JP2009522389A5 - - Google Patents
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- Publication number
- JP2009522389A5 JP2009522389A5 JP2008547970A JP2008547970A JP2009522389A5 JP 2009522389 A5 JP2009522389 A5 JP 2009522389A5 JP 2008547970 A JP2008547970 A JP 2008547970A JP 2008547970 A JP2008547970 A JP 2008547970A JP 2009522389 A5 JP2009522389 A5 JP 2009522389A5
- Authority
- JP
- Japan
- Prior art keywords
- additive
- reactor
- reaction mixture
- residence time
- monomer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000178 monomer Substances 0.000 claims description 10
- 238000004519 manufacturing process Methods 0.000 claims description 3
- 239000002245 particle Substances 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 claims 12
- 239000000654 additive Substances 0.000 claims 10
- 230000000996 additive effect Effects 0.000 claims 10
- 239000011541 reaction mixture Substances 0.000 claims 8
- 239000011347 resin Substances 0.000 claims 6
- 229920005989 resin Polymers 0.000 claims 6
- 239000000843 powder Substances 0.000 claims 4
- 239000000203 mixture Substances 0.000 claims 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 2
- 239000002250 absorbent Substances 0.000 claims 2
- 239000003795 chemical substances by application Substances 0.000 claims 2
- 239000003431 cross linking reagent Substances 0.000 claims 2
- 239000000945 filler Substances 0.000 claims 2
- 239000000017 hydrogel Substances 0.000 claims 2
- 239000010954 inorganic particle Substances 0.000 claims 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- 229910021536 Zeolite Inorganic materials 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 239000004927 clay Substances 0.000 claims 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 1
- 238000010348 incorporation Methods 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 229910044991 metal oxide Inorganic materials 0.000 claims 1
- 150000004706 metal oxides Chemical class 0.000 claims 1
- 229910001463 metal phosphate Inorganic materials 0.000 claims 1
- 238000006116 polymerization reaction Methods 0.000 claims 1
- 230000000379 polymerizing effect Effects 0.000 claims 1
- 239000010457 zeolite Substances 0.000 claims 1
- 230000000052 comparative effect Effects 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005062929.6 | 2005-12-29 | ||
| DE102005062929A DE102005062929A1 (de) | 2005-12-29 | 2005-12-29 | Herstellung eines wasserabsorbierenden Harzes unter Einmischen eines wasserabsorbierenden Harzpulvers |
| PCT/EP2006/070250 WO2007074167A2 (de) | 2005-12-29 | 2006-12-28 | Herstellung eines wasserabsorbierenden harzes unter einmischen eines teilchenförmigen additivs |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2009522389A JP2009522389A (ja) | 2009-06-11 |
| JP2009522389A5 true JP2009522389A5 (https=) | 2012-01-12 |
| JP5091159B2 JP5091159B2 (ja) | 2012-12-05 |
Family
ID=38118047
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008547970A Expired - Fee Related JP5091159B2 (ja) | 2005-12-29 | 2006-12-28 | 粒子状添加剤の混入下での吸水性樹脂の製造 |
Country Status (8)
| Country | Link |
|---|---|
| US (2) | US7786211B2 (https=) |
| EP (1) | EP1969017B1 (https=) |
| JP (1) | JP5091159B2 (https=) |
| CN (1) | CN101389661B (https=) |
| AT (1) | ATE449793T1 (https=) |
| DE (2) | DE102005062929A1 (https=) |
| TW (1) | TW200732354A (https=) |
| WO (1) | WO2007074167A2 (https=) |
Families Citing this family (41)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102005001789A1 (de) * | 2005-01-13 | 2006-07-27 | Basf Ag | Verfahren zum Klassieren eines teilchenförmigen wasserabsorbierenden Harzes |
| WO2008095893A1 (de) * | 2007-02-06 | 2008-08-14 | Basf Se | Verfahren zur herstellung von polymerpartikeln durch polymerisation von flüssigkeitstropfen in einer gasphase |
| US20100261604A1 (en) * | 2007-12-19 | 2010-10-14 | Norbert Herfert | Process for Producing Surface Crosslinked Superabsorbents |
| CN101959538A (zh) * | 2008-03-05 | 2011-01-26 | 巴斯夫欧洲公司 | 制备超吸收剂的方法 |
| WO2009119754A1 (ja) | 2008-03-28 | 2009-10-01 | 株式会社日本触媒 | 吸水性樹脂の製造方法 |
| JP5290413B2 (ja) † | 2008-07-15 | 2013-09-18 | ビーエーエスエフ ソシエタス・ヨーロピア | 吸水性ポリマー粒子の製造方法 |
| CN102124039B (zh) | 2008-09-16 | 2013-04-24 | 株式会社日本触媒 | 吸水性树脂的制造方法和通液性提高方法 |
| CN104974358B (zh) | 2009-03-31 | 2018-11-23 | 株式会社日本触媒 | 颗粒状吸水性树脂的制造方法 |
| JP2012527502A (ja) * | 2009-05-18 | 2012-11-08 | ビーエーエスエフ ソシエタス・ヨーロピア | 吸水性ポリマー粒子のための被覆方法 |
| KR20110006771A (ko) | 2009-07-15 | 2011-01-21 | 주식회사 엘지화학 | 고흡수성 수지의 제조 방법 |
| WO2011034146A1 (ja) | 2009-09-16 | 2011-03-24 | 株式会社日本触媒 | 吸水性樹脂粉末の製造方法 |
| JP5731390B2 (ja) | 2009-09-30 | 2015-06-10 | 株式会社日本触媒 | ポリアクリル酸（塩）系吸水性樹脂およびその製造方法 |
| JP5647625B2 (ja) | 2009-12-24 | 2015-01-07 | 株式会社日本触媒 | ポリアクリル酸系吸水性樹脂粉末及びその製造方法 |
| EP2565219B1 (en) | 2010-04-27 | 2018-06-27 | Nippon Shokubai Co., Ltd. | Method for producing polyacrylic acid (salt)-based water absorbent resin powder |
| DE102010040921A1 (de) | 2010-09-16 | 2012-03-22 | Basf Se | Verfahren zur Herstellung von Acrylsäure aus Methanol und Essigsäure |
| DE102010040923A1 (de) | 2010-09-16 | 2012-03-22 | Basf Se | Verfahren zur Herstellung von Acrylsäure aus Ethanol und Formaldehyd |
| JP5722921B2 (ja) | 2011-01-28 | 2015-05-27 | 株式会社日本触媒 | ポリアクリル酸（塩）系吸水性樹脂粉末の製造方法 |
| EP2700667B1 (en) | 2011-04-20 | 2017-08-09 | Nippon Shokubai Co., Ltd. | Process and apparatus for producing water-absorbable resin of polyacrylic acid (salt) type |
| US9738769B2 (en) * | 2012-02-15 | 2017-08-22 | Basf Se | Water-absorbing polymer particles with high free swell rate and high permeability |
| US8945716B2 (en) * | 2012-06-19 | 2015-02-03 | Basf Se | Process for producing water-absorbing polymer particles |
| DE102012105440A1 (de) * | 2012-06-22 | 2013-12-24 | Chemische Fabrik Budenheim Kg | Feuchteregulierendes Material |
| KR102125105B1 (ko) | 2012-08-01 | 2020-06-19 | 가부시키가이샤 닛폰 쇼쿠바이 | 폴리아크릴산(염)계 흡수성 수지의 제조 방법 |
| US20150225514A1 (en) | 2012-09-11 | 2015-08-13 | Nippon Shokubai Co., Ltd. | Method for producing polyacrylic acid (salt)-based water absorbing agent, and water absorbing agent |
| EP2896454B1 (en) | 2012-09-11 | 2022-05-11 | Nippon Shokubai Co., Ltd. | Method for manufacturing polyacrylic acid (polyacrylate)-based absorbent, and absorbent |
| JP5996664B2 (ja) | 2012-10-01 | 2016-09-21 | 株式会社日本触媒 | 多元金属化合物からなる粉塵低減剤、多元金属化合物を含む吸水剤及びその製造方法 |
| JP6092236B2 (ja) | 2012-10-03 | 2017-03-08 | 株式会社日本触媒 | 吸水剤及びその製造方法 |
| US20140121403A1 (en) | 2012-10-31 | 2014-05-01 | Celanese International Corporation | Integrated Process for the Production of Acrylic Acids and Acrylates |
| CN104936997B (zh) | 2012-11-21 | 2017-09-12 | 巴斯夫欧洲公司 | 制备表面后交联吸水性聚合物颗粒的方法 |
| EP3085439B1 (en) | 2013-12-20 | 2023-10-04 | Nippon Shokubai Co., Ltd. | Water absorbing agent based on polyacrylic acid and/or a salt thereof |
| CN106132534B (zh) * | 2014-03-31 | 2020-06-19 | 株式会社日本触媒 | 颗粒状吸水剂及其制造方法 |
| KR101899924B1 (ko) | 2014-08-04 | 2018-09-18 | 주식회사 엘지화학 | 고흡수성 수지 및 이의 제조 방법 |
| CN106574006B (zh) * | 2014-10-08 | 2019-10-22 | 株式会社Lg化学 | 高吸水性树脂的制造方法 |
| KR101960042B1 (ko) * | 2016-03-24 | 2019-03-19 | 주식회사 엘지화학 | 고흡수성 수지의 제조 방법 및 이로부터 제조된 고흡수성 수지 |
| KR101959547B1 (ko) * | 2016-03-25 | 2019-03-18 | 주식회사 엘지화학 | 고흡수성 수지의 제조 방법 |
| JP7063634B2 (ja) * | 2017-01-23 | 2022-05-09 | 住友精化株式会社 | 架橋重合体の製造方法および吸水性樹脂の製造方法 |
| EP3391962A1 (en) * | 2017-04-19 | 2018-10-24 | The Procter & Gamble Company | Method for making water-absorbing polymer particles |
| JP7257090B2 (ja) * | 2018-03-29 | 2023-04-13 | Ｓｄｐグローバル株式会社 | 吸水性樹脂粒子及びその製造方法 |
| CN110790975A (zh) * | 2019-12-02 | 2020-02-14 | 承德石油高等专科学校 | 一种高静态吸水量除湿材料及其制备方法 |
| EP4474432A1 (en) | 2022-02-04 | 2024-12-11 | Nippon Shokubai Co., Ltd. | Method for producing water-absorbing resin containing recycled water-absorbing resin, and use thereof |
| WO2025033458A1 (ja) | 2023-08-09 | 2025-02-13 | 株式会社日本触媒 | 吸水性樹脂の回収方法 |
| CN121270758A (zh) * | 2025-12-11 | 2026-01-06 | 中国天辰工程有限公司 | 一种吸水性树脂的制备方法 |
Family Cites Families (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5525473A (en) * | 1978-08-14 | 1980-02-23 | Satsuki Kitani | Polymeric substance having swelling tendency |
| JPS598711A (ja) * | 1982-07-06 | 1984-01-18 | Sumitomo Chem Co Ltd | ヒドロゲルの製造法 |
| US4609311A (en) | 1983-09-23 | 1986-09-02 | Combustion Engineering, Inc. | Stud hole boring and tapping machine |
| DE4021847C2 (de) * | 1990-07-09 | 1994-09-08 | Stockhausen Chem Fab Gmbh | Verfahren zur Herstellung wasserquellbarer Produkte unter Verwendung von Feinstanteilen wasserquellbarer Polymerer |
| JP3145459B2 (ja) * | 1991-01-22 | 2001-03-12 | 株式会社日本触媒 | 吸水性樹脂の製造方法 |
| US5478879A (en) | 1991-01-22 | 1995-12-26 | Nippon Shokubai Co., Ltd. | Method for production of absorbent resin |
| US5342899A (en) | 1991-05-16 | 1994-08-30 | The Dow Chemical Company | Process for recycling aqueous fluid absorbents fines to a polymerizer |
| GB9413605D0 (en) * | 1994-07-06 | 1994-08-24 | American Colloid Co | Method of increasing the size and absorption under load of super-absorbent fine particles by impregnation with an aqueous acrylic monomer solution |
| US6599989B2 (en) * | 1998-03-03 | 2003-07-29 | Nippon Skokubai Co., Ltd. | Water-absorbent agents containing polycarboxylic amine chelating agents |
| JP2000007790A (ja) * | 1998-06-29 | 2000-01-11 | Nippon Shokubai Co Ltd | 吸水性樹脂の製造方法 |
| JP2001226416A (ja) * | 2000-02-15 | 2001-08-21 | Toagosei Co Ltd | 吸水性樹脂の製造方法 |
| BR0212696B1 (pt) | 2001-09-12 | 2013-02-05 | processo contÍnuo de polimerizaÇço para a preparaÇço de polÍmeros absorventes de Água, insoléveis em Água. | |
| US7193006B2 (en) | 2002-12-06 | 2007-03-20 | Nippon Shokubai Co., Ltd. | Process for continuous production of water-absorbent resin product |
-
2005
- 2005-12-29 DE DE102005062929A patent/DE102005062929A1/de not_active Withdrawn
-
2006
- 2006-12-28 DE DE502006005477T patent/DE502006005477D1/de active Active
- 2006-12-28 JP JP2008547970A patent/JP5091159B2/ja not_active Expired - Fee Related
- 2006-12-28 US US12/158,502 patent/US7786211B2/en not_active Expired - Fee Related
- 2006-12-28 CN CN2006800500491A patent/CN101389661B/zh not_active Expired - Fee Related
- 2006-12-28 EP EP06830841A patent/EP1969017B1/de not_active Not-in-force
- 2006-12-28 AT AT06830841T patent/ATE449793T1/de not_active IP Right Cessation
- 2006-12-28 WO PCT/EP2006/070250 patent/WO2007074167A2/de not_active Ceased
- 2006-12-29 TW TW095149952A patent/TW200732354A/zh unknown
-
2010
- 2010-08-23 US US12/861,338 patent/US8349946B2/en not_active Expired - Fee Related
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