JP2015110778A5 - - Google Patents
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- Publication number
- JP2015110778A5 JP2015110778A5 JP2014252502A JP2014252502A JP2015110778A5 JP 2015110778 A5 JP2015110778 A5 JP 2015110778A5 JP 2014252502 A JP2014252502 A JP 2014252502A JP 2014252502 A JP2014252502 A JP 2014252502A JP 2015110778 A5 JP2015110778 A5 JP 2015110778A5
- Authority
- JP
- Japan
- Prior art keywords
- difluorobenzophenone
- diphenylsulfone
- ppm
- poly
- determined
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- KZTYYGOKRVBIMI-UHFFFAOYSA-N diphenyl sulfone Chemical compound C=1C=CC=CC=1S(=O)(=O)C1=CC=CC=C1 KZTYYGOKRVBIMI-UHFFFAOYSA-N 0.000 claims description 36
- 238000000034 method Methods 0.000 claims description 17
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 14
- 239000012535 impurity Substances 0.000 claims description 14
- -1 silver ions Chemical class 0.000 claims description 6
- 238000004817 gas chromatography Methods 0.000 claims description 3
- LSQARZALBDFYQZ-UHFFFAOYSA-N 4,4'-difluorobenzophenone Chemical compound C1=CC(F)=CC=C1C(=O)C1=CC=C(F)C=C1 LSQARZALBDFYQZ-UHFFFAOYSA-N 0.000 claims 12
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 claims 6
- LKFIWRPOVFNPKR-UHFFFAOYSA-N (2-fluorophenyl)-(4-fluorophenyl)methanone Chemical compound C1=CC(F)=CC=C1C(=O)C1=CC=CC=C1F LKFIWRPOVFNPKR-UHFFFAOYSA-N 0.000 claims 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims 4
- 238000002485 combustion reaction Methods 0.000 claims 4
- 239000000203 mixture Substances 0.000 claims 4
- 229920006260 polyaryletherketone Polymers 0.000 claims 4
- 229920002530 polyetherether ketone Polymers 0.000 claims 4
- 241001550224 Apha Species 0.000 claims 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 3
- 238000004458 analytical method Methods 0.000 claims 3
- 125000003118 aryl group Chemical group 0.000 claims 3
- 239000000460 chlorine Substances 0.000 claims 3
- 229910052801 chlorine Inorganic materials 0.000 claims 3
- 239000012038 nucleophile Substances 0.000 claims 3
- 238000010534 nucleophilic substitution reaction Methods 0.000 claims 3
- 238000004448 titration Methods 0.000 claims 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 2
- 229910052786 argon Inorganic materials 0.000 claims 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 2
- 239000000567 combustion gas Substances 0.000 claims 2
- 239000008367 deionised water Substances 0.000 claims 2
- 229910021641 deionized water Inorganic materials 0.000 claims 2
- LTYMSROWYAPPGB-UHFFFAOYSA-N diphenyl sulfide Chemical compound C=1C=CC=CC=1SC1=CC=CC=C1 LTYMSROWYAPPGB-UHFFFAOYSA-N 0.000 claims 2
- 230000004927 fusion Effects 0.000 claims 2
- 229910000041 hydrogen chloride Inorganic materials 0.000 claims 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 claims 2
- 229910052742 iron Inorganic materials 0.000 claims 2
- 238000004811 liquid chromatography Methods 0.000 claims 2
- 239000001301 oxygen Substances 0.000 claims 2
- 229910052760 oxygen Inorganic materials 0.000 claims 2
- 229910052709 silver Inorganic materials 0.000 claims 2
- 239000004332 silver Substances 0.000 claims 2
- 239000011734 sodium Substances 0.000 claims 2
- 229910052708 sodium Inorganic materials 0.000 claims 2
- 229910000029 sodium carbonate Inorganic materials 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- OGTSHGYHILFRHD-UHFFFAOYSA-N (4-fluorophenyl)-phenylmethanone Chemical compound C1=CC(F)=CC=C1C(=O)C1=CC=CC=C1 OGTSHGYHILFRHD-UHFFFAOYSA-N 0.000 claims 1
- RXNYJUSEXLAVNQ-UHFFFAOYSA-N 4,4'-Dihydroxybenzophenone Chemical compound C1=CC(O)=CC=C1C(=O)C1=CC=C(O)C=C1 RXNYJUSEXLAVNQ-UHFFFAOYSA-N 0.000 claims 1
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 claims 1
- 229920008285 Poly(ether ketone) PEK Polymers 0.000 claims 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- ADUODNZKKNUWBZ-UHFFFAOYSA-N [4-(4-hydroxybenzoyl)phenyl]-(4-hydroxyphenyl)methanone Chemical compound C1=CC(O)=CC=C1C(=O)C1=CC=C(C(=O)C=2C=CC(O)=CC=2)C=C1 ADUODNZKKNUWBZ-UHFFFAOYSA-N 0.000 claims 1
- 238000004380 ashing Methods 0.000 claims 1
- 238000000559 atomic spectroscopy Methods 0.000 claims 1
- VCCBEIPGXKNHFW-UHFFFAOYSA-N biphenyl-4,4'-diol Chemical compound C1=CC(O)=CC=C1C1=CC=C(O)C=C1 VCCBEIPGXKNHFW-UHFFFAOYSA-N 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 claims 1
- 229910052736 halogen Inorganic materials 0.000 claims 1
- 150000002367 halogens Chemical class 0.000 claims 1
- 238000009616 inductively coupled plasma Methods 0.000 claims 1
- 238000005259 measurement Methods 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 1
- 230000014759 maintenance of location Effects 0.000 description 2
- 208000033962 Fontaine progeroid syndrome Diseases 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- 239000001307 helium Substances 0.000 description 1
- 229910052734 helium Inorganic materials 0.000 description 1
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000012488 sample solution Substances 0.000 description 1
Applications Claiming Priority (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US10809708P | 2008-10-24 | 2008-10-24 | |
| US10809608P | 2008-10-24 | 2008-10-24 | |
| US61/108,097 | 2008-10-24 | ||
| US61/108,096 | 2008-10-24 | ||
| US14020508P | 2008-12-23 | 2008-12-23 | |
| US61/140,205 | 2008-12-23 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011532649A Division JP5734859B2 (ja) | 2008-10-24 | 2009-10-23 | 高純度４，４′−ジフルオロベンゾフェノンを使用する、ポリ（アリールエーテルケトン）を製造するための改善された方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015110778A JP2015110778A (ja) | 2015-06-18 |
| JP2015110778A5 true JP2015110778A5 (enExample) | 2016-05-26 |
| JP5985598B2 JP5985598B2 (ja) | 2016-09-06 |
Family
ID=41445399
Family Applications (5)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011532648A Active JP5734858B2 (ja) | 2008-10-24 | 2009-10-23 | 高純度ジフェニルスルホン、調製、およびポリ（アリールエーテルケトン）の調製のためのその使用 |
| JP2011532650A Active JP5606443B2 (ja) | 2008-10-24 | 2009-10-23 | 炭酸ナトリウムの存在下でポリ（アリールエーテルケトン）を製造するための方法 |
| JP2011532649A Active JP5734859B2 (ja) | 2008-10-24 | 2009-10-23 | 高純度４，４′−ジフルオロベンゾフェノンを使用する、ポリ（アリールエーテルケトン）を製造するための改善された方法 |
| JP2014252460A Active JP5933676B2 (ja) | 2008-10-24 | 2014-12-12 | 高純度ジフェニルスルホン、調製、およびポリ（アリールエーテルケトン）の調製のためのその使用 |
| JP2014252502A Active JP5985598B2 (ja) | 2008-10-24 | 2014-12-12 | 高純度４，４′−ジフルオロベンゾフェノンを使用する、ポリ（アリールエーテルケトン）を製造するための改善された方法 |
Family Applications Before (4)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011532648A Active JP5734858B2 (ja) | 2008-10-24 | 2009-10-23 | 高純度ジフェニルスルホン、調製、およびポリ（アリールエーテルケトン）の調製のためのその使用 |
| JP2011532650A Active JP5606443B2 (ja) | 2008-10-24 | 2009-10-23 | 炭酸ナトリウムの存在下でポリ（アリールエーテルケトン）を製造するための方法 |
| JP2011532649A Active JP5734859B2 (ja) | 2008-10-24 | 2009-10-23 | 高純度４，４′−ジフルオロベンゾフェノンを使用する、ポリ（アリールエーテルケトン）を製造するための改善された方法 |
| JP2014252460A Active JP5933676B2 (ja) | 2008-10-24 | 2014-12-12 | 高純度ジフェニルスルホン、調製、およびポリ（アリールエーテルケトン）の調製のためのその使用 |
Country Status (8)
| Country | Link |
|---|---|
| US (7) | US8710171B2 (enExample) |
| EP (5) | EP2342261A1 (enExample) |
| JP (5) | JP5734858B2 (enExample) |
| CN (6) | CN109912794A (enExample) |
| AU (1) | AU2009306298A1 (enExample) |
| CA (3) | CA2740252C (enExample) |
| RU (1) | RU2011120794A (enExample) |
| WO (4) | WO2010046482A1 (enExample) |
Families Citing this family (49)
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| CA2740252C (en) | 2008-10-24 | 2017-05-09 | Solvay Advanced Polymers, L.L.C. | High purity diphenyl sulfone, preparation and use thereof for the preparation of a poly(aryletherketone) |
| CN101580583B (zh) * | 2009-06-26 | 2011-03-30 | 金发科技股份有限公司 | 采用四元共聚技术制备聚芳醚酮类共聚物的方法 |
| CN102471477B (zh) | 2009-07-24 | 2014-09-03 | 因温斯特技术公司 | 使用离子液体的合成方法 |
| JP5316727B1 (ja) * | 2011-09-21 | 2013-10-16 | 東レ株式会社 | 環式ポリフェニレンエーテルエーテルケトン組成物の回収方法およびそれを用いたポリフェニレンエーテルエーテルケトンの製造方法 |
| CN104870519B (zh) * | 2012-12-21 | 2017-11-24 | 东丽株式会社 | 环式聚苯醚醚酮组合物及线状聚苯醚醚酮的制造方法、聚苯醚醚酮的制造方法 |
| JP6221311B2 (ja) * | 2013-04-05 | 2017-11-01 | 東レ株式会社 | ポリフェニレンエーテルエーテルケトンの製造方法 |
| US20160075833A1 (en) * | 2013-05-02 | 2016-03-17 | Basf Se | Polyarylethersulfone copolymers |
| EP2992033B1 (de) * | 2013-05-02 | 2017-03-08 | Basf Se | Polyarylethersulfoncopolymere |
| GB201311376D0 (en) * | 2013-06-26 | 2013-08-14 | Victrex Mfg Ltd | Polymetric Materials |
| GB2526243B (en) | 2014-02-24 | 2021-07-14 | Victrex Mfg Ltd | Polymeric materials |
| GB201409128D0 (en) * | 2014-05-22 | 2014-07-09 | Ketonex Ltd | Method |
| WO2016028614A1 (en) | 2014-08-21 | 2016-02-25 | Ticona Llc | Composition containing a polyaryletherketone and low naphthenic liquid crystalline polymer |
| WO2016028613A1 (en) | 2014-08-21 | 2016-02-25 | Ticona Llc | Polyaryletherketone composition |
| GB201415972D0 (en) | 2014-09-10 | 2014-10-22 | Ketonex Ltd | Process |
| JP6841759B2 (ja) * | 2014-12-19 | 2021-03-10 | メルク パテント ゲゼルシャフト ミット ベシュレンクテル ハフツングＭｅｒｃｋ Ｐａｔｅｎｔ Ｇｅｓｅｌｌｓｃｈａｆｔ ｍｉｔ ｂｅｓｃｈｒａｅｎｋｔｅｒ Ｈａｆｔｕｎｇ | ビメソゲン化合物およびメソゲン性媒体 |
| KR102574669B1 (ko) * | 2015-01-23 | 2023-09-04 | 바스프 에스이 | 용융 추출에 의한 폴리아릴 에테르의 탈염화 |
| US20180009950A1 (en) * | 2015-01-23 | 2018-01-11 | Basf Se | Desalination of polyaryl ethers from a melt polymerization method |
| EP3222651A1 (de) | 2016-03-21 | 2017-09-27 | Basf Se | Entsalzung von polyarylethern mittels schmelzeextraktion |
| WO2018055384A1 (en) * | 2016-09-26 | 2018-03-29 | Victrex Manufacturing Limited | Polymers and process for their manufacture |
| KR102592751B1 (ko) | 2016-11-11 | 2023-10-24 | 솔베이 스페셜티 폴리머즈 유에스에이, 엘.엘.씨. | 폴리아릴에테르 케톤 공중합체 |
| WO2018086873A1 (en) | 2016-11-11 | 2018-05-17 | Solvay Specialty Polymers Usa, Llc | Polyarylether ketone copolymer |
| WO2018115035A1 (en) | 2016-12-21 | 2018-06-28 | Solvay Specialty Polymers Usa, Llc | Poly(ether ketone ketone) polymers, corresponding synthesis methods and polymer compositions and articles made therefrom |
| EP3558918B1 (en) * | 2016-12-21 | 2021-11-10 | Solvay Specialty Polymers USA, LLC | Method for decreasing the concentration of a metal in a monomer composition comprising bis(benzoyl)benzene |
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| EP4286026A1 (en) * | 2022-05-31 | 2023-12-06 | Basf Se | Method for separating an aprotic polar solvent from a mixture comprising water, the aprotic polar solvent and at least one inorganic salt |
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-
2009
- 2009-10-23 CA CA2740252A patent/CA2740252C/en not_active Expired - Fee Related
- 2009-10-23 CN CN201910088673.XA patent/CN109912794A/zh active Pending
- 2009-10-23 CN CN200980142463.9A patent/CN102197064B/zh active Active
- 2009-10-23 JP JP2011532648A patent/JP5734858B2/ja active Active
- 2009-10-23 JP JP2011532650A patent/JP5606443B2/ja active Active
- 2009-10-23 US US13/125,508 patent/US8710171B2/en active Active
- 2009-10-23 CN CN201610339978.XA patent/CN106167545B/zh active Active
- 2009-10-23 EP EP20090744124 patent/EP2342261A1/en not_active Withdrawn
- 2009-10-23 CN CN200980142309.1A patent/CN102203165B/zh active Active
- 2009-10-23 WO PCT/EP2009/064007 patent/WO2010046482A1/en not_active Ceased
- 2009-10-23 EP EP20090737003 patent/EP2344565B1/en active Active
- 2009-10-23 AU AU2009306298A patent/AU2009306298A1/en not_active Abandoned
- 2009-10-23 WO PCT/EP2009/064011 patent/WO2010046484A1/en not_active Ceased
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- 2009-10-23 CN CN200980151189.1A patent/CN102257033B/zh not_active Expired - Fee Related
- 2009-10-23 US US13/125,537 patent/US9175136B2/en active Active
- 2009-10-23 WO PCT/EP2009/064016 patent/WO2010046487A1/en not_active Ceased
- 2009-10-23 EP EP20090740140 patent/EP2342259B1/en not_active Revoked
- 2009-10-23 EP EP20090740326 patent/EP2342260B1/en not_active Revoked
- 2009-10-23 RU RU2011120794/04A patent/RU2011120794A/ru not_active Application Discontinuation
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