JP2008528422A5 - - Google Patents
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- Publication number
- JP2008528422A5 JP2008528422A5 JP2007552566A JP2007552566A JP2008528422A5 JP 2008528422 A5 JP2008528422 A5 JP 2008528422A5 JP 2007552566 A JP2007552566 A JP 2007552566A JP 2007552566 A JP2007552566 A JP 2007552566A JP 2008528422 A5 JP2008528422 A5 JP 2008528422A5
- Authority
- JP
- Japan
- Prior art keywords
- cesium
- solution
- alum
- process according
- ore
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000000034 method Methods 0.000 claims 32
- 239000000243 solution Substances 0.000 claims 19
- FLJPGEWQYJVDPF-UHFFFAOYSA-L caesium sulfate Chemical compound [Cs+].[Cs+].[O-]S([O-])(=O)=O FLJPGEWQYJVDPF-UHFFFAOYSA-L 0.000 claims 14
- VHUJINUACVEASK-UHFFFAOYSA-J aluminum;cesium;disulfate;dodecahydrate Chemical compound O.O.O.O.O.O.O.O.O.O.O.O.[Al+3].[Cs+].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O VHUJINUACVEASK-UHFFFAOYSA-J 0.000 claims 11
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 10
- 238000010411 cooking Methods 0.000 claims 8
- 229910052792 caesium Inorganic materials 0.000 claims 7
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 claims 7
- 239000011541 reaction mixture Substances 0.000 claims 7
- MFGOFGRYDNHJTA-UHFFFAOYSA-N 2-amino-1-(2-fluorophenyl)ethanol Chemical compound NCC(O)C1=CC=CC=C1F MFGOFGRYDNHJTA-UHFFFAOYSA-N 0.000 claims 4
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims 4
- 229910052782 aluminium Inorganic materials 0.000 claims 4
- HUCVOHYBFXVBRW-UHFFFAOYSA-M caesium hydroxide Inorganic materials [OH-].[Cs+] HUCVOHYBFXVBRW-UHFFFAOYSA-M 0.000 claims 4
- 239000007787 solid Substances 0.000 claims 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 4
- 239000002253 acid Substances 0.000 claims 3
- 238000001816 cooling Methods 0.000 claims 3
- 230000029087 digestion Effects 0.000 claims 3
- 238000002156 mixing Methods 0.000 claims 3
- RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical compound [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 claims 2
- 229910001863 barium hydroxide Inorganic materials 0.000 claims 2
- 238000002425 crystallisation Methods 0.000 claims 2
- 230000008025 crystallization Effects 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- 239000012452 mother liquor Substances 0.000 claims 2
- 238000001953 recrystallisation Methods 0.000 claims 2
- 238000000926 separation method Methods 0.000 claims 2
- 229940037003 alum Drugs 0.000 claims 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 claims 1
- LYADUWZTFLUWGI-UHFFFAOYSA-J aluminum;cesium;disulfate;hydrate Chemical compound O.[Al+3].[Cs+].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O LYADUWZTFLUWGI-UHFFFAOYSA-J 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 238000009835 boiling Methods 0.000 claims 1
- 239000012141 concentrate Substances 0.000 claims 1
- 238000010790 dilution Methods 0.000 claims 1
- 239000012895 dilution Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 239000002245 particle Substances 0.000 claims 1
- 239000002244 precipitate Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
- UUCCCPNEFXQJEL-UHFFFAOYSA-L strontium dihydroxide Chemical compound [OH-].[OH-].[Sr+2] UUCCCPNEFXQJEL-UHFFFAOYSA-L 0.000 claims 1
- 229910001866 strontium hydroxide Inorganic materials 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102005003999 | 2005-01-27 | ||
| DE102005003999.5 | 2005-01-27 | ||
| PCT/EP2006/000634 WO2006079514A1 (de) | 2005-01-27 | 2006-01-25 | Verfahren zur herstellung von cesiumhydroxidlösungen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2008528422A JP2008528422A (ja) | 2008-07-31 |
| JP2008528422A5 true JP2008528422A5 (enExample) | 2012-11-01 |
| JP5424562B2 JP5424562B2 (ja) | 2014-02-26 |
Family
ID=35985438
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2007552566A Active JP5424562B2 (ja) | 2005-01-27 | 2006-01-25 | 水酸化セシウム溶液の製造法 |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US20080166281A1 (enExample) |
| EP (1) | EP1843977B1 (enExample) |
| JP (1) | JP5424562B2 (enExample) |
| KR (1) | KR20070095439A (enExample) |
| CN (1) | CN101107199A (enExample) |
| BR (1) | BRPI0607265A2 (enExample) |
| CA (1) | CA2595622C (enExample) |
| DK (1) | DK1843977T3 (enExample) |
| MX (1) | MX2007009038A (enExample) |
| RU (1) | RU2408534C2 (enExample) |
| UA (1) | UA92905C2 (enExample) |
| WO (1) | WO2006079514A1 (enExample) |
| ZA (1) | ZA200707251B (enExample) |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101774613B (zh) * | 2010-02-04 | 2011-11-30 | 江西东鹏新材料有限责任公司 | 以铯榴石生产碳酸铯的新工艺 |
| CN102230081B (zh) * | 2011-04-23 | 2012-11-21 | 大悟华龙吕王石材有限公司 | 一种从钾长石中提取钾、铝、硅元素的酸浸方法 |
| CN103803589B (zh) * | 2014-03-04 | 2015-08-19 | 湖北百杰瑞新材料股份有限公司 | 一种高纯硫酸铯的制备方法 |
| WO2017127936A1 (en) * | 2016-01-29 | 2017-08-03 | Cascadero Copper Corporation | Recovery of cesium from epithermal mineral deposits |
| CN105540621B (zh) * | 2016-03-16 | 2017-05-03 | 江西东鹏新材料有限责任公司 | 一种生产氟化铯的方法 |
| CN107140662B (zh) * | 2017-05-05 | 2019-03-01 | 江西东鹏新材料有限责任公司 | 一种生产氢氧化铯的新方法 |
| CN107698443A (zh) * | 2017-09-19 | 2018-02-16 | 江西东鹏新材料有限责任公司 | 一种甲酸铷铯及其制备工艺、应用 |
| JP7083276B2 (ja) * | 2018-05-22 | 2022-06-10 | Ｕｂｅ株式会社 | セシウムの回収方法 |
| WO2020073079A1 (en) * | 2018-10-10 | 2020-04-16 | Li-Technology Pty Ltd | Brine and method for producing same |
| CN113528822B (zh) * | 2020-11-19 | 2022-04-08 | 江西理工大学 | 一种从高碱性溶液回收钨钼钒并再生氢氧化钠的方法 |
| KR102390682B1 (ko) * | 2021-10-28 | 2022-04-27 | 한국지질자원연구원 | 폐황산바나듐 촉매로부터 바나듐 및 세슘의 선택적인 회수방법 및 이를 통해 제조된 고품위 바나듐 수용액과 세슘알럼 |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3207571A (en) * | 1962-04-09 | 1965-09-21 | San Antonio Chemicals Inc | Process for preparing cesium compounds from cesium alum |
| US3489509A (en) * | 1967-05-18 | 1970-01-13 | Kewanee Oil Co | Process for recovery of cesium compounds of high purity |
| DD268925A1 (de) * | 1986-12-16 | 1989-06-14 | Freiberg Bergakademie | Verfahren zur herstellung von caesiumhydroxid aus caesiumalaun |
| RU2070426C1 (ru) * | 1993-02-23 | 1996-12-20 | Татьяна Андреевна Седнева | Способ получения гидроксида цезия или рубидия и кислоты |
| DE4313480C1 (de) * | 1993-04-24 | 1994-04-14 | Metallgesellschaft Ag | Verfahren zur Herstellung von Cäsiumsalzen aus Cäsium-Aluminium-Alaun |
| US6015535A (en) * | 1995-04-06 | 2000-01-18 | Cabot Corporation | Process for producing purified cesium compound from cesium alum |
| US6652820B2 (en) * | 2001-04-02 | 2003-11-25 | Cabot Corporation | Methods of making cesium salts and other alkali metal salts |
-
2006
- 2006-01-25 BR BRPI0607265-8A patent/BRPI0607265A2/pt not_active Application Discontinuation
- 2006-01-25 UA UAA200709677A patent/UA92905C2/ru unknown
- 2006-01-25 DK DK06703807.5T patent/DK1843977T3/da active
- 2006-01-25 CA CA2595622A patent/CA2595622C/en active Active
- 2006-01-25 US US11/795,855 patent/US20080166281A1/en not_active Abandoned
- 2006-01-25 RU RU2007132122/05A patent/RU2408534C2/ru active
- 2006-01-25 MX MX2007009038A patent/MX2007009038A/es active IP Right Grant
- 2006-01-25 ZA ZA200707251A patent/ZA200707251B/xx unknown
- 2006-01-25 KR KR1020077019195A patent/KR20070095439A/ko not_active Ceased
- 2006-01-25 WO PCT/EP2006/000634 patent/WO2006079514A1/de not_active Ceased
- 2006-01-25 EP EP06703807.5A patent/EP1843977B1/de active Active
- 2006-01-25 CN CNA2006800032472A patent/CN101107199A/zh active Pending
- 2006-01-25 JP JP2007552566A patent/JP5424562B2/ja active Active
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