JP2012530672A5 - - Google Patents
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- Publication number
- JP2012530672A5 JP2012530672A5 JP2012516703A JP2012516703A JP2012530672A5 JP 2012530672 A5 JP2012530672 A5 JP 2012530672A5 JP 2012516703 A JP2012516703 A JP 2012516703A JP 2012516703 A JP2012516703 A JP 2012516703A JP 2012530672 A5 JP2012530672 A5 JP 2012530672A5
- Authority
- JP
- Japan
- Prior art keywords
- compound
- particles
- general formula
- carbon
- drying
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002245 particle Substances 0.000 claims 14
- 150000001875 compounds Chemical class 0.000 claims 13
- 238000000034 method Methods 0.000 claims 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 4
- 229910052799 carbon Inorganic materials 0.000 claims 4
- 239000000203 mixture Substances 0.000 claims 4
- 239000007787 solid Substances 0.000 claims 4
- 239000003638 chemical reducing agent Substances 0.000 claims 3
- 238000001035 drying Methods 0.000 claims 3
- 229910052731 fluorine Inorganic materials 0.000 claims 3
- 238000004519 manufacturing process Methods 0.000 claims 3
- 229910052757 nitrogen Inorganic materials 0.000 claims 3
- 230000003647 oxidation Effects 0.000 claims 3
- 238000007254 oxidation reaction Methods 0.000 claims 3
- 229910052760 oxygen Inorganic materials 0.000 claims 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 2
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims 2
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 claims 2
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims 2
- 229910052783 alkali metal Inorganic materials 0.000 claims 2
- 150000001340 alkali metals Chemical class 0.000 claims 2
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 2
- 238000001354 calcination Methods 0.000 claims 2
- 239000007833 carbon precursor Substances 0.000 claims 2
- 239000008103 glucose Substances 0.000 claims 2
- 150000004676 glycans Chemical class 0.000 claims 2
- 229910001416 lithium ion Inorganic materials 0.000 claims 2
- 229910052755 nonmetal Inorganic materials 0.000 claims 2
- 239000001301 oxygen Substances 0.000 claims 2
- 229920001282 polysaccharide Polymers 0.000 claims 2
- 239000005017 polysaccharide Substances 0.000 claims 2
- 229910052723 transition metal Inorganic materials 0.000 claims 2
- 150000003624 transition metals Chemical class 0.000 claims 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims 1
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 claims 1
- 229910010707 LiFePO 4 Inorganic materials 0.000 claims 1
- 239000007864 aqueous solution Substances 0.000 claims 1
- 229910052785 arsenic Inorganic materials 0.000 claims 1
- 229960005070 ascorbic acid Drugs 0.000 claims 1
- 235000010323 ascorbic acid Nutrition 0.000 claims 1
- 239000011668 ascorbic acid Substances 0.000 claims 1
- 150000002016 disaccharides Chemical class 0.000 claims 1
- 239000011737 fluorine Substances 0.000 claims 1
- 229910052732 germanium Inorganic materials 0.000 claims 1
- 229910052742 iron Inorganic materials 0.000 claims 1
- 229910052748 manganese Inorganic materials 0.000 claims 1
- 150000002772 monosaccharides Chemical class 0.000 claims 1
- 229910052759 nickel Inorganic materials 0.000 claims 1
- 125000004437 phosphorous atom Chemical group 0.000 claims 1
- 229910052698 phosphorus Inorganic materials 0.000 claims 1
- 229910052710 silicon Inorganic materials 0.000 claims 1
- 238000001694 spray drying Methods 0.000 claims 1
- 229910052717 sulfur Inorganic materials 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US21980209P | 2009-06-24 | 2009-06-24 | |
| US61/219,802 | 2009-06-24 | ||
| PCT/EP2010/058868 WO2010149681A1 (en) | 2009-06-24 | 2010-06-23 | Process for the preparation of lifepo4-carbon composites |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012530672A JP2012530672A (ja) | 2012-12-06 |
| JP2012530672A5 true JP2012530672A5 (OSRAM) | 2013-07-25 |
| JP5886193B2 JP5886193B2 (ja) | 2016-03-16 |
Family
ID=42584231
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012516703A Active JP5886193B2 (ja) | 2009-06-24 | 2010-06-23 | ＬｉＦｅＰＯ４−炭素合成物を製造するための方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US9209461B2 (OSRAM) |
| EP (1) | EP2445834B1 (OSRAM) |
| JP (1) | JP5886193B2 (OSRAM) |
| KR (1) | KR101718972B1 (OSRAM) |
| CN (1) | CN102803133B (OSRAM) |
| CA (1) | CA2764410A1 (OSRAM) |
| TW (1) | TW201111276A (OSRAM) |
| WO (1) | WO2010149681A1 (OSRAM) |
Families Citing this family (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20120292367A1 (en) | 2006-01-31 | 2012-11-22 | Ethicon Endo-Surgery, Inc. | Robotically-controlled end effector |
| CN102556996A (zh) * | 2010-12-30 | 2012-07-11 | 中国电子科技集团公司第十八研究所 | 一种高振实密度磷酸铁锂的制备方法 |
| CA2827930A1 (en) * | 2011-03-16 | 2012-09-20 | Hanwha Chemical Corporation | Method for calcining electrode materials using a rotary kiln |
| JP2012204322A (ja) * | 2011-03-28 | 2012-10-22 | Gs Yuasa Corp | 非水電解質二次電池用活物質の製造方法 |
| FR2997076B1 (fr) * | 2012-10-19 | 2014-12-26 | Commissariat Energie Atomique | Materiau composite comprenant des nano-objets notamment des nano-objets de carbone, son procede de preparation, et encre et electrode comprenant ce materiau. |
| US10236512B2 (en) | 2013-05-08 | 2019-03-19 | Advanced Lithium Electrochemistry Co., Ltd. | Preparation method of battery composite material and precursor thereof |
| EP2835349A1 (en) * | 2013-08-09 | 2015-02-11 | Basf Se | Process for the preparation of an electrode material and its use in lithium-ion batteries |
| KR101608632B1 (ko) * | 2013-08-20 | 2016-04-05 | 주식회사 엘지화학 | 리튬 복합 전이금속 산화물 제조용 전구체, 그 제조방법 및 이를 이용한 리튬 복합 전이금속 산화물 |
| PL233550B1 (pl) * | 2014-03-12 | 2019-10-31 | Akademia Gorniczo Hutnicza Im Stanislawa Staszica W Krakowie | Sposób otrzymywania krystalicznego nanometrycznego fosforanu litowo-żelazowego |
| JP6326366B2 (ja) * | 2014-12-25 | 2018-05-16 | 信越化学工業株式会社 | リチウムリン系複合酸化物炭素複合体及びその製造方法並びに、電気化学デバイス及びリチウムイオン二次電池 |
| KR102161590B1 (ko) * | 2016-03-29 | 2020-10-05 | 주식회사 엘지화학 | 이차전지용 양극의 제조방법, 및 이를 이용하여 제조된 양극 및 이차전지 |
| FR3077012B1 (fr) | 2018-01-25 | 2020-01-03 | Brgm | Procede d'obtention de (nano)particules minerales enrobees de carbone |
| JP6964055B2 (ja) * | 2018-08-23 | 2021-11-10 | 住友大阪セメント株式会社 | リチウムイオン二次電池用正極材料の製造方法 |
| TWI785881B (zh) | 2019-06-28 | 2022-12-01 | 美商壹久公司 | 具有輔助氣體流的處理系統與方法及所製成用於電池的材料 |
| US11376559B2 (en) | 2019-06-28 | 2022-07-05 | eJoule, Inc. | Processing system and method for producing a particulate material |
| US11121354B2 (en) | 2019-06-28 | 2021-09-14 | eJoule, Inc. | System with power jet modules and method thereof |
Family Cites Families (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6514640B1 (en) | 1996-04-23 | 2003-02-04 | Board Of Regents, The University Of Texas System | Cathode materials for secondary (rechargeable) lithium batteries |
| CA2270771A1 (fr) | 1999-04-30 | 2000-10-30 | Hydro-Quebec | Nouveaux materiaux d'electrode presentant une conductivite de surface elevee |
| US6528033B1 (en) | 2000-01-18 | 2003-03-04 | Valence Technology, Inc. | Method of making lithium-containing materials |
| US6777132B2 (en) * | 2000-04-27 | 2004-08-17 | Valence Technology, Inc. | Alkali/transition metal halo—and hydroxy-phosphates and related electrode active materials |
| CA2320661A1 (fr) * | 2000-09-26 | 2002-03-26 | Hydro-Quebec | Nouveau procede de synthese de materiaux limpo4 a structure olivine |
| JP2003203628A (ja) * | 2001-12-28 | 2003-07-18 | Sanyo Electric Co Ltd | 非水電解質電池及びその製造方法 |
| US6913855B2 (en) * | 2002-07-22 | 2005-07-05 | Valence Technology, Inc. | Method of synthesizing electrochemically active materials from a slurry of precursors |
| FR2852148B1 (fr) | 2003-03-07 | 2014-04-11 | Batscap Sa | Materiau pour electrode composite, procede pour sa preparation |
| CN1233054C (zh) | 2003-12-17 | 2005-12-21 | 北京科技大学 | 一种采用微波法制备LiFePO4材料的方法 |
| JP2006155941A (ja) | 2004-11-25 | 2006-06-15 | Kyushu Univ | 電極活物質の製造方法 |
| DE102005012640B4 (de) | 2005-03-18 | 2015-02-05 | Süd-Chemie Ip Gmbh & Co. Kg | Kreisprozess zur nasschemischen Herstellung von Lithiummetallphosphaten |
| DE102005015613A1 (de) | 2005-04-05 | 2006-10-12 | Süd-Chemie AG | Kristallines Ionenleitendes Nanomaterial und Verfahren zu seiner Herstellung |
| JP4804045B2 (ja) * | 2005-06-15 | 2011-10-26 | Ａｇｃセイミケミカル株式会社 | リチウム鉄複合酸化物の製造方法 |
| US7964118B2 (en) * | 2005-09-21 | 2011-06-21 | Kanto Denka Kogyo Co., Ltd. | Positive electrode active material and method of producing the same and nonaqueous electrolyte battery having positive electrode containing positive electrode active material |
| CN101200289A (zh) | 2006-12-15 | 2008-06-18 | 中国电子科技集团公司第十八研究所 | 一种磷酸铁锂材料及其制备方法 |
| JP5385616B2 (ja) * | 2007-01-29 | 2014-01-08 | 関東電化工業株式会社 | オリビン構造を有する化合物及びその製造方法、並びにオリビン構造を有する化合物を使用する正極活物質及び非水電解質電池 |
| CN100540465C (zh) | 2007-07-23 | 2009-09-16 | 河北工业大学 | 锂离子电池正极材料磷酸铁锂的水热合成制备方法 |
| DE102008002989A1 (de) | 2007-08-16 | 2009-02-19 | Basf Se | Elektrisch leitfähiges, magnetisches Kompositmaterial, Verfahren zu seiner Herstellung und seine Verwendung |
| CN100511778C (zh) | 2007-08-24 | 2009-07-08 | 郑州德朗能电池有限公司 | 高性能锂离子电池正极材料LiFePO4/C的制备方法 |
| CN100502103C (zh) * | 2007-09-13 | 2009-06-17 | 广西师范大学 | 一种核壳型纳米级碳包覆磷酸铁锂复合正极材料及其制备方法 |
| CN102123943B (zh) | 2007-10-01 | 2013-07-10 | 巴斯夫欧洲公司 | 制备包含锂、钒和磷酸根的多孔材料的方法 |
| KR101519686B1 (ko) | 2007-10-01 | 2015-05-12 | 바스프 에스이 | 결정질 리튬, 바나듐 및 포스페이트 함유 물질의 제조 방법 |
| DE102007058674A1 (de) * | 2007-12-06 | 2009-07-02 | Süd-Chemie AG | Nanopartikuläre Zusammensetzung und Verfahren zu deren Herstellung |
| TW201010944A (en) | 2008-04-17 | 2010-03-16 | Basf Se | Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials |
| TW200951066A (en) * | 2008-04-17 | 2009-12-16 | Basf Se | Process for the preparation of crystalline lithium-, iron-and phosphate-comprising materials |
| TW201002623A (en) | 2008-05-30 | 2010-01-16 | Basf Se | Process for preparing lithium vanadium oxides and their use as cathode material |
| CN101339995A (zh) * | 2008-08-12 | 2009-01-07 | 中国兵器工业第二一三研究所 | 锂离子动力电池用磷酸铁锂正极材料的制备方法 |
| TWI440597B (zh) | 2008-08-26 | 2014-06-11 | Basf Se | 於水熱條件下合成ＬｉＦｅＰＯ4 |
| TW201038469A (en) | 2009-03-17 | 2010-11-01 | Basf Se | Synthesis of lithium-iron-phosphates |
| US20110249603A1 (en) | 2009-06-16 | 2011-10-13 | Qualcomm Incorporated | Apparatus and method for multiple wireless service coexistence |
-
2010
- 2010-06-23 KR KR1020127001823A patent/KR101718972B1/ko active Active
- 2010-06-23 CA CA2764410A patent/CA2764410A1/en not_active Abandoned
- 2010-06-23 WO PCT/EP2010/058868 patent/WO2010149681A1/en not_active Ceased
- 2010-06-23 CN CN201080028061.9A patent/CN102803133B/zh active Active
- 2010-06-23 JP JP2012516703A patent/JP5886193B2/ja active Active
- 2010-06-23 US US13/379,048 patent/US9209461B2/en active Active
- 2010-06-23 EP EP10724538.3A patent/EP2445834B1/en active Active
- 2010-06-24 TW TW099120631A patent/TW201111276A/zh unknown
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