JP2013502391A - ３−ジブチルラミノ−６−メチル−７−アニリノフルオランの製造方法 - Google Patents

３−ジブチルラミノ−６−メチル−７−アニリノフルオランの製造方法 Download PDF

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Publication number
JP2013502391A
JP2013502391A JP2012525122A JP2012525122A JP2013502391A JP 2013502391 A JP2013502391 A JP 2013502391A JP 2012525122 A JP2012525122 A JP 2012525122A JP 2012525122 A JP2012525122 A JP 2012525122A JP 2013502391 A JP2013502391 A JP 2013502391A
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JP
Japan
Prior art keywords
mixture
sulfuric acid
temperature
organic phase
reaction
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
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JP2012525122A
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English (en)
Japanese (ja)
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JP2013502391A5 (https=
Inventor
モンゴメリー オニール ロバート
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BASF SE
Original Assignee
BASF SE
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Application filed by BASF SE filed Critical BASF SE
Publication of JP2013502391A publication Critical patent/JP2013502391A/ja
Publication of JP2013502391A5 publication Critical patent/JP2013502391A5/ja
Withdrawn legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D493/00—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system
    • C07D493/02—Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system in which the condensed system contains two hetero rings
    • C07D493/10—Spiro-condensed systems
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B11/00—Diaryl- or thriarylmethane dyes
    • C09B11/28—Pyronines ; Xanthon, thioxanthon, selenoxanthan, telluroxanthon dyes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
    • C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
    • C09B67/0025—Crystal modifications; Special X-ray patterns

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Heat Sensitive Colour Forming Recording (AREA)
  • Color Printing (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
JP2012525122A 2009-08-20 2010-08-09 ３−ジブチルラミノ−６−メチル−７−アニリノフルオランの製造方法 Withdrawn JP2013502391A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP09168288A EP2289896A1 (en) 2009-08-20 2009-08-20 Process for the manufacture of 3-dibutylamino-6-methyl-7-anilinofluoran
EP09168288.0 2009-08-20
PCT/EP2010/061530 WO2011020726A1 (en) 2009-08-20 2010-08-09 Process for the manufacture of 3-dibutylamino-6-methyl-7-anilinofluoran

Publications (2)

Publication Number Publication Date
JP2013502391A true JP2013502391A (ja) 2013-01-24
JP2013502391A5 JP2013502391A5 (https=) 2013-03-14

Family

ID=41314566

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2012525122A Withdrawn JP2013502391A (ja) 2009-08-20 2010-08-09 ３−ジブチルラミノ−６−メチル−７−アニリノフルオランの製造方法

Country Status (6)

Country Link
US (1) US20120149918A1 (https=)
EP (2) EP2289896A1 (https=)
JP (1) JP2013502391A (https=)
KR (1) KR20120062795A (https=)
CN (1) CN102471348A (https=)
WO (1) WO2011020726A1 (https=)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105838105B (zh) * 2016-04-23 2017-12-05 浙江鸿盛化工有限公司 一步法制备黑色荧烷类热压敏染料的方法
CN112010868B (zh) * 2020-09-02 2021-07-27 华烁科技股份有限公司 一种制备黑色可逆热致变色染料的方法
CN114349765B (zh) * 2022-01-21 2023-05-16 内蒙古源宏精细化工有限公司 2-苯氨基-3-甲基-6-二丁氨基荧烷高效绿色合成的方法
CN121494866B (zh) * 2026-01-14 2026-03-20 济南大学 一种提高热敏染料odb-2纯度的方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5166350A (en) 1989-06-10 1992-11-24 Ciba-Geigy Corporation Process for the manufacture of fluoran compounds
GB9827569D0 (en) * 1998-12-16 1999-02-10 Ciba Geigy Ag Heat sensitive recording material
EP1438126B1 (en) 2001-10-25 2012-07-04 Basf Se Process for the preparation of microcapsules
JP5194526B2 (ja) * 2007-04-06 2013-05-08 コニカミノルタホールディングス株式会社 薄膜トランジスタの製造方法、画素アレイの製造方法
CN101323619A (zh) * 2007-06-12 2008-12-17 上海瑞年精细化工有限公司 荧烷类化合物的制造方法

Also Published As

Publication number Publication date
EP2289896A1 (en) 2011-03-02
KR20120062795A (ko) 2012-06-14
EP2467386A1 (en) 2012-06-27
US20120149918A1 (en) 2012-06-14
CN102471348A (zh) 2012-05-23
WO2011020726A1 (en) 2011-02-24

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