JP2011502758A5 - - Google Patents
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- JP2011502758A5 JP2011502758A5 JP2010532584A JP2010532584A JP2011502758A5 JP 2011502758 A5 JP2011502758 A5 JP 2011502758A5 JP 2010532584 A JP2010532584 A JP 2010532584A JP 2010532584 A JP2010532584 A JP 2010532584A JP 2011502758 A5 JP2011502758 A5 JP 2011502758A5
- Authority
- JP
- Japan
- Prior art keywords
- catalyst
- metal
- platinum group
- complex
- stage
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 229910052751 metal Inorganic materials 0.000 claims description 67
- 239000002184 metal Substances 0.000 claims description 67
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical group [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims description 39
- 239000003054 catalyst Substances 0.000 claims description 36
- 238000000034 method Methods 0.000 claims description 23
- 150000001875 compounds Chemical class 0.000 claims description 13
- 239000000843 powder Substances 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 8
- -1 platinum group metals Chemical class 0.000 claims description 8
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 6
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 claims description 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 6
- 229910052799 carbon Inorganic materials 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 6
- 239000002904 solvent Substances 0.000 claims description 6
- 229910052723 transition metal Inorganic materials 0.000 claims description 6
- 150000003624 transition metals Chemical class 0.000 claims description 6
- 150000002170 ethers Chemical class 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 229910052697 platinum Inorganic materials 0.000 claims description 4
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 claims description 3
- 229910017052 cobalt Inorganic materials 0.000 claims description 3
- 239000010941 cobalt Substances 0.000 claims description 3
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 3
- 229910052759 nickel Inorganic materials 0.000 claims description 3
- 229910052763 palladium Inorganic materials 0.000 claims description 3
- 229910052707 ruthenium Inorganic materials 0.000 claims description 3
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 239000012298 atmosphere Substances 0.000 claims 6
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 claims 4
- 238000005984 hydrogenation reaction Methods 0.000 claims 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims 3
- 150000004696 coordination complex Chemical class 0.000 claims 3
- 239000001257 hydrogen Substances 0.000 claims 3
- 229910052739 hydrogen Inorganic materials 0.000 claims 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 claims 2
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 claims 2
- 238000005868 electrolysis reaction Methods 0.000 claims 2
- 239000007789 gas Substances 0.000 claims 2
- 239000003446 ligand Substances 0.000 claims 2
- POILWHVDKZOXJZ-ARJAWSKDSA-M (z)-4-oxopent-2-en-2-olate Chemical compound C\C([O-])=C\C(C)=O POILWHVDKZOXJZ-ARJAWSKDSA-M 0.000 claims 1
- DTIGTFJLLYWKTF-UHFFFAOYSA-N 2-methylnona-2,4-diene Chemical compound CCCCC=CC=C(C)C DTIGTFJLLYWKTF-UHFFFAOYSA-N 0.000 claims 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 claims 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- 239000005922 Phosphane Substances 0.000 claims 1
- XYFCBTPGUUZFHI-UHFFFAOYSA-N Phosphine Chemical compound P XYFCBTPGUUZFHI-UHFFFAOYSA-N 0.000 claims 1
- 150000007824 aliphatic compounds Chemical class 0.000 claims 1
- 150000001336 alkenes Chemical class 0.000 claims 1
- 238000005576 amination reaction Methods 0.000 claims 1
- 150000001491 aromatic compounds Chemical class 0.000 claims 1
- 125000003118 aryl group Chemical group 0.000 claims 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 1
- 229910002091 carbon monoxide Inorganic materials 0.000 claims 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims 1
- 238000001816 cooling Methods 0.000 claims 1
- 125000004093 cyano group Chemical group *C#N 0.000 claims 1
- 238000006356 dehydrogenation reaction Methods 0.000 claims 1
- 239000010411 electrocatalyst Substances 0.000 claims 1
- 238000006056 electrooxidation reaction Methods 0.000 claims 1
- 150000002148 esters Chemical class 0.000 claims 1
- 150000002391 heterocyclic compounds Chemical class 0.000 claims 1
- 150000002431 hydrogen Chemical class 0.000 claims 1
- 125000002462 isocyano group Chemical group *[N+]#[C-] 0.000 claims 1
- 239000002480 mineral oil Substances 0.000 claims 1
- 235000010446 mineral oil Nutrition 0.000 claims 1
- 125000002560 nitrile group Chemical group 0.000 claims 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 claims 1
- 229910052757 nitrogen Inorganic materials 0.000 claims 1
- 239000012299 nitrogen atmosphere Substances 0.000 claims 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 claims 1
- 150000002902 organometallic compounds Chemical class 0.000 claims 1
- 230000003647 oxidation Effects 0.000 claims 1
- 238000007254 oxidation reaction Methods 0.000 claims 1
- 239000001301 oxygen Substances 0.000 claims 1
- 229910052760 oxygen Inorganic materials 0.000 claims 1
- 229910000064 phosphane Inorganic materials 0.000 claims 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 3
- 239000000956 alloy Substances 0.000 description 3
- 229910045601 alloy Inorganic materials 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 2
- 239000006229 carbon black Substances 0.000 description 2
- 238000005229 chemical vapour deposition Methods 0.000 description 2
- 238000000151 deposition Methods 0.000 description 2
- 238000005240 physical vapour deposition Methods 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- RMGHERXMTMUMMV-UHFFFAOYSA-N 2-methoxypropane Chemical compound COC(C)C RMGHERXMTMUMMV-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 150000001721 carbon Chemical class 0.000 description 1
- 229910021393 carbon nanotube Inorganic materials 0.000 description 1
- 239000002041 carbon nanotube Substances 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 150000004292 cyclic ethers Chemical class 0.000 description 1
- POLCUAVZOMRGSN-UHFFFAOYSA-N dipropyl ether Chemical compound CCCOCCC POLCUAVZOMRGSN-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 229910052741 iridium Inorganic materials 0.000 description 1
- GKOZUEZYRPOHIO-UHFFFAOYSA-N iridium atom Chemical compound [Ir] GKOZUEZYRPOHIO-UHFFFAOYSA-N 0.000 description 1
- 239000003273 ketjen black Substances 0.000 description 1
- 150000002736 metal compounds Chemical class 0.000 description 1
- 125000002524 organometallic group Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000011164 primary particle Substances 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 239000010948 rhodium Substances 0.000 description 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP07120359.0 | 2007-11-09 | ||
| EP07120359 | 2007-11-09 | ||
| PCT/EP2008/065039 WO2009060019A1 (de) | 2007-11-09 | 2008-11-06 | Verfahren zur herstellung eines katalysators sowie verwendung als elektrokatalysator |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2011502758A JP2011502758A (ja) | 2011-01-27 |
| JP2011502758A5 true JP2011502758A5 (https=) | 2011-12-22 |
| JP5579071B2 JP5579071B2 (ja) | 2014-08-27 |
Family
ID=40349945
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2010532584A Expired - Fee Related JP5579071B2 (ja) | 2007-11-09 | 2008-11-06 | 触媒の製造方法並びに電気触媒としての使用 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US8293675B2 (https=) |
| EP (1) | EP2217372A1 (https=) |
| JP (1) | JP5579071B2 (https=) |
| KR (1) | KR101541207B1 (https=) |
| CN (1) | CN101990462A (https=) |
| CA (1) | CA2704667A1 (https=) |
| RU (1) | RU2010123285A (https=) |
| WO (1) | WO2009060019A1 (https=) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8569196B2 (en) * | 2008-08-26 | 2013-10-29 | Basf Se | Process for the continuous production of a catalyst |
| EP2417059B1 (de) | 2009-04-06 | 2014-12-10 | Basf Se | Verfahren zur umsetzung von erdgas zu aromaten mit elektrochemischer abtrennung von wasserstoff |
| JP2012526741A (ja) | 2009-05-14 | 2012-11-01 | ビーエーエスエフ ソシエタス・ヨーロピア | 芳香族アミンの製造方法 |
| WO2010139596A2 (en) * | 2009-06-02 | 2010-12-09 | Basf Se | Catalyst for electrochemical applications |
| JP5471252B2 (ja) * | 2009-09-30 | 2014-04-16 | 国立大学法人北海道大学 | 合金化度と分散性を制御したＰｔＲｕ／Ｃ触媒及びその製造方法 |
| JP5660917B2 (ja) * | 2011-02-04 | 2015-01-28 | 国立大学法人東京工業大学 | 燃料電池用空気極触媒とその製造方法 |
| WO2013182535A1 (de) | 2012-06-06 | 2013-12-12 | Basf Se | Verfahren zur herstellung von stickstoff-dotierten übergangsmetallkatalysatoren und ihre verwendung für die elektrochemische oxidation von s(iv) verbindungen |
| CN103915633B (zh) * | 2014-04-01 | 2016-08-24 | 上海交通大学 | 一种复合碳纤维载金属催化剂及其制备方法和应用 |
| WO2015175759A1 (en) | 2014-05-16 | 2015-11-19 | Dow Global Technologies Llc | Process for synthesizing iron carbide fischer-tropsch catalysts |
| WO2016063968A1 (ja) * | 2014-10-24 | 2016-04-28 | 株式会社キャタラー | 燃料電池用電極触媒及びその製造方法 |
| US20190314805A1 (en) * | 2016-10-20 | 2019-10-17 | Basf Se | A process for producing a catalyst comprising an intermetallic compound and a catalyst produced by the process |
| US20200230581A1 (en) * | 2017-10-03 | 2020-07-23 | Northwestern University | Nanocatalysts for electrochemical hydrogen production and catalyst screening methods |
| KR102291160B1 (ko) * | 2018-11-08 | 2021-08-19 | 한국과학기술원 | 연료전지용 금 도핑 백금계 합금 촉매 및 이의 제조 방법 |
| KR102425528B1 (ko) * | 2020-10-28 | 2022-07-25 | 한국화학연구원 | 화학 기상 증착법을 이용한 저온활성이 향상된 deNOx 촉매의 제조방법 및 이로부터 제조된 deNOx촉매 |
| KR102451629B1 (ko) * | 2020-11-25 | 2022-10-06 | 충남대학교산학협력단 | 산소 환원 반응용 백금계 촉매 및 그 제조방법 |
| KR102468470B1 (ko) * | 2020-12-09 | 2022-11-18 | 비나텍주식회사 | 연료전지용 백금계 합금 촉매의 제조 방법 |
| KR102466103B1 (ko) * | 2020-12-18 | 2022-11-11 | 비나텍주식회사 | 연료전지용 백금계 합금 촉매의 제조 방법 |
| KR102459158B1 (ko) * | 2020-12-18 | 2022-10-26 | 비나텍주식회사 | 코발트를 함유하는 연료전지용 백금계 합금 촉매의 제조 방법 |
| CN113437318A (zh) * | 2021-06-25 | 2021-09-24 | 北京大学 | 一种碳负载的贵金属合金纳米颗粒及其制备方法和应用 |
| CN115863678A (zh) * | 2022-12-20 | 2023-03-28 | 佛山仙湖实验室 | 一种富含缺陷的铂基纳米片催化剂及其制备方法和应用 |
Family Cites Families (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2628417B1 (fr) * | 1988-03-08 | 1990-07-27 | Rhone Poulenc Sante | Procede de preparation d'alcools insatures |
| US5916702A (en) * | 1997-08-15 | 1999-06-29 | Exxon Research And Engineering Co. | CO tolerant platinum-zinc fuel cell electrode |
| JP2001198469A (ja) * | 1999-11-05 | 2001-07-24 | Sekisui Chem Co Ltd | 水素貯蔵・供給用金属担持触媒及びこれを利用した水素貯蔵・供給システム |
| JP2002095969A (ja) * | 2000-09-21 | 2002-04-02 | Ishifuku Metal Ind Co Ltd | 白金−コバルト合金触媒の製造方法 |
| US7157401B2 (en) * | 2002-10-17 | 2007-01-02 | Carnegie Mellon University | Catalyst for the treatment of organic compounds |
| US20040101718A1 (en) * | 2002-11-26 | 2004-05-27 | Lixin Cao | Metal alloy for electrochemical oxidation reactions and method of production thereof |
| KR100506091B1 (ko) * | 2003-02-19 | 2005-08-04 | 삼성에스디아이 주식회사 | 연료전지의 캐소드용 촉매 |
| US7208437B2 (en) * | 2004-01-16 | 2007-04-24 | T/J Technologies, Inc. | Catalyst and method for its manufacture |
| US7335245B2 (en) * | 2004-04-22 | 2008-02-26 | Honda Motor Co., Ltd. | Metal and alloy nanoparticles and synthesis methods thereof |
| JP4490201B2 (ja) * | 2004-08-04 | 2010-06-23 | Ｄｏｗａホールディングス株式会社 | 凹凸表面をもつ微細な合金粒子粉末およびその製造法 |
| JP4390693B2 (ja) * | 2004-12-17 | 2009-12-24 | 富士通株式会社 | 燃料電池用触媒の製造方法および燃料電池の製造方法 |
| US7507495B2 (en) * | 2004-12-22 | 2009-03-24 | Brookhaven Science Associates, Llc | Hydrogen absorption induced metal deposition on palladium and palladium-alloy particles |
-
2008
- 2008-11-06 CN CN200880124347XA patent/CN101990462A/zh active Pending
- 2008-11-06 EP EP08848397A patent/EP2217372A1/de not_active Withdrawn
- 2008-11-06 KR KR1020107012730A patent/KR101541207B1/ko not_active Expired - Fee Related
- 2008-11-06 US US12/742,026 patent/US8293675B2/en not_active Expired - Fee Related
- 2008-11-06 CA CA2704667A patent/CA2704667A1/en not_active Abandoned
- 2008-11-06 WO PCT/EP2008/065039 patent/WO2009060019A1/de not_active Ceased
- 2008-11-06 RU RU2010123285/04A patent/RU2010123285A/ru unknown
- 2008-11-06 JP JP2010532584A patent/JP5579071B2/ja not_active Expired - Fee Related
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