363T2 (enExample) |
| RU (1) | RU2014128460A (enExample) |
| WO (1) | WO2013087613A1 (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9156802B2 (en) | 2011-12-13 | 2015-10-13 | Basf Se | Separating off 5-hydroxymethylfurfural (HMF) from reaction solutions by steam distillation |
| DE102016224073A1 (de) * | 2016-12-02 | 2018-06-07 | Südzucker AG | Verbessertes HMF-Herstellungsverfahren |
| CN113825745B (zh) * | 2019-04-15 | 2025-04-04 | 斯道拉恩索公司 | 用于回收溶剂和分离腐殖质材料及其组合物的方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2929823A (en) * | 1956-11-26 | 1960-03-22 | Merck & Co Inc | Production of 5-hydroxymethylfurfural |
| US3201331A (en) * | 1962-10-17 | 1965-08-17 | Atlas Chem Ind | Purification of hydroxymethyl furfural |
| DE3601281A1 (de) | 1986-01-17 | 1987-07-23 | Sueddeutsche Zucker Ag | Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel |
| FR2663933B1 (fr) * | 1990-06-27 | 1994-06-17 | Beghin Say Sa | Nouveau procede de preparation du 5-hydroxymethylfurfural a partir de saccharides. |
| EP1834950A1 (en) | 2006-03-10 | 2007-09-19 | Avantium International B.V. | Method for the synthesis of 5-alkoxymethylfurfural ethers and their use |
| EP1834951A1 (en) | 2006-03-10 | 2007-09-19 | Avantium International B.V. | Method for the synthesis of organic acid esters of 5-hydroxymethylfurfural and their use |
| EP2033958A1 (en) * | 2007-09-07 | 2009-03-11 | Furanix Technologies B.V | Hydroxymethylfurfural ethers from sugars and di- and triols |
| CN101456850A (zh) * | 2007-12-12 | 2009-06-17 | 中国科学院大连化学物理研究所 | 一种制备5-羟甲基糠醛的方法 |
| CN101812039B (zh) * | 2010-05-14 | 2012-09-26 | 天津大学 | 一种利用离子液体催化生成5－羟甲基糠醛的方法 |
| CN102399203B (zh) * | 2011-12-19 | 2014-05-07 | 浙江大学 | 一种离子液体降解碳水化合物制备5-羟甲基糠醛的方法 |
-
2012
- 2012-12-11 CA CA2856864A patent/CA2856864C/en not_active Expired - Fee Related
- 2012-12-11 BR BR112014014054-5A patent/BR112014014054B1/pt not_active IP Right Cessation
- 2012-12-11 ES ES12808306.0T patent/ES2626835T3/es active Active
- 2012-12-11 KR KR1020147019046A patent/KR101970853B1/ko not_active Expired - Fee Related
- 2012-12-11 HU HUE12808306A patent/HUE033363T2/en unknown
- 2012-12-11 WO PCT/EP2012/075055 patent/WO2013087613A1/de not_active Ceased
- 2012-12-11 RU RU2014128460A patent/RU2014128460A/ru not_active Application Discontinuation
- 2012-12-11 EP EP12808306.0A patent/EP2791126B1/de not_active Not-in-force
- 2012-12-11 JP JP2014546456A patent/JP6073363B2/ja not_active Expired - Fee Related
- 2012-12-11 CN CN201280059056.3A patent/CN104169263B/zh not_active Expired - Fee Related
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