JP2014534972A5 - - Google Patents
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- Publication number
- JP2014534972A5 JP2014534972A5 JP2014539381A JP2014539381A JP2014534972A5 JP 2014534972 A5 JP2014534972 A5 JP 2014534972A5 JP 2014539381 A JP2014539381 A JP 2014539381A JP 2014539381 A JP2014539381 A JP 2014539381A JP 2014534972 A5 JP2014534972 A5 JP 2014534972A5
- Authority
- JP
- Japan
- Prior art keywords
- fluid
- rich
- reaction
- octyl acrylate
- recycled
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000012530 fluid Substances 0.000 claims 28
- SJWFXCIHNDVPSH-UHFFFAOYSA-N octan-2-ol Chemical compound CCCCCCC(C)O SJWFXCIHNDVPSH-UHFFFAOYSA-N 0.000 claims 18
- HZLFQUWNZMMHQM-UHFFFAOYSA-N piperazin-1-ylmethanol Chemical compound OCN1CCNCC1 HZLFQUWNZMMHQM-UHFFFAOYSA-N 0.000 claims 14
- 238000004821 distillation Methods 0.000 claims 12
- 238000006243 chemical reaction Methods 0.000 claims 10
- 239000008346 aqueous phase Substances 0.000 claims 9
- 238000000034 method Methods 0.000 claims 9
- 239000011541 reaction mixture Substances 0.000 claims 9
- 239000003054 catalyst Substances 0.000 claims 8
- 238000000926 separation method Methods 0.000 claims 8
- 239000010409 thin film Substances 0.000 claims 8
- 239000006227 byproduct Substances 0.000 claims 6
- 239000012074 organic phase Substances 0.000 claims 6
- 239000007795 chemical reaction product Substances 0.000 claims 5
- 238000000746 purification Methods 0.000 claims 5
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims 4
- 239000003112 inhibitor Substances 0.000 claims 4
- 238000006116 polymerization reaction Methods 0.000 claims 4
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 3
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical group CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 239000010408 film Substances 0.000 claims 2
- 239000012071 phase Substances 0.000 claims 2
- 238000011084 recovery Methods 0.000 claims 2
- 238000004064 recycling Methods 0.000 claims 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 1
- 238000009833 condensation Methods 0.000 claims 1
- 230000005494 condensation Effects 0.000 claims 1
- 238000010924 continuous production Methods 0.000 claims 1
- 230000032050 esterification Effects 0.000 claims 1
- 238000005886 esterification reaction Methods 0.000 claims 1
- 150000002148 esters Chemical class 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 239000012535 impurity Substances 0.000 claims 1
- 229940098779 methanesulfonic acid Drugs 0.000 claims 1
- 238000002156 mixing Methods 0.000 claims 1
- 239000000047 product Substances 0.000 claims 1
- 238000003756 stirring Methods 0.000 claims 1
- 229910052717 sulfur Inorganic materials 0.000 claims 1
- 239000011593 sulfur Substances 0.000 claims 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1159983A FR2982258B1 (fr) | 2011-11-04 | 2011-11-04 | Procede de production d'acrylate de 2-octyle par esterification directe |
| FR1159983 | 2011-11-04 | ||
| FR1256457 | 2012-07-05 | ||
| FR1256457A FR2982259B1 (fr) | 2011-11-04 | 2012-07-05 | Procede de production d'acrylate de 2-octyle par esterification directe |
| PCT/FR2012/052502 WO2013064775A1 (fr) | 2011-11-04 | 2012-10-30 | Procédé de production d'acrylate de 2-octyle par estérification directe |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2014534972A JP2014534972A (ja) | 2014-12-25 |
| JP2014534972A5 true JP2014534972A5 (enExample) | 2015-11-12 |
| JP6043800B2 JP6043800B2 (ja) | 2016-12-14 |
Family
ID=46650816
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014539381A Active JP6043800B2 (ja) | 2011-11-04 | 2012-10-30 | 直接エステル化により２−オクチルアクリラートを製造するための方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US9403750B2 (enExample) |
| EP (1) | EP2773608B1 (enExample) |
| JP (1) | JP6043800B2 (enExample) |
| KR (1) | KR101985985B1 (enExample) |
| CN (1) | CN104024210B (enExample) |
| BR (1) | BR112014010416B1 (enExample) |
| FR (2) | FR2982258B1 (enExample) |
| MY (1) | MY166880A (enExample) |
| SG (1) | SG11201402013YA (enExample) |
| WO (1) | WO2013064775A1 (enExample) |
Families Citing this family (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3024143B1 (fr) * | 2014-07-28 | 2016-07-15 | Arkema France | Procede perfectionne de fabrication de (meth)acrylates d'alkyle |
| JP2019524999A (ja) | 2016-07-18 | 2019-09-05 | ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ | 縮合反応のための低腐食性アルカンスルホン酸 |
| KR102745052B1 (ko) * | 2019-09-27 | 2024-12-23 | 주식회사 엘지화학 | 디에스터계 물질의 정제 유닛 및 이를 포함하는 디에스터계 물질의 정제 시스템 |
| KR102683132B1 (ko) * | 2019-09-27 | 2024-07-10 | 주식회사 엘지화학 | 디에스터계 물질의 정제 유닛 및 이를 포함하는 디에스터계 물질의 정제 시스템 |
| CN113045421A (zh) * | 2019-12-26 | 2021-06-29 | 江苏怡达化学股份有限公司 | 一种己二酸二异丙酯的制备工艺及其设备 |
| CN113045411A (zh) * | 2019-12-26 | 2021-06-29 | 江苏怡达化学股份有限公司 | 一种乙酸正戊酯的制备工艺及其设备 |
| CN113045412A (zh) * | 2019-12-26 | 2021-06-29 | 江苏怡达化学股份有限公司 | 一种己二酸二元酯的制备工艺及其设备 |
| FI4436948T3 (fi) | 2021-11-25 | 2025-10-23 | Basf Se | Menetelmä 2-oktyyli(met)akrylaatin valmistamiseksi |
| EP4335878A1 (en) | 2022-09-07 | 2024-03-13 | Arkema France | Copolymers, compositions and uses thereof |
| KR20250086752A (ko) * | 2022-11-18 | 2025-06-13 | 가부시키가이샤 닛폰 쇼쿠바이 | (메타)아크릴산 에스테르의 제조방법 |
| WO2023249129A2 (ja) | 2022-11-18 | 2023-12-28 | 株式会社日本触媒 | （メタ）アクリル酸エステルの製造方法 |
| EP4638409A1 (de) | 2022-12-21 | 2025-10-29 | Basf Se | Weichmacher-verbindung |
| WO2024153687A1 (de) | 2023-01-19 | 2024-07-25 | Basf Se | Verfahren zur herstellung von 1,2-cyclohexandicarbonsäuredialkylestern |
| FI130915B1 (en) * | 2023-05-22 | 2024-05-27 | Chempolis Oy | Heteroazeotrope extractive distillation process device and method |
Family Cites Families (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19604253A1 (de) * | 1996-02-06 | 1997-08-07 | Basf Ag | Verfahren zur kontinuierlichen Herstellung von Alkylestern der (Meth)acrylsäure |
| DE69812682T2 (de) | 1997-10-31 | 2003-12-18 | Celanese International Corp., Dallas | Entfernung von schwefel aus einem acrylatstrom |
| US6084122A (en) | 1997-10-31 | 2000-07-04 | Celanese International Corporation | Sulfur removal process from an acrylate waste stream |
| DE19851984A1 (de) * | 1998-11-11 | 2000-05-18 | Basf Ag | Verfahren zum Verestern von (Meth)acrylsäure mit einem Alkanol |
| CN1090610C (zh) * | 2000-12-06 | 2002-09-11 | 北京化学工业集团有限责任公司东方化工厂 | 丙烯酸辛酯的生产方法 |
| DE102005010588A1 (de) * | 2005-03-08 | 2006-05-24 | Basf Ag | Verfahren zur Herstellung von Alkylestern der (Meth)acrylsäure |
| JP4160087B2 (ja) * | 2006-07-11 | 2008-10-01 | 株式会社日本触媒 | アクリル酸エステルの製造方法 |
| US7385020B2 (en) * | 2006-10-13 | 2008-06-10 | 3M Innovative Properties Company | 2-octyl (meth)acrylate adhesive composition |
| CN102428065B (zh) * | 2009-05-15 | 2014-02-26 | 株式会社日本触媒 | 制备(甲基)丙烯酸的方法 |
-
2011
- 2011-11-04 FR FR1159983A patent/FR2982258B1/fr not_active Expired - Fee Related
-
2012
- 2012-07-05 FR FR1256457A patent/FR2982259B1/fr not_active Expired - Fee Related
- 2012-10-30 JP JP2014539381A patent/JP6043800B2/ja active Active
- 2012-10-30 KR KR1020147014941A patent/KR101985985B1/ko active Active
- 2012-10-30 SG SG11201402013YA patent/SG11201402013YA/en unknown
- 2012-10-30 EP EP12794403.1A patent/EP2773608B1/fr active Active
- 2012-10-30 MY MYPI2014001293A patent/MY166880A/en unknown
- 2012-10-30 BR BR112014010416-6A patent/BR112014010416B1/pt active IP Right Grant
- 2012-10-30 CN CN201280053578.2A patent/CN104024210B/zh active Active
- 2012-10-30 WO PCT/FR2012/052502 patent/WO2013064775A1/fr not_active Ceased
- 2012-10-30 US US14/354,986 patent/US9403750B2/en active Active
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