CA2704667A1 - Process for producing a catalyst and use of the catalyst - Google Patents

Process for producing a catalyst and use of the catalyst Download PDF

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Publication number
CA2704667A1
CA2704667A1 CA2704667A CA2704667A CA2704667A1 CA 2704667 A1 CA2704667 A1 CA 2704667A1 CA 2704667 A CA2704667 A CA 2704667A CA 2704667 A CA2704667 A CA 2704667A CA 2704667 A1 CA2704667 A1 CA 2704667A1
Authority
CA
Canada
Prior art keywords
metal
catalyst
process according
platinum group
carried out
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
CA2704667A
Other languages
English (en)
French (fr)
Inventor
Stefan Kotrel
Gerhard Cox
Ekkehard Schwab
Alexander Panchenko
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CA2704667A1 publication Critical patent/CA2704667A1/en
Abandoned legal-status Critical Current

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/082—Decomposition and pyrolysis
    • B01J37/086—Decomposition of an organometallic compound, a metal complex or a metal salt of a carboxylic acid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/92—Chemical or biological purification of waste gases of engine exhaust gases
    • B01D53/94—Chemical or biological purification of waste gases of engine exhaust gases by catalytic processes
    • B01D53/9445—Simultaneously removing carbon monoxide, hydrocarbons or nitrogen oxides making use of three-way catalysts [TWC] or four-way-catalysts [FWC]
    • B01D53/945—Simultaneously removing carbon monoxide, hydrocarbons or nitrogen oxides making use of three-way catalysts [TWC] or four-way-catalysts [FWC] characterised by a specific catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/46—Ruthenium, rhodium, osmium or iridium
    • B01J23/462—Ruthenium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/89—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with noble metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
    • B01J35/391—Physical properties of the active metal ingredient
    • B01J35/393—Metal or metal oxide crystallite size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/04—Mixing
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90—Selection of catalytic material
    • H01M4/92—Metals of platinum group
    • H01M4/921—Alloys or mixtures with metallic elements
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00—Electrodes
    • H01M4/86—Inert electrodes with catalytic activity, e.g. for fuel cells
    • H01M4/90—Selection of catalytic material
    • H01M4/92—Metals of platinum group
    • H01M4/925—Metals of platinum group supported on carriers, e.g. powder carriers
    • H01M4/926—Metals of platinum group supported on carriers, e.g. powder carriers on carbon or graphite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2255/00—Catalysts
    • B01D2255/10—Noble metals or compounds thereof
    • B01D2255/102—Platinum group metals
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2255/00—Catalysts
    • B01D2255/20—Metals or compounds thereof
    • B01D2255/207—Transition metals
    • B01D2255/20746—Cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2255/00—Catalysts
    • B01D2255/20—Metals or compounds thereof
    • B01D2255/207—Transition metals
    • B01D2255/20753—Nickel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2255/00—Catalysts
    • B01D2255/70—Non-metallic catalysts, additives or dopants
    • B01D2255/702—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/30—Scanning electron microscopy; Transmission electron microscopy
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56—Platinum group metals
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M8/00—Fuel cells; Manufacture thereof
    • H01M8/10—Fuel cells with solid electrolytes
    • H01M8/1009—Fuel cells with solid electrolytes with one of the reactants being liquid, solid or liquid-charged
    • H01M8/1011—Direct alcohol fuel cells [DAFC], e.g. direct methanol fuel cells [DMFC]
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/30—Hydrogen technology
    • Y02E60/50—Fuel cells
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02T—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO TRANSPORTATION
    • Y02T10/00—Road transport of goods or passengers
    • Y02T10/10—Internal combustion engine [ICE] based vehicles
    • Y02T10/12—Improving ICE efficiencies

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Biomedical Technology (AREA)
  • Environmental & Geological Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Catalysts (AREA)
  • Inert Electrodes (AREA)
CA2704667A 2007-11-09 2008-11-06 Process for producing a catalyst and use of the catalyst Abandoned CA2704667A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP07120359.0 2007-11-09
EP07120359 2007-11-09
PCT/EP2008/065039 WO2009060019A1 (de) 2007-11-09 2008-11-06 Verfahren zur herstellung eines katalysators sowie verwendung als elektrokatalysator

Publications (1)

Publication Number Publication Date
CA2704667A1 true CA2704667A1 (en) 2009-05-14

Family

ID=40349945

Family Applications (1)

Application Number Title Priority Date Filing Date
CA2704667A Abandoned CA2704667A1 (en) 2007-11-09 2008-11-06 Process for producing a catalyst and use of the catalyst

Country Status (8)

Country Link
US (1) US8293675B2 (https=)
EP (1) EP2217372A1 (https=)
JP (1) JP5579071B2 (https=)
KR (1) KR101541207B1 (https=)
CN (1) CN101990462A (https=)
CA (1) CA2704667A1 (https=)
RU (1) RU2010123285A (https=)
WO (1) WO2009060019A1 (https=)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8569196B2 (en) * 2008-08-26 2013-10-29 Basf Se Process for the continuous production of a catalyst
EP2417059B1 (de) 2009-04-06 2014-12-10 Basf Se Verfahren zur umsetzung von erdgas zu aromaten mit elektrochemischer abtrennung von wasserstoff
JP2012526741A (ja) 2009-05-14 2012-11-01 ビーエーエスエフ ソシエタス・ヨーロピア 芳香族アミンの製造方法
WO2010139596A2 (en) * 2009-06-02 2010-12-09 Basf Se Catalyst for electrochemical applications
JP5471252B2 (ja) * 2009-09-30 2014-04-16 国立大学法人北海道大学 合金化度と分散性を制御したＰｔＲｕ／Ｃ触媒及びその製造方法
JP5660917B2 (ja) * 2011-02-04 2015-01-28 国立大学法人東京工業大学 燃料電池用空気極触媒とその製造方法
WO2013182535A1 (de) 2012-06-06 2013-12-12 Basf Se Verfahren zur herstellung von stickstoff-dotierten übergangsmetallkatalysatoren und ihre verwendung für die elektrochemische oxidation von s(iv) verbindungen
CN103915633B (zh) * 2014-04-01 2016-08-24 上海交通大学 一种复合碳纤维载金属催化剂及其制备方法和应用
WO2015175759A1 (en) 2014-05-16 2015-11-19 Dow Global Technologies Llc Process for synthesizing iron carbide fischer-tropsch catalysts
WO2016063968A1 (ja) * 2014-10-24 2016-04-28 株式会社キャタラー 燃料電池用電極触媒及びその製造方法
US20190314805A1 (en) * 2016-10-20 2019-10-17 Basf Se A process for producing a catalyst comprising an intermetallic compound and a catalyst produced by the process
US20200230581A1 (en) * 2017-10-03 2020-07-23 Northwestern University Nanocatalysts for electrochemical hydrogen production and catalyst screening methods
KR102291160B1 (ko) * 2018-11-08 2021-08-19 한국과학기술원 연료전지용 금 도핑 백금계 합금 촉매 및 이의 제조 방법
KR102425528B1 (ko) * 2020-10-28 2022-07-25 한국화학연구원 화학 기상 증착법을 이용한 저온활성이 향상된 deNOx 촉매의 제조방법 및 이로부터 제조된 deNOx촉매
KR102451629B1 (ko) * 2020-11-25 2022-10-06 충남대학교산학협력단 산소 환원 반응용 백금계 촉매 및 그 제조방법
KR102468470B1 (ko) * 2020-12-09 2022-11-18 비나텍주식회사 연료전지용 백금계 합금 촉매의 제조 방법
KR102466103B1 (ko) * 2020-12-18 2022-11-11 비나텍주식회사 연료전지용 백금계 합금 촉매의 제조 방법
KR102459158B1 (ko) * 2020-12-18 2022-10-26 비나텍주식회사 코발트를 함유하는 연료전지용 백금계 합금 촉매의 제조 방법
CN113437318A (zh) * 2021-06-25 2021-09-24 北京大学 一种碳负载的贵金属合金纳米颗粒及其制备方法和应用
CN115863678A (zh) * 2022-12-20 2023-03-28 佛山仙湖实验室 一种富含缺陷的铂基纳米片催化剂及其制备方法和应用

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2628417B1 (fr) * 1988-03-08 1990-07-27 Rhone Poulenc Sante Procede de preparation d'alcools insatures
US5916702A (en) * 1997-08-15 1999-06-29 Exxon Research And Engineering Co. CO tolerant platinum-zinc fuel cell electrode
JP2001198469A (ja) * 1999-11-05 2001-07-24 Sekisui Chem Co Ltd 水素貯蔵・供給用金属担持触媒及びこれを利用した水素貯蔵・供給システム
JP2002095969A (ja) * 2000-09-21 2002-04-02 Ishifuku Metal Ind Co Ltd 白金−コバルト合金触媒の製造方法
US7157401B2 (en) * 2002-10-17 2007-01-02 Carnegie Mellon University Catalyst for the treatment of organic compounds
US20040101718A1 (en) * 2002-11-26 2004-05-27 Lixin Cao Metal alloy for electrochemical oxidation reactions and method of production thereof
KR100506091B1 (ko) * 2003-02-19 2005-08-04 삼성에스디아이 주식회사 연료전지의 캐소드용 촉매
US7208437B2 (en) * 2004-01-16 2007-04-24 T/J Technologies, Inc. Catalyst and method for its manufacture
US7335245B2 (en) * 2004-04-22 2008-02-26 Honda Motor Co., Ltd. Metal and alloy nanoparticles and synthesis methods thereof
JP4490201B2 (ja) * 2004-08-04 2010-06-23 Ｄｏｗａホールディングス株式会社 凹凸表面をもつ微細な合金粒子粉末およびその製造法
JP4390693B2 (ja) * 2004-12-17 2009-12-24 富士通株式会社 燃料電池用触媒の製造方法および燃料電池の製造方法
US7507495B2 (en) * 2004-12-22 2009-03-24 Brookhaven Science Associates, Llc Hydrogen absorption induced metal deposition on palladium and palladium-alloy particles

Also Published As

Publication number Publication date
JP5579071B2 (ja) 2014-08-27
US8293675B2 (en) 2012-10-23
CN101990462A (zh) 2011-03-23
US20100267551A1 (en) 2010-10-21
JP2011502758A (ja) 2011-01-27
EP2217372A1 (de) 2010-08-18
KR20100099160A (ko) 2010-09-10
KR101541207B1 (ko) 2015-07-31
RU2010123285A (ru) 2011-12-20
WO2009060019A1 (de) 2009-05-14

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