JP2014524940A5 - - Google Patents
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- Publication number
- JP2014524940A5 JP2014524940A5 JP2014502874A JP2014502874A JP2014524940A5 JP 2014524940 A5 JP2014524940 A5 JP 2014524940A5 JP 2014502874 A JP2014502874 A JP 2014502874A JP 2014502874 A JP2014502874 A JP 2014502874A JP 2014524940 A5 JP2014524940 A5 JP 2014524940A5
- Authority
- JP
- Japan
- Prior art keywords
- prepreg
- type epoxy
- temperature
- epoxy resin
- curing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003822 epoxy resin Substances 0.000 claims description 41
- 229920000647 polyepoxide Polymers 0.000 claims description 41
- 229920001187 thermosetting polymer Polymers 0.000 claims description 17
- 229920005989 resin Polymers 0.000 claims description 16
- 239000011347 resin Substances 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 11
- PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 claims description 10
- 239000011342 resin composition Substances 0.000 claims description 9
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 claims description 8
- 239000003733 fiber-reinforced composite Substances 0.000 claims description 6
- 239000000463 material Substances 0.000 claims description 6
- CDAWCLOXVUBKRW-UHFFFAOYSA-N 2-aminophenol Chemical compound NC1=CC=CC=C1O CDAWCLOXVUBKRW-UHFFFAOYSA-N 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 229920003986 novolac Polymers 0.000 claims description 3
- VAUOPRZOGIRSMI-UHFFFAOYSA-N n-(oxiran-2-ylmethyl)aniline Chemical compound C1OC1CNC1=CC=CC=C1 VAUOPRZOGIRSMI-UHFFFAOYSA-N 0.000 claims description 2
- 238000001723 curing Methods 0.000 claims 10
- 239000010410 layer Substances 0.000 claims 8
- 238000000465 moulding Methods 0.000 claims 7
- 239000002245 particle Substances 0.000 claims 6
- 230000001186 cumulative effect Effects 0.000 claims 4
- 238000009826 distribution Methods 0.000 claims 3
- 239000011159 matrix material Substances 0.000 claims 3
- 239000012783 reinforcing fiber Substances 0.000 claims 3
- 238000000790 scattering method Methods 0.000 claims 3
- 238000010030 laminating Methods 0.000 claims 2
- 238000007872 degassing Methods 0.000 claims 1
- 239000000835 fiber Substances 0.000 claims 1
- 238000001879 gelation Methods 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 238000005470 impregnation Methods 0.000 claims 1
- 239000011229 interlayer Substances 0.000 claims 1
- 150000002924 oxiranes Chemical class 0.000 claims 1
- 229920005992 thermoplastic resin Polymers 0.000 claims 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 18
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- QTWJRLJHJPIABL-UHFFFAOYSA-N 2-methylphenol;3-methylphenol;4-methylphenol Chemical compound CC1=CC=C(O)C=C1.CC1=CC=CC(O)=C1.CC1=CC=CC=C1O QTWJRLJHJPIABL-UHFFFAOYSA-N 0.000 description 3
- 150000001412 amines Chemical class 0.000 description 3
- 229930003836 cresol Natural products 0.000 description 3
- 239000002243 precursor Substances 0.000 description 3
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 2
- IGALFTFNPPBUDN-UHFFFAOYSA-N phenyl-[2,3,4,5-tetrakis(oxiran-2-ylmethyl)phenyl]methanediamine Chemical compound C=1C(CC2OC2)=C(CC2OC2)C(CC2OC2)=C(CC2OC2)C=1C(N)(N)C1=CC=CC=C1 IGALFTFNPPBUDN-UHFFFAOYSA-N 0.000 description 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
- PUFWGUZSDHANBX-UHFFFAOYSA-N 1-phenyl-9h-fluorene Chemical compound C=12CC3=CC=CC=C3C2=CC=CC=1C1=CC=CC=C1 PUFWGUZSDHANBX-UHFFFAOYSA-N 0.000 description 1
- HECLRDQVFMWTQS-RGOKHQFPSA-N 1755-01-7 Chemical compound C1[C@H]2[C@@H]3CC=C[C@@H]3[C@@H]1C=C2 HECLRDQVFMWTQS-RGOKHQFPSA-N 0.000 description 1
- FLROJJGKUKLCAE-UHFFFAOYSA-N 3-amino-2-methylphenol Chemical compound CC1=C(N)C=CC=C1O FLROJJGKUKLCAE-UHFFFAOYSA-N 0.000 description 1
- VPWNQTHUCYMVMZ-UHFFFAOYSA-N 4,4'-sulfonyldiphenol Chemical compound C1=CC(O)=CC=C1S(=O)(=O)C1=CC=C(O)C=C1 VPWNQTHUCYMVMZ-UHFFFAOYSA-N 0.000 description 1
- CXXSQMDHHYTRKY-UHFFFAOYSA-N 4-amino-2,3,5-tris(oxiran-2-ylmethyl)phenol Chemical compound C1=C(O)C(CC2OC2)=C(CC2OC2)C(N)=C1CC1CO1 CXXSQMDHHYTRKY-UHFFFAOYSA-N 0.000 description 1
- 229920000049 Carbon (fiber) Polymers 0.000 description 1
- 235000010290 biphenyl Nutrition 0.000 description 1
- 239000004305 biphenyl Substances 0.000 description 1
- 239000004917 carbon fiber Substances 0.000 description 1
- 239000011203 carbon fibre reinforced carbon Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical compound C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 description 1
- 150000002118 epoxides Chemical class 0.000 description 1
- 230000020169 heat generation Effects 0.000 description 1
- 125000001624 naphthyl group Chemical group 0.000 description 1
- AFEQENGXSMURHA-UHFFFAOYSA-N oxiran-2-ylmethanamine Chemical compound NCC1CO1 AFEQENGXSMURHA-UHFFFAOYSA-N 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161469529P | 2011-03-30 | 2011-03-30 | |
| US61/469,529 | 2011-03-30 | ||
| US201261586232P | 2012-01-13 | 2012-01-13 | |
| US61/586,232 | 2012-01-13 | ||
| PCT/US2012/031672 WO2012135754A1 (en) | 2011-03-30 | 2012-03-30 | Prepreg, fiber reinforced composite material, and manufacturing method for fiber reinforced composite material |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2014524940A JP2014524940A (ja) | 2014-09-25 |
| JP2014524940A5 true JP2014524940A5 (https=) | 2015-04-09 |
| JP5971325B2 JP5971325B2 (ja) | 2016-08-17 |
Family
ID=46931959
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014502874A Active JP5971325B2 (ja) | 2011-03-30 | 2012-03-30 | プリプレグ、繊維強化複合材料、および繊維強化複合材料の製造方法 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US20140087178A1 (https=) |
| EP (1) | EP2691199B1 (https=) |
| JP (1) | JP5971325B2 (https=) |
| KR (1) | KR101951058B1 (https=) |
| CN (1) | CN103429371B (https=) |
| BR (1) | BR112013024886A2 (https=) |
| CA (1) | CA2830836A1 (https=) |
| RU (1) | RU2013148117A (https=) |
| WO (1) | WO2012135754A1 (https=) |
Families Citing this family (47)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2641004C2 (ru) * | 2012-11-15 | 2018-01-15 | Сайтек Индастриз Инк. | Композиционные материалы из термореактивной смолы, содержащие межслойные повышающие ударопрочность частицы |
| US9205633B2 (en) * | 2013-03-15 | 2015-12-08 | Henkel IP & Holding GmbH | Prepreg curing process for preparing composites having superior surface finish and high fiber consolidation |
| KR20150135270A (ko) * | 2013-03-29 | 2015-12-02 | 제이엑스 닛코닛세키에너지주식회사 | 섬유 강화 복합 재료의 제조 방법 |
| WO2015083820A1 (ja) * | 2013-12-06 | 2015-06-11 | 三菱レイヨン株式会社 | 繊維強化熱可塑性プラスチックを用いた積層基材とこれを用いた成形品の製造方法 |
| JP6210007B2 (ja) * | 2014-03-26 | 2017-10-11 | 東レ株式会社 | プリプレグおよびその製造方法、ならびに炭素繊維強化複合材料 |
| WO2015160468A1 (en) * | 2014-04-14 | 2015-10-22 | Dow Global Technologies Llc | Epoxy resin compositions for pre-gel ovens |
| JP6733178B2 (ja) * | 2014-09-19 | 2020-07-29 | 東レ株式会社 | 繊維強化プラスチックの製造方法 |
| US9587076B2 (en) * | 2014-09-23 | 2017-03-07 | The Boeing Company | Polymer nanoparticles for controlling resin reaction rates |
| US10808123B2 (en) | 2014-09-23 | 2020-10-20 | The Boeing Company | Nanoparticles for improving the dimensional stability of resins |
| US10662302B2 (en) * | 2014-09-23 | 2020-05-26 | The Boeing Company | Polymer nanoparticles for improved distortion capability in composites |
| US10472472B2 (en) | 2014-09-23 | 2019-11-12 | The Boeing Company | Placement of modifier material in resin-rich pockets to mitigate microcracking in a composite structure |
| US10072126B2 (en) | 2014-09-23 | 2018-09-11 | The Boeing Company | Soluble nanoparticles for composite performance enhancement |
| US10011695B2 (en) | 2015-01-07 | 2018-07-03 | Toray Industries, Inc. | Prepreg |
| US10479029B2 (en) * | 2015-01-16 | 2019-11-19 | The Boeing Company | Composite forming apparatus |
| US10201959B2 (en) | 2015-01-30 | 2019-02-12 | The Boeing Company | Gradient curing of composite laminate parts |
| US20170021596A1 (en) * | 2015-05-05 | 2017-01-26 | Sunrez Corp. | Fiber Reinforced Core |
| CN104875790A (zh) * | 2015-05-26 | 2015-09-02 | 北京汽车股份有限公司 | 一种车顶盖及车顶盖的加工方法 |
| CN108137839B (zh) * | 2015-12-16 | 2021-07-06 | 东丽株式会社 | 预浸料坯、层压体、纤维增强复合材料、及纤维增强复合材料的制造方法 |
| CN105415775A (zh) * | 2015-12-30 | 2016-03-23 | 联想(北京)有限公司 | 碳纤维板和电子设备 |
| CN105907062B (zh) * | 2016-05-10 | 2018-01-02 | 中南林业科技大学 | 高强低密度天然植物纤维增强聚己内酯复合材料及其制备方法 |
| CA3025499A1 (en) * | 2016-05-26 | 2017-11-30 | Hanwha Azdel, Inc. | Prepregs, cores and composite articles including powder coated layers |
| US10472474B2 (en) | 2016-06-22 | 2019-11-12 | Hexcel Corporation | Semipreg with thermoplastic toughened novolac-based epoxy resin matrix |
| WO2018066600A1 (ja) * | 2016-10-04 | 2018-04-12 | 三菱ケミカル株式会社 | プリプレグ、プリプレグ積層体、および繊維強化複合材料 |
| KR102362050B1 (ko) * | 2016-10-26 | 2022-02-11 | 도레이 카부시키가이샤 | 프리프레그 적층체, 섬유 강화 복합 재료 및 섬유 강화 복합 재료의 제조 방법 |
| US20200230843A1 (en) * | 2016-10-26 | 2020-07-23 | Standardgraphene Co., Ltd. | Carbon fiber prepreg or carbon fiber-reinforced plastic, and interior and exterior material comprising same |
| KR20190127685A (ko) * | 2017-03-29 | 2019-11-13 | 도레이 카부시키가이샤 | 프리프레그 및 섬유 강화 복합 재료 |
| KR101951629B1 (ko) * | 2017-05-30 | 2019-02-25 | 주식회사 한국카본 | 내마모성이 우수한 얇은 폭 프리프레그, 이를 이용한 프리프레그 직물 및 이의 제조방법 |
| CN109134900B (zh) * | 2017-06-27 | 2022-06-07 | 深圳光启高等理工研究院 | 一种预浸料及其制备方法 |
| TR201722409A2 (tr) | 2017-12-28 | 2019-07-22 | Kordsa Teknik Tekstil As | Yüzey örtüsü ve yüzey fi̇lmi̇yle entegre prepreg tabakasi ve bunun üreti̇mi̇ i̇çi̇n i̇şlemler |
| EP3746500B1 (en) * | 2018-01-31 | 2026-04-15 | Toray Industries, Inc. | Prepreg sheets and prepreg stacks useful for preparing low void content fiber-reinforced compostite materials |
| JP7209470B2 (ja) | 2018-03-13 | 2023-01-20 | 帝人株式会社 | プリプレグ及び炭素繊維強化複合材料 |
| JP7283382B2 (ja) * | 2018-03-30 | 2023-05-30 | 東レ株式会社 | 成形品および成形品の製造方法 |
| JP6699803B1 (ja) * | 2018-06-26 | 2020-05-27 | 東レ株式会社 | プリプレグおよびその製造方法、スリットテーププリプレグ、炭素繊維強化複合材料 |
| CN112292419A (zh) * | 2018-06-26 | 2021-01-29 | 东丽株式会社 | 预浸料坯及其制造方法、分切带预浸料坯、碳纤维增强复合材料 |
| JP7140131B2 (ja) * | 2018-08-22 | 2022-09-21 | 東レ株式会社 | 離型シート付き多層構造プリプレグ、プリプレグロール、プリプレグテープおよび複合材料 |
| CN109263089B (zh) * | 2018-09-26 | 2021-01-01 | 牧世复合材料科技(苏州)有限公司 | 一种通过纤维增强树脂拉挤工艺制备夹芯型材的方法及所得型材 |
| JP2020101195A (ja) * | 2018-12-20 | 2020-07-02 | 本田技研工業株式会社 | 圧力容器及びその製造方法 |
| EP3974142A4 (en) * | 2019-05-23 | 2023-06-14 | Toray Industries, Inc. | PROCESS FOR THE MANUFACTURE OF A FIBER-REINFORCED RESIN SUBSTRATE, FIBER-REINFORCED RESIN SUBSTRATE AND MOLDING ARTICLES EQUIPPED THEREWITH |
| JP7803040B2 (ja) * | 2019-12-11 | 2026-01-21 | 東レ株式会社 | プリプレグ、積層体および一体化成形品 |
| EP4074766A4 (en) | 2019-12-11 | 2023-12-27 | Toray Industries, Inc. | PREPREG, LAMINATE AND INTEGRATED MOLDING |
| RU2751337C1 (ru) * | 2020-11-27 | 2021-07-13 | Акционерное общество "Научно-исследовательский институт конструкционных материалов на основе графита "НИИграфит" | Антифрикционная композиция и способ её получения |
| CN113307643B (zh) * | 2021-06-02 | 2022-10-21 | 中国航空制造技术研究院 | 一种基于单向带SiCf/SiC复合材料制备方法 |
| US12600109B2 (en) * | 2021-07-27 | 2026-04-14 | Toray Industries, Inc. | Carbon fiber-reinforced composite material |
| CN113882090B (zh) * | 2021-11-02 | 2023-01-06 | 天津工业大学 | 基于单边缝合工艺的三维复合材料预制体制备方法及装置 |
| CN115256796B (zh) * | 2022-09-27 | 2022-12-09 | 四川纤谷塑业有限公司 | 一种玄武岩纤维复合材料的成型工艺 |
| CN115819973B (zh) * | 2022-11-04 | 2023-10-20 | 航天特种材料及工艺技术研究所 | 一种大尺寸连续气凝胶卷材快速复合制备方法 |
| TR2023016248A2 (tr) * | 2023-12-01 | 2023-12-21 | Cukurova Ueniversitesi Rektoerluegue | Hava ve uzay araçlarinda kullanilan kompozi̇t uygulamalari i̇çi̇n yüksek dayanimli elyafla bi̇rli̇kte monofi̇lament i̇pli̇k i̇çeren ara katmanlar |
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| US4590122A (en) | 1980-12-18 | 1986-05-20 | Fiberite Corporation | High conductivity graphite material with electrically conductive filaments wrapped around warp and fill elements |
| CA2056034C (en) * | 1990-11-29 | 2001-04-17 | Toshihiro Hattori | Prepregs, process for producing the same and laminates produced with the same |
| JPH06240022A (ja) * | 1993-02-19 | 1994-08-30 | Dainippon Ink & Chem Inc | プリプレグ |
| JP3150901B2 (ja) * | 1996-03-22 | 2001-03-26 | 東邦レーヨン株式会社 | 木材強化用炭素繊維プリプレグおよび炭素繊維強化木材 |
| JPH10231372A (ja) | 1996-12-18 | 1998-09-02 | Toray Ind Inc | プリプレグおよびその製造方法 |
| US6139942A (en) * | 1997-02-06 | 2000-10-31 | Cytec Technology, Inc. | Resin composition, a fiber reinforced material having a partially impregnated resin and composites made therefrom |
| TW467940B (en) * | 1997-10-14 | 2001-12-11 | Toray Industries | Thermosetting resin composition for carbon-fiber reinforced composite material |
| EP1408084B1 (en) | 1998-05-20 | 2009-10-28 | Cytec Technology Corporation | Epoxy resin compositions for the manufacture of void-free laminates |
| GB9907204D0 (en) * | 1999-03-30 | 1999-05-26 | Woolstencroft David H | A composite |
| JP2004182923A (ja) * | 2002-12-05 | 2004-07-02 | Mitsubishi Rayon Co Ltd | プリプレグ及びそれを用いた繊維強化複合材料の製造方法 |
| JP4177041B2 (ja) * | 2002-07-18 | 2008-11-05 | 三菱レイヨン株式会社 | 繊維強化複合材料の製造方法 |
| ES2527168T3 (es) * | 2002-07-18 | 2015-01-21 | Mitsubishi Rayon Co., Ltd. | Preimpregnado y procedimientos para la producción de materiales compuestos reforzados con fibras |
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| JP2009511297A (ja) * | 2005-10-11 | 2009-03-19 | シーアールシー フォー アドバンスト コンポジット ストラクチャーズ リミテッド | 乾燥強化繊維の結合方法 |
| JP4969363B2 (ja) * | 2006-08-07 | 2012-07-04 | 東レ株式会社 | プリプレグおよび炭素繊維強化複合材料 |
| GB0619401D0 (en) * | 2006-10-02 | 2006-11-08 | Hexcel Composites Ltd | Composite materials with improved performance |
| KR101519951B1 (ko) * | 2007-04-17 | 2015-05-13 | 헥셀 코포레이션 | 개선된 성능을 갖는 사전-함침된 복합 재료 |
| MY145926A (en) * | 2007-04-17 | 2012-05-31 | Hexcel Corp | Composite material with blend of thermoplastic particles |
| GB0717507D0 (en) | 2007-09-07 | 2007-10-17 | Cytec Tech Corp | Composite materials and their use |
| ES2395741T3 (es) * | 2008-09-30 | 2013-02-14 | Hexcel Composites, Ltd. | Material semi-impregnado con una pelicula de resina de superficie potenciadora y mejoradora de las propiedades del mismo |
| BRPI0919688B1 (pt) | 2008-10-22 | 2019-04-02 | Cytec Technology Corp. | Método para formar prepregs conformados com componentes voláteis reduzidos |
| WO2010099029A1 (en) | 2009-02-27 | 2010-09-02 | Cytec Technology Corp. | Epoxy compositions with improved mechanical performance |
-
2012
- 2012-03-30 KR KR1020137026543A patent/KR101951058B1/ko not_active Expired - Fee Related
- 2012-03-30 US US14/009,045 patent/US20140087178A1/en not_active Abandoned
- 2012-03-30 BR BR112013024886A patent/BR112013024886A2/pt not_active IP Right Cessation
- 2012-03-30 EP EP12765220.4A patent/EP2691199B1/en active Active
- 2012-03-30 CN CN201280011819.7A patent/CN103429371B/zh not_active Expired - Fee Related
- 2012-03-30 RU RU2013148117/05A patent/RU2013148117A/ru not_active Application Discontinuation
- 2012-03-30 WO PCT/US2012/031672 patent/WO2012135754A1/en not_active Ceased
- 2012-03-30 JP JP2014502874A patent/JP5971325B2/ja active Active
- 2012-03-30 CA CA 2830836 patent/CA2830836A1/en not_active Abandoned
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