CA2856864C - Production of 5-hydroxymethylfurfural (hmf) from hexose solutions in the presence of steam - Google Patents

Production of 5-hydroxymethylfurfural (hmf) from hexose solutions in the presence of steam Download PDF

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Publication number
CA2856864C
CA2856864C CA2856864A CA2856864A CA2856864C CA 2856864 C CA2856864 C CA 2856864C CA 2856864 A CA2856864 A CA 2856864A CA 2856864 A CA2856864 A CA 2856864A CA 2856864 C CA2856864 C CA 2856864C
Authority
CA
Canada
Prior art keywords
hmf
steam
starting solution
hexose
solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CA2856864A
Other languages
English (en)
French (fr)
Other versions
CA2856864A1 (en
Inventor
Rene Backes
Benoit BLANK
Alois Kindler
Carmen FELDNER
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CA2856864A1 publication Critical patent/CA2856864A1/en
Application granted granted Critical
Publication of CA2856864C publication Critical patent/CA2856864C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Furan Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CA2856864A 2011-12-13 2012-12-11 Production of 5-hydroxymethylfurfural (hmf) from hexose solutions in the presence of steam Expired - Fee Related CA2856864C (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11193157 2011-12-13
EP11193157.2 2011-12-13
PCT/EP2012/075055 WO2013087613A1 (de) 2011-12-13 2012-12-11 Herstellung von 5-hydroxymethylfurfural (hmf) aus hexoselösungen in gegenwart von wasserdampf

Publications (2)

Publication Number Publication Date
CA2856864A1 CA2856864A1 (en) 2013-06-20
CA2856864C true CA2856864C (en) 2021-05-25

Family

ID=47458896

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2856864A Expired - Fee Related CA2856864C (en) 2011-12-13 2012-12-11 Production of 5-hydroxymethylfurfural (hmf) from hexose solutions in the presence of steam

Country Status (10)

Country Link
EP (1) EP2791126B1 (enExample)
JP (1) JP6073363B2 (enExample)
KR (1) KR101970853B1 (enExample)
CN (1) CN104169263B (enExample)
BR (1) BR112014014054B1 (enExample)
CA (1) CA2856864C (enExample)
ES (1) ES2626835T3 (enExample)
HU (1) HUE033363T2 (enExample)
RU (1) RU2014128460A (enExample)
WO (1) WO2013087613A1 (enExample)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9156802B2 (en) 2011-12-13 2015-10-13 Basf Se Separating off 5-hydroxymethylfurfural (HMF) from reaction solutions by steam distillation
DE102016224073A1 (de) * 2016-12-02 2018-06-07 Südzucker AG Verbessertes HMF-Herstellungsverfahren
CN113825745B (zh) * 2019-04-15 2025-04-04 斯道拉恩索公司 用于回收溶剂和分离腐殖质材料及其组合物的方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2929823A (en) * 1956-11-26 1960-03-22 Merck & Co Inc Production of 5-hydroxymethylfurfural
US3201331A (en) * 1962-10-17 1965-08-17 Atlas Chem Ind Purification of hydroxymethyl furfural
DE3601281A1 (de) 1986-01-17 1987-07-23 Sueddeutsche Zucker Ag Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel
FR2663933B1 (fr) * 1990-06-27 1994-06-17 Beghin Say Sa Nouveau procede de preparation du 5-hydroxymethylfurfural a partir de saccharides.
EP1834950A1 (en) 2006-03-10 2007-09-19 Avantium International B.V. Method for the synthesis of 5-alkoxymethylfurfural ethers and their use
EP1834951A1 (en) 2006-03-10 2007-09-19 Avantium International B.V. Method for the synthesis of organic acid esters of 5-hydroxymethylfurfural and their use
EP2033958A1 (en) * 2007-09-07 2009-03-11 Furanix Technologies B.V Hydroxymethylfurfural ethers from sugars and di- and triols
CN101456850A (zh) * 2007-12-12 2009-06-17 中国科学院大连化学物理研究所 一种制备5-羟甲基糠醛的方法
CN101812039B (zh) * 2010-05-14 2012-09-26 天津大学 一种利用离子液体催化生成5－羟甲基糠醛的方法
CN102399203B (zh) * 2011-12-19 2014-05-07 浙江大学 一种离子液体降解碳水化合物制备5-羟甲基糠醛的方法

Also Published As

Publication number Publication date
EP2791126A1 (de) 2014-10-22
CA2856864A1 (en) 2013-06-20
BR112014014054B1 (pt) 2019-03-19
RU2014128460A (ru) 2016-02-10
EP2791126B1 (de) 2017-03-01
HUE033363T2 (en) 2017-11-28
CN104169263B (zh) 2016-06-15
WO2013087613A1 (de) 2013-06-20
KR20140101849A (ko) 2014-08-20
JP2015500313A (ja) 2015-01-05
CN104169263A (zh) 2014-11-26
JP6073363B2 (ja) 2017-02-01
KR101970853B1 (ko) 2019-04-19
BR112014014054A2 (pt) 2017-06-13
ES2626835T3 (es) 2017-07-26

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Legal Events

Date Code Title Description
EEER Examination request

Effective date: 20171208

MKLA Lapsed

Effective date: 20211213