JP6073363B2 - スチームの存在下におけるヘキソース溶液からの５−ヒドロキシメチルフルフラール（ｈｍｆ）の調製 - Google Patents

スチームの存在下におけるヘキソース溶液からの５−ヒドロキシメチルフルフラール（ｈｍｆ）の調製 Download PDF

Info

Publication number
JP6073363B2
JP6073363B2 JP2014546456A JP2014546456A JP6073363B2 JP 6073363 B2 JP6073363 B2 JP 6073363B2 JP 2014546456 A JP2014546456 A JP 2014546456A JP 2014546456 A JP2014546456 A JP 2014546456A JP 6073363 B2 JP6073363 B2 JP 6073363B2
Authority
JP
Japan
Prior art keywords
hmf
starting solution
steam
solution
hexose
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2014546456A
Other languages
English (en)
Japanese (ja)
Other versions
JP2015500313A (ja
JP2015500313A5 (enExample
Inventor
バッケス，レーン
ブランク，ベノイト
キンドラー，アロイス
フェルドナー，カルメン
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2015500313A publication Critical patent/JP2015500313A/ja
Publication of JP2015500313A5 publication Critical patent/JP2015500313A5/ja
Application granted granted Critical
Publication of JP6073363B2 publication Critical patent/JP6073363B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Furan Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
JP2014546456A 2011-12-13 2012-12-11 スチームの存在下におけるヘキソース溶液からの５−ヒドロキシメチルフルフラール（ｈｍｆ）の調製 Expired - Fee Related JP6073363B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11193157 2011-12-13
EP11193157.2 2011-12-13
PCT/EP2012/075055 WO2013087613A1 (de) 2011-12-13 2012-12-11 Herstellung von 5-hydroxymethylfurfural (hmf) aus hexoselösungen in gegenwart von wasserdampf

Publications (3)

Publication Number Publication Date
JP2015500313A JP2015500313A (ja) 2015-01-05
JP2015500313A5 JP2015500313A5 (enExample) 2015-02-12
JP6073363B2 true JP6073363B2 (ja) 2017-02-01

Family

ID=47458896

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2014546456A Expired - Fee Related JP6073363B2 (ja) 2011-12-13 2012-12-11 スチームの存在下におけるヘキソース溶液からの５−ヒドロキシメチルフルフラール（ｈｍｆ）の調製

Country Status (10)

Country Link
EP (1) EP2791126B1 (enExample)
JP (1) JP6073363B2 (enExample)
KR (1) KR101970853B1 (enExample)
CN (1) CN104169263B (enExample)
BR (1) BR112014014054B1 (enExample)
CA (1) CA2856864C (enExample)
ES (1) ES2626835T3 (enExample)
HU (1) HUE033363T2 (enExample)
RU (1) RU2014128460A (enExample)
WO (1) WO2013087613A1 (enExample)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9156802B2 (en) 2011-12-13 2015-10-13 Basf Se Separating off 5-hydroxymethylfurfural (HMF) from reaction solutions by steam distillation
DE102016224073A1 (de) * 2016-12-02 2018-06-07 Südzucker AG Verbessertes HMF-Herstellungsverfahren
EP3956319A1 (en) * 2019-04-15 2022-02-23 Stora Enso Oyj Process for the recovery of solvent and isolation of humin materials and compositions thereof

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2929823A (en) * 1956-11-26 1960-03-22 Merck & Co Inc Production of 5-hydroxymethylfurfural
US3201331A (en) * 1962-10-17 1965-08-17 Atlas Chem Ind Purification of hydroxymethyl furfural
DE3601281A1 (de) 1986-01-17 1987-07-23 Sueddeutsche Zucker Ag Verfahren zur herstellung von 5-hydroxymethylfurfural einschliesslich eines kristallinen produktes unter ausschliesslicher verwendung von wasser als loesungsmittel
FR2663933B1 (fr) * 1990-06-27 1994-06-17 Beghin Say Sa Nouveau procede de preparation du 5-hydroxymethylfurfural a partir de saccharides.
EP1834950A1 (en) 2006-03-10 2007-09-19 Avantium International B.V. Method for the synthesis of 5-alkoxymethylfurfural ethers and their use
ATE473218T1 (de) 2006-03-10 2010-07-15 Furanix Technologies Bv Verwendung organischer säureester von 5- hydroxymethylfurfural
EP2033958A1 (en) * 2007-09-07 2009-03-11 Furanix Technologies B.V Hydroxymethylfurfural ethers from sugars and di- and triols
CN101456850A (zh) * 2007-12-12 2009-06-17 中国科学院大连化学物理研究所 一种制备5-羟甲基糠醛的方法
CN101812039B (zh) * 2010-05-14 2012-09-26 天津大学 一种利用离子液体催化生成5－羟甲基糠醛的方法
CN102399203B (zh) * 2011-12-19 2014-05-07 浙江大学 一种离子液体降解碳水化合物制备5-羟甲基糠醛的方法

Also Published As

Publication number Publication date
ES2626835T3 (es) 2017-07-26
HUE033363T2 (en) 2017-11-28
JP2015500313A (ja) 2015-01-05
CN104169263A (zh) 2014-11-26
EP2791126B1 (de) 2017-03-01
KR20140101849A (ko) 2014-08-20
CA2856864C (en) 2021-05-25
BR112014014054A2 (pt) 2017-06-13
RU2014128460A (ru) 2016-02-10
BR112014014054B1 (pt) 2019-03-19
CN104169263B (zh) 2016-06-15
WO2013087613A1 (de) 2013-06-20
KR101970853B1 (ko) 2019-04-19
CA2856864A1 (en) 2013-06-20
EP2791126A1 (de) 2014-10-22

Similar Documents

Publication Publication Date Title
US11028063B2 (en) Processes for producing 2,5-furandicarboxylic acid and derivatives thereof and polymers made therefrom
JP5618983B2 (ja) 二無水糖の製造方法
US9156802B2 (en) Separating off 5-hydroxymethylfurfural (HMF) from reaction solutions by steam distillation
US9169227B2 (en) Production of 5 hydroxymethyulfurfural (HMF) from hexose solutions in the presence of steam
JP6073363B2 (ja) スチームの存在下におけるヘキソース溶液からの５−ヒドロキシメチルフルフラール（ｈｍｆ）の調製
CN103974942A (zh) 在沸点高于60℃且低于200℃(在标准压力下，简称为低沸化合物)存在下由糖溶液制备5-羟甲基糠醛(hmf)
JP6073362B2 (ja) ５−ヒドロキシメチルフルフラール（ｈｍｆ）の水蒸気蒸留による反応溶液からの分離
JP6852263B2 (ja) アンヒドロ糖アルコールの製造方法
JP7686991B2 (ja) アンヒドロ糖アルコールの製造方法
US20250296908A1 (en) Method for separating levulinic acid by thermal separation in the presence of a flux
WO2014087014A1 (en) Process for the preparation of a levulinic acid derived compound

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20140812

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20141203

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20151208

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20160721

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A132

Effective date: 20160809

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20161109

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20161206

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20170104

R150 Certificate of patent or registration of utility model

Ref document number: 6073363

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees