JP2009522136A - 多層ポリマー積層体及びそれから製造される高強度積層体 - Google Patents
多層ポリマー積層体及びそれから製造される高強度積層体 Download PDFInfo
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- JP2009522136A JP2009522136A JP2008548685A JP2008548685A JP2009522136A JP 2009522136 A JP2009522136 A JP 2009522136A JP 2008548685 A JP2008548685 A JP 2008548685A JP 2008548685 A JP2008548685 A JP 2008548685A JP 2009522136 A JP2009522136 A JP 2009522136A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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Landscapes
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Abstract
Description
標準積層手順
積層体中の層が希望する順序で積み重ねられた予備プレス組立体を、真空バッグ中に入れ、90℃〜100℃で30分間加熱することで、予備プレス組立体の層の間に含まれる空気を除去する。その予備プレス組立体を、空気オートクレーブ中200psig(14.3バール)の圧力で135℃で30分間加熱する。次に、ガスを追加することなく空気を冷却することで、オートクレーブ内の圧力を低下させる。20分間冷却すると、空気の温度は約50℃未満となり、その後、過剰の圧力を排出し、積層体をオートクレーブから取り出す。
弾性率
すべての弾性率は、ASTM D 638−03(2003)に準拠して測定した。
曇り度は、積層体を透過する非散乱光の経路によって画定される軸から2.5度を超える角度で散乱する光束のパーセント値である。曇り度は、Columbia,MDのBYK−Gardner USAより入手可能なHazegardヘイズメーターを使用し、ASTM規格D1003−61の方法Aに一致するASTM規格NF−54−111に準拠して測定した。曇り度は、積層体の左側、積層体の中央、および積層体の右側で測定し、これらの測定値を平均して、各シート厚さにおける平均曇り度を求めた。
パーセント透過率は、UV−Vis分光計による350nm〜800nmの間の算術平均透過率を表している。
90度剥離強度接着試験法によって剥離試験を行った。Model SP−102B−3M90 SLIP/PEEL Tester(Instrumentors,Inc.,Strongsville,Ohio 44149)を使用して90度の角度で積層体を剥離した。積層体は5インチ/分の速度で剥離した。
ガラスビーム試料の入力インピーダンスを測定することによって音響損失係数を求めた。ガラス/多層ポリマー積層体/ガラス積層体、(約25mm×300mm)の中央を衝撃ボタン(直径15mm)上に置き、シアノアクリル接着剤で固定した。衝撃ボタンはインピーダンスヘッド上に支持されており、これは、衝撃ボタンによって試験体に測定された力を加えるために使用した。0〜7000Hzの間のホワイトノイズ型の力を使用して、試験体に力を加えた。次に、次式を使用して損失係数を計算した:
損失係数=Δfi/fresi
式中、Δfiは、最大インピーダンスよりも3dB小さいインピーダンスを有する共鳴曲線上の周波数の間の周波数差であり、およびfresiは共鳴周波数である。試験体は、測定前および測定中は所望の設定温度の環境室中に維持した。試料は、10℃、20℃、および30℃の温度で試験を行った。インピーダンスはダッシュポットに接続し、ダッシュポットは電力増幅器に接続し、電力増幅器は雑音発生器に接続した。インピーダンスは、FFTアナライザー/コンピューターセットアップによって測定した。このような方法は、たとえばISO 140試験プロトコルにまとめられている。
層A、B、およびCのすべてが、19重量パーセントのメタクリル酸を含み、37パーセントの量までナトリウムイオンで中和されたエチレン−コ−メタクリル酸コポリマーである、「剛直層−剛直層−剛直層」構造(層A/B/C)を有する多層ポリマー積層体を作製した。
ゾーン (℃)
供給 周囲温度
ゾーン1 180
ゾーン2 205
ゾーン3 210
ゾーン (℃)
供給 周囲温度
ゾーン1 170
ゾーン2 180
ゾーン3 206
ブロック 210
ダイ 210
ゾーン (℃)
供給 周囲温度
ゾーン1 170
ゾーン2 180
ゾーン3 205
1つのガラス層と、比較実験CE1で作製した多層ポリマー積層体とからなる積層体を以下の方法で作製した。比較実験CE1で作製した多層ポリマー積層体を、相対湿度(RH)8パーセント未満および温度72°Fで終夜コンディショニングした。順番に、アニールした透明フロートガラス板層、ガラス層のスズ側を多層ポリマー積層体と接触するようにした比較実験CE1で作製した多層ポリマー積層体、薄いTeflon(登録商標)フィルム層、およびアニールした透明フロートガラス層(各層の寸法は7インチ×3.5インチ(178mm×89mm);ガラス層の厚さ2.5mm;多層ポリマー積層体の厚さ30ミル(0.75mm))からなるガラス/多層ポリマー積層体/Teflon(登録商標)フィルム/ガラス予備プレス組立体を、標準積層手順により積層した。Teflon(登録商標)フィルムおよびガラスカバーシートを除去して、所望の積層体を得た。
比較実験CE2に記載の方法を使用して、1つのガラス層と、比較実験CE1で作製した多層ポリマー積層体とからなる積層体を作製したが、唯一の相違点は、比較実験CE1で作製した多層ポリマー積層体を、相対湿度(RH)23パーセントおよび温度72°Fで終夜コンディショニングした後に予備プレス組立体中に使用したことであった。
比較実験CE2に記載の方法を使用して、1つのガラス層と、比較実験CE1で作製した多層ポリマー積層体とからなる積層体を作製したが、唯一の相違点は、比較実験CE1で作製した多層ポリマー積層体を、相対湿度(RH)50パーセントおよび温度72°Fで終夜コンディショニングした後に予備プレス組立体中に使用したことであった。
1つのガラス層、比較実験CE1で作製した多層ポリマー積層体、および1つのガラス層とからなる積層体を以下の方法で作製した。比較実験CE1で作製した多層ポリマー積層体を、相対湿度(RH)23パーセントおよび温度72°Fで終夜コンディショニングした。順番に、アニールした透明フロートガラス板層、比較実験CE1で作製した多層ポリマー積層体、およびアニールした透明フロートガラス層(各層の寸法は12インチ×12インチ(305mm×305mm);ガラス層の厚さ2.15mm;多層ポリマー積層体の厚さ30ミル(0.75mm))からなるガラス/多層ポリマー積層体/ガラス予備プレス組立体を、標準積層手順により積層した。
「剛直層−剛直層−剛直層」構造(層A/B/C)を有する多層ポリマー積層体を、比較実験1に記載の方法を使用して作製したが、以下の相違点を有した。11重量パーセントのメタクリル酸および6重量パーセントのマレイン酸モノメチルエステルを含み、酸官能性の全量に基づいて40パーセントの量までナトリウムイオンと亜鉛イオンとの混合物で中和されたエチレン−コ−メタクリル酸−コ−マレイン酸モノメチルエステルターポリマーから層Aを形成した。19重量パーセントのメタクリル酸を含み、37パーセントの量までナトリウムイオンで中和されたエチレン−コ−メタクリル酸コポリマーから層Bを形成した。層Cは、層Aに使用したものと実質的に同じターポリマーから形成した。押出機Aの処理量は、スクリュー速度を70.0rpmに調整することによって制御した。押出機Bの処理量は、スクリュー速度を13.4rpmに調整することによって制御した。押出機Cの処理量は、スクリュー速度を14.6rpmに調整することによって制御した。3本ロールスタックに通した後、得られた多層ポリマー積層体を4.5フィート/分の速度で紙管上に巻き取った。
比較実験2に記載の方法を使用して、1つのガラス層と、比較実験CE6で作製した多層ポリマー積層体とからなる積層体を作製した。
比較実験3に記載の方法を使用して、1つのガラス層と、比較実験CE6で作製した多層ポリマー積層体とからなる積層体を作製した。
比較実験4に記載の方法を使用して、1つのガラス層と、比較実験CE6で作製した多層ポリマー積層体とからなる積層体を作製した。
比較実験5に記載の方法を使用して、1つのガラス層と、比較実験CE6で作製した多層ポリマー積層体と、1つのガラス層からなる積層体を作製した。
比較実験1に記載の方法を使用して、「軟質層−剛直層−軟質層」構造(層A/B/C)を有する多層ポリマー積層体を作製したが、以下の相違点を有した。9.6重量パーセントのメタクリル酸および23.5重量パーセントのアクリル酸n−ブチルを含み、52パーセントの量までナトリウムイオンで中和されたエチレン−コ−メタクリル酸−コ−アクリル酸n−ブチルターポリマーから層Aを形成した。19重量パーセントのメタクリル酸を含み、37パーセントの量までナトリウムイオンで中和されたエチレン−コ−メタクリル酸コポリマーから層Bを形成した。層Cは、層Aに使用したものと実質的に同じターポリマーから形成した。押出機Aの処理量は、スクリュー速度を70.5rpmに調整することによって制御した。押出機Bの処理量は、スクリュー速度を14.5rpmに調整することによって制御した。押出機Cの処理量は、スクリュー速度を15.1rpmに調整することによって制御した。3本ロールスタックに通した後、得られた多層ポリマー積層体を4.5フィート/分の速度で紙管上に巻き取った。
比較実験2に記載の方法を使用して、1つのガラス層と、比較実験CE11で作製した多層ポリマー積層体とからなる積層体を作製した。
比較実験3に記載の方法を使用して、1つのガラス層と、比較実験CE11で作製した多層ポリマー積層体とからなる積層体を作製した。
比較実験4に記載の方法を使用して、1つのガラス層と、比較実験CE11で作製した多層ポリマー積層体とからなる積層体を作製した。
比較実験5に記載の方法を使用して、1つのガラス層と、比較実験CE11で作製した多層ポリマー積層体と、1つのガラス層からなる積層体を作製した。
比較実験1に記載の方法を使用して、「剛直層−軟質層−剛直層」構造(層A/B/C)を有する多層ポリマー積層体を作製したが、以下の相違点を有した。19重量パーセントのメタクリル酸を含み、37パーセントの量までナトリウムイオンで中和されたエチレン−コ−メタクリル酸コポリマーから層Aを形成した。9.6重量パーセントのメタクリル酸および23.5重量パーセントのアクリル酸n−ブチルを含み、52パーセントの量までナトリウムイオンで中和されたエチレン−コ−メタクリル酸−コ−アクリル酸n−ブチルターポリマーから層Bを形成した。層Cは、層Aに使用したものと実質的に同じターポリマーから形成した。押出機Aの処理量は、スクリュー速度を70.6rpmに調整することによって制御した。押出機Bの処理量は、スクリュー速度を15.4rpmに調整することによって制御した。押出機Cの処理量は、スクリュー速度を14.3rpmに調整することによって制御した。3本ロールスタックに通した後、得られた多層ポリマー積層体を4.2フィート/分の速度で紙管上に巻き取った。
比較実験2に記載の方法を使用して、1つのガラス層と、実施例1で作製した多層ポリマー積層体とからなる積層体を作製した。
比較実験3に記載の方法を使用して、1つのガラス層と、実施例1で作製した多層ポリマー積層体とからなる積層体を作製した。
比較実験4に記載の方法を使用して、1つのガラス層と、実施例1で作製した多層ポリマー積層体とからなる積層体を作製した。
比較実験CE5に記載の方法を使用して、1つのガラス層と、実施例1で作製した多層ポリマー積層体と、1つのガラス層からなる積層体を作製した。
Claims (12)
- 2つの外層が内層のそれぞれの面上にあるように積層された3つのアイオノマー材料層を含む多層ポリマー積層体であって、前記アイオノマー材料のそれぞれが独立に、αオレフィンと、金属イオンで部分的に中和されたα,β−エチレン系不飽和カルボン酸とのコポリマーを含み、前記アイオノマー材料の内層が、約1,000psi(7MPa)〜約15,000psi(103MPa)の弾性率を有し、前記アイオノマー材料層のそれぞれが、少なくとも約1ミル(0.025mm)以上の厚さを有し、多層ポリマー積層体の全体の厚さが少なくとも約20ミル(0.5mm)以上である、多層ポリマー積層体。
- 前記アイオノマー材料の2つの外層のそれぞれが、約16,000psi(110MPa)〜約100,000psi(690MPa)の弾性率を有する、請求項1に記載の多層ポリマー積層体。
- 前記アイオノマー材料の2つの外層のそれぞれが、約30,000psi(207MPa)〜約80,000psi(552MPa)の弾性率を有し、前記アイオノマー材料の内層が、約3,000psi(21MPa)〜約10,000psi(69MPa)の弾性率を有する、請求項1に記載の高強度積層体。
- 前記αオレフィンと前記α,β−エチレン系不飽和カルボン酸とのコポリマーのそれぞれが独立に、約0.1〜約30重量パーセントの前記α,β−エチレン系不飽和カルボン酸成分を含み、前記アイオノマー材料のそれぞれは独立に、全カルボン酸含有率を基準にして約5〜約100パーセントが金属イオンで中和されている、請求項1に記載の多層ポリマー積層体。
- 前記アイオノマー材料の2つの外層のそれぞれが、約1,000psi(7MPa)〜約15,000psi(103MPa)の弾性率を有する、請求項1に記載の多層ポリマー積層体。
- 2つの剛性シートと、2つの外層が内層のそれぞれの面上にあるように積層された3つのアイオノマー材料層を含む多層ポリマー積層体とを含む高強度積層体であって、前記アイオノマー材料のそれぞれが独立に、αオレフィンと、金属イオンで部分的に中和されたα,β−エチレン系不飽和カルボン酸とのコポリマーを含み、前記アイオノマー材料の内層が、約1,000psi(7MPa)〜約15,000psi(103MPa)の弾性率を有し、前記アイオノマー材料層のそれぞれが、少なくとも約1ミル(0.025mm)以上の厚さを有し、前記多層ポリマー積層体の全体の厚さが少なくとも約20ミル(0.5mm)以上であり、前記2つの剛性シートが前記多層ポリマー積層体の反対側の面上に配置されている、高強度積層体。
- 前記剛性シートがガラスである、請求項6に記載の高強度積層体。
- 前記アイオノマー材料の2つの外層のそれぞれが、約16,000psi(110MPa)〜約100,000psi(690MPa)の弾性率を有する、請求項6に記載の高強度積層体。
- 前記アイオノマー材料の2つの外層のそれぞれが、約30,000psi(207MPa)〜約80,000psi(552MPa)の弾性率を有し、前記アイオノマー材料の内層が、約3,000psi(21MPa)〜約10,000psi(69MPa)の弾性率を有する、請求項6に記載の高強度積層体。
- 前記αオレフィンと前記α,β−エチレン系不飽和カルボン酸とのコポリマーのそれぞれが独立に、約0.1〜約30重量パーセントの前記α,β−エチレン系不飽和カルボン酸成分を含み、前記アイオノマー材料のそれぞれは独立に、全カルボン酸含有率を基準にして約5〜約100パーセントが金属イオンで中和されている、請求項6に記載の高強度積層体。
- 前記ガラス剛性シートの一方と前記多層ポリマー積層体との間に配置されたポリマーフィルムまたはシートをさらに含む、請求項7に記載の高強度積層体。
- 前記アイオノマー材料の2つの外層のそれぞれが約1,000psi(7MPa)〜約15,000psi(103MPa)の弾性率を有する、請求項6に記載の高強度積層体。
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Also Published As
Publication number | Publication date |
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US8101267B2 (en) | 2012-01-24 |
WO2007079091A1 (en) | 2007-07-12 |
EP1979159A1 (en) | 2008-10-15 |
EP1979159B1 (en) | 2016-02-17 |
US20070154694A1 (en) | 2007-07-05 |
CN101389472A (zh) | 2009-03-18 |
AU2006332769A1 (en) | 2007-07-12 |
CN101389472B (zh) | 2013-04-10 |
JP5001954B2 (ja) | 2012-08-15 |
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