CN103124716B - 具有低dgn含量的dmapn和从具有低dgn含量的dmapn制备dmapa的方法 - Google Patents

具有低dgn含量的dmapn和从具有低dgn含量的dmapn制备dmapa的方法 Download PDF

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Publication number
CN103124716B
CN103124716B CN201180046977.1A CN201180046977A CN103124716B CN 103124716 B CN103124716 B CN 103124716B CN 201180046977 A CN201180046977 A CN 201180046977A CN 103124716 B CN103124716 B CN 103124716B
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China
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dmapn
methylaminopropionitrile
dmpm
low
temperature
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Chinese (zh)
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CN103124716A (zh
Inventor
W·马格莱恩
J·埃伯哈特
J-P·梅尔德
U·克勒
T·哈恩
M·克赖奇曼
D·赫布雷克特
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/84—Purification
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00—Preparation of carboxylic acid nitriles
    • C07C253/30—Preparation of carboxylic acid nitriles by reactions not involving the formation of cyano groups

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201180046977.1A 2010-07-29 2011-07-21 具有低dgn含量的dmapn和从具有低dgn含量的dmapn制备dmapa的方法 Active CN103124716B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP10171187.7 2010-07-29
EP10171187 2010-07-29
PCT/EP2011/062496 WO2012013563A1 (de) 2010-07-29 2011-07-21 Dmapn mit niedrigem dgn-gehalt und ein verfahren zur herstellung von dmapa aus dmapn mit niedrigem dgn-gehalt

Publications (2)

Publication Number Publication Date
CN103124716A CN103124716A (zh) 2013-05-29
CN103124716B true CN103124716B (zh) 2014-11-05

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ID=43127415

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CN201180046977.1A Active CN103124716B (zh) 2010-07-29 2011-07-21 具有低dgn含量的dmapn和从具有低dgn含量的dmapn制备dmapa的方法

Country Status (6)

Country Link
EP (1) EP2412698B1 (OSRAM)
JP (1) JP5980206B2 (OSRAM)
CN (1) CN103124716B (OSRAM)
BR (1) BR112013002105B1 (OSRAM)
ES (1) ES2394680T3 (OSRAM)
WO (1) WO2012013563A1 (OSRAM)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8981093B2 (en) 2012-06-06 2015-03-17 Basf Se Process for preparing piperazine
CN103018237B (zh) * 2012-09-19 2014-09-24 济南大学 快速高选择性硫化氢比色探针的应用
CN109970574B (zh) * 2019-04-11 2022-04-15 中北大学 一种n,n-二异丙基-1,3-丙二胺的制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1367164A (zh) * 2001-01-05 2002-09-04 巴斯福股份公司 由腈制备仲胺的方法
WO2004060039A2 (en) * 2002-12-23 2004-07-22 Solutia, Inc Low pressure process for manufacture of 3-dimethylaminopropylamine (dmapa)
WO2006082202A1 (de) * 2005-02-01 2006-08-10 Basf Aktiengesellschaft Verfahren zur herstellung von bis-[(3-dimethylamino)propyl]amin (bisdmapa)
WO2007128803A1 (de) * 2006-05-09 2007-11-15 Basf Se Verfahren zur herstellung von aminoalkylnitrilen und diaminen aus solchen nitrilen
CN101400442A (zh) * 2006-03-10 2009-04-01 巴斯夫欧洲公司 混合氧化物催化剂

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DD58306A (OSRAM)
DE2709966C2 (de) 1977-03-08 1979-04-12 Ruhrchemie Ag, 4200 Oberhausen Verfahren zur Herstellung von ß- Dimethylaminopropionitril
DD222011A1 (de) 1983-11-15 1985-05-08 Schwarzheide Synthesewerk Veb Verfahren und vorrichtung zur kontinuierlichen herstellung von 3(n,n-dimethylamino)propionitril
DE4325847A1 (de) 1993-07-31 1995-02-02 Basf Ag Kobaltkatalysatoren
EP0742045B1 (de) 1995-05-09 2001-12-12 Basf Aktiengesellschaft Kobaltkatalysatoren
DE10152135A1 (de) 2001-10-23 2003-04-30 Basf Ag Cobalt-Trägerkatalysatoren für Nitrilhydrierungen
EP1575897A4 (en) * 2002-12-23 2007-03-14 Solutia Inc LOW-PRESSURE PROCESS FOR PREPARING 3-DIMETHYLAMINOPROPYLAMINE (DMAPA)
DE102005052457A1 (de) * 2005-11-03 2007-05-10 Basf Ag Verfahren zur Synthese von DMAPA
FR2971248B1 (fr) * 2011-02-04 2013-08-16 Rhodia Operations Preparation de diamine via la preparation d'aminonitrile

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1367164A (zh) * 2001-01-05 2002-09-04 巴斯福股份公司 由腈制备仲胺的方法
WO2004060039A2 (en) * 2002-12-23 2004-07-22 Solutia, Inc Low pressure process for manufacture of 3-dimethylaminopropylamine (dmapa)
WO2006082202A1 (de) * 2005-02-01 2006-08-10 Basf Aktiengesellschaft Verfahren zur herstellung von bis-[(3-dimethylamino)propyl]amin (bisdmapa)
CN101400442A (zh) * 2006-03-10 2009-04-01 巴斯夫欧洲公司 混合氧化物催化剂
WO2007128803A1 (de) * 2006-05-09 2007-11-15 Basf Se Verfahren zur herstellung von aminoalkylnitrilen und diaminen aus solchen nitrilen

Also Published As

Publication number Publication date
BR112013002105B1 (pt) 2019-04-30
WO2012013563A1 (de) 2012-02-02
BR112013002105A2 (pt) 2016-05-24
JP5980206B2 (ja) 2016-08-31
ES2394680T3 (es) 2013-02-04
JP2013535455A (ja) 2013-09-12
CN103124716A (zh) 2013-05-29
EP2412698A1 (de) 2012-02-01
EP2412698B1 (de) 2012-11-21

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