JP2013535455A5 - - Google Patents
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- Publication number
- JP2013535455A5 JP2013535455A5 JP2013521074A JP2013521074A JP2013535455A5 JP 2013535455 A5 JP2013535455 A5 JP 2013535455A5 JP 2013521074 A JP2013521074 A JP 2013521074A JP 2013521074 A JP2013521074 A JP 2013521074A JP 2013535455 A5 JP2013535455 A5 JP 2013535455A5
- Authority
- JP
- Japan
- Prior art keywords
- dmapn
- reaction
- range
- dmapa
- hydrogenation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- MTPJEFOSTIKRSS-UHFFFAOYSA-N 3-(dimethylamino)propanenitrile Chemical compound CN(C)CCC#N MTPJEFOSTIKRSS-UHFFFAOYSA-N 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 description 6
- KFYRJJBUHYILSO-YFKPBYRVSA-N (2s)-2-amino-3-dimethylarsanylsulfanyl-3-methylbutanoic acid Chemical compound C[As](C)SC(C)(C)[C@@H](N)C(O)=O KFYRJJBUHYILSO-YFKPBYRVSA-N 0.000 description 3
- 238000005984 hydrogenation reaction Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000003054 catalyst Substances 0.000 description 2
- 238000006722 reduction reaction Methods 0.000 description 2
- 238000000746 purification Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP10171187 | 2010-07-29 | ||
| EP10171187.7 | 2010-07-29 | ||
| PCT/EP2011/062496 WO2012013563A1 (de) | 2010-07-29 | 2011-07-21 | Dmapn mit niedrigem dgn-gehalt und ein verfahren zur herstellung von dmapa aus dmapn mit niedrigem dgn-gehalt |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013535455A JP2013535455A (ja) | 2013-09-12 |
| JP2013535455A5 true JP2013535455A5 (OSRAM) | 2015-07-30 |
| JP5980206B2 JP5980206B2 (ja) | 2016-08-31 |
Family
ID=43127415
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013521074A Expired - Fee Related JP5980206B2 (ja) | 2010-07-29 | 2011-07-21 | 低い２−（ジメチルアミノメチル）−グルタロニトリル（ｄｇｎ）含量を有する３−ジメチルアミノプリオニトリル（ｄｍａｐｎ）および低い２−（ジメチルアミノメチル）−グルタロニトリル（ｄｇｎ）含量を有する３−ジメチルアミノプロピオニトリル（ｄｍａｐｎ）から３−ジメチルアミノプロピルアミン（ｄｍａｐａ）を製造する方法 |
Country Status (6)
| Country | Link |
|---|---|
| EP (1) | EP2412698B1 (OSRAM) |
| JP (1) | JP5980206B2 (OSRAM) |
| CN (1) | CN103124716B (OSRAM) |
| BR (1) | BR112013002105B1 (OSRAM) |
| ES (1) | ES2394680T3 (OSRAM) |
| WO (1) | WO2012013563A1 (OSRAM) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8981093B2 (en) | 2012-06-06 | 2015-03-17 | Basf Se | Process for preparing piperazine |
| CN102993047B (zh) * | 2012-09-19 | 2014-09-24 | 济南大学 | 快速高选择性硫化氢比色探针 |
| CN109970574B (zh) * | 2019-04-11 | 2022-04-15 | 中北大学 | 一种n,n-二异丙基-1,3-丙二胺的制备方法 |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DD58306A (OSRAM) | ||||
| DE2709966C2 (de) * | 1977-03-08 | 1979-04-12 | Ruhrchemie Ag, 4200 Oberhausen | Verfahren zur Herstellung von ß- Dimethylaminopropionitril |
| DD222011A1 (de) | 1983-11-15 | 1985-05-08 | Schwarzheide Synthesewerk Veb | Verfahren und vorrichtung zur kontinuierlichen herstellung von 3(n,n-dimethylamino)propionitril |
| DE4325847A1 (de) | 1993-07-31 | 1995-02-02 | Basf Ag | Kobaltkatalysatoren |
| EP0742045B1 (de) | 1995-05-09 | 2001-12-12 | Basf Aktiengesellschaft | Kobaltkatalysatoren |
| DE10100314A1 (de) * | 2001-01-05 | 2002-07-11 | Basf Ag | Verfahren zur Herstellung von sekundären Aminen aus Nitrilen |
| DE10152135A1 (de) | 2001-10-23 | 2003-04-30 | Basf Ag | Cobalt-Trägerkatalysatoren für Nitrilhydrierungen |
| AU2003299603A1 (en) * | 2002-12-23 | 2004-07-29 | Ascend Performance Materials Llc | Low pressure process for manufacture of 3-dimethylaminopropylamine (dmapa) |
| US6660887B1 (en) * | 2002-12-23 | 2003-12-09 | Solutia Inc. | Low pressure process for manufacture of 3-dimethylaminopropylamine (DMAPA) |
| DE102005004853A1 (de) * | 2005-02-01 | 2006-08-03 | Basf Ag | Verfahren zur Herstellung von Bis-[(3-Dimethylamino)propyl]amin (BisDMAPA) |
| DE102005052457A1 (de) | 2005-11-03 | 2007-05-10 | Basf Ag | Verfahren zur Synthese von DMAPA |
| WO2007104663A1 (de) * | 2006-03-10 | 2007-09-20 | Basf Se | Mischoxid-katalysatoren |
| CN102746186B (zh) * | 2006-05-09 | 2016-01-20 | 巴斯夫欧洲公司 | 制备氨烷基腈和由该腈制备二胺的方法 |
| FR2971248B1 (fr) * | 2011-02-04 | 2013-08-16 | Rhodia Operations | Preparation de diamine via la preparation d'aminonitrile |
-
2011
- 2011-07-21 ES ES11174776T patent/ES2394680T3/es active Active
- 2011-07-21 WO PCT/EP2011/062496 patent/WO2012013563A1/de not_active Ceased
- 2011-07-21 EP EP20110174776 patent/EP2412698B1/de active Active
- 2011-07-21 BR BR112013002105-5A patent/BR112013002105B1/pt not_active IP Right Cessation
- 2011-07-21 CN CN201180046977.1A patent/CN103124716B/zh active Active
- 2011-07-21 JP JP2013521074A patent/JP5980206B2/ja not_active Expired - Fee Related
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