JP2005506274A - 微粒状エマルション - Google Patents

Info

Publication number

JP2005506274A

JP2005506274A JP2002545650A JP2002545650A JP2005506274A JP 2005506274 A JP2005506274 A JP 2005506274A JP 2002545650 A JP2002545650 A JP 2002545650A JP 2002545650 A JP2002545650 A JP 2002545650A JP 2005506274 A JP2005506274 A JP 2005506274A

Authority

JP

Japan

Prior art keywords

acid

fatty

polyglyceryl

branched

esters

Prior art date

2000-11-30

Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)

Pending

Links

• Espacenet
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• 239000000839 emulsion Substances 0.000 title claims abstract description 35
• 239000003995 emulsifying agent Substances 0.000 claims abstract description 24
• 239000002245 particle Substances 0.000 claims abstract description 20
• XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
• 238000004519 manufacturing process Methods 0.000 claims abstract description 4
• -1 fatty alcohol esters Chemical class 0.000 claims description 77
• 239000000194 fatty acid Substances 0.000 claims description 53
• 235000014113 dietary fatty acids Nutrition 0.000 claims description 52
• 229930195729 fatty acid Natural products 0.000 claims description 52
• 150000004665 fatty acids Chemical class 0.000 claims description 38
• 239000003921 oil Substances 0.000 claims description 34
• 235000019198 oils Nutrition 0.000 claims description 34
• 238000000034 method Methods 0.000 claims description 28
• 125000004432 carbon atom Chemical group C* 0.000 claims description 27
• 239000000203 mixture Substances 0.000 claims description 25
• 150000002148 esters Chemical class 0.000 claims description 23
• 238000000265 homogenisation Methods 0.000 claims description 22
• 150000002191 fatty alcohols Chemical class 0.000 claims description 17
• 125000000217 alkyl group Chemical group 0.000 claims description 15
• LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
• 229920005862 polyol Polymers 0.000 claims description 12
• 150000003077 polyols Chemical class 0.000 claims description 11
• 150000001298 alcohols Chemical class 0.000 claims description 9
• 239000004359 castor oil Substances 0.000 claims description 9
• 235000019438 castor oil Nutrition 0.000 claims description 9
• ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 9
• 239000002537 cosmetic Substances 0.000 claims description 8
• 241000209140 Triticum Species 0.000 claims description 7
• 235000021307 Triticum Nutrition 0.000 claims description 7
• 108090000623 proteins and genes Proteins 0.000 claims description 7
• 102000004169 proteins and genes Human genes 0.000 claims description 7
• 239000002253 acid Substances 0.000 claims description 6
• RMTFNDVZYPHUEF-XZBKPIIZSA-N 3-O-methyl-D-glucose Chemical compound O=C[C@H](O)[C@@H](OC)[C@H](O)[C@H](O)CO RMTFNDVZYPHUEF-XZBKPIIZSA-N 0.000 claims description 5
• 239000007788 liquid Substances 0.000 claims description 5
• ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 5
• 229930195733 hydrocarbon Natural products 0.000 claims description 4
• 150000002430 hydrocarbons Chemical class 0.000 claims description 4
• 229940049964 oleate Drugs 0.000 claims description 4
• 239000000825 pharmaceutical preparation Substances 0.000 claims description 4
• 229910052708 sodium Inorganic materials 0.000 claims description 4
• 239000011734 sodium Substances 0.000 claims description 4
• 150000005846 sugar alcohols Polymers 0.000 claims description 4
• 125000001931 aliphatic group Chemical group 0.000 claims description 3
• 235000013871 bee wax Nutrition 0.000 claims description 3
• 239000012166 beeswax Substances 0.000 claims description 3
• GHVNFZFCNZKVNT-UHFFFAOYSA-M decanoate Chemical compound CCCCCCCCCC([O-])=O GHVNFZFCNZKVNT-UHFFFAOYSA-M 0.000 claims description 3
• 238000002156 mixing Methods 0.000 claims description 3
• 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
• 229940048845 polyglyceryl-3 diisostearate Drugs 0.000 claims description 3
• 238000007142 ring opening reaction Methods 0.000 claims description 3
• UFTFJSFQGQCHQW-UHFFFAOYSA-N triformin Chemical compound O=COCC(OC=O)COC=O UFTFJSFQGQCHQW-UHFFFAOYSA-N 0.000 claims description 3
• RZRNAYUHWVFMIP-KTKRTIGZSA-N 1-oleoylglycerol Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OCC(O)CO RZRNAYUHWVFMIP-KTKRTIGZSA-N 0.000 claims description 2
• XDOFQFKRPWOURC-UHFFFAOYSA-N 16-methylheptadecanoic acid Chemical compound CC(C)CCCCCCCCCCCCCCC(O)=O XDOFQFKRPWOURC-UHFFFAOYSA-N 0.000 claims description 2
• HOSGXJWQVBHGLT-UHFFFAOYSA-N 6-hydroxy-3,4-dihydro-1h-quinolin-2-one Chemical group N1C(=O)CCC2=CC(O)=CC=C21 HOSGXJWQVBHGLT-UHFFFAOYSA-N 0.000 claims description 2
• BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims description 2
• DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 2
• CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 2
• 229930006000 Sucrose Natural products 0.000 claims description 2
• PHYFQTYBJUILEZ-UHFFFAOYSA-N Trioleoylglycerol Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC(OC(=O)CCCCCCCC=CCCCCCCCC)COC(=O)CCCCCCCC=CCCCCCCCC PHYFQTYBJUILEZ-UHFFFAOYSA-N 0.000 claims description 2
• UFVWHIGSVGIZRQ-UHFFFAOYSA-N bis(2-ethylhexyl) naphthalene-2,6-dicarboxylate Chemical compound C1=C(C(=O)OCC(CC)CCCC)C=CC2=CC(C(=O)OCC(CC)CCCC)=CC=C21 UFVWHIGSVGIZRQ-UHFFFAOYSA-N 0.000 claims description 2
• 229940085262 cetyl dimethicone Drugs 0.000 claims description 2
• 150000001983 dialkylethers Chemical class 0.000 claims description 2
• 150000001991 dicarboxylic acids Chemical class 0.000 claims description 2
• 239000006185 dispersion Substances 0.000 claims description 2
• 229940100518 polyglyceryl-4 isostearate Drugs 0.000 claims description 2
• RMGVATURDVPNOZ-UHFFFAOYSA-M potassium;hexadecyl hydrogen phosphate Chemical compound [K+].CCCCCCCCCCCCCCCCOP(O)([O-])=O RMGVATURDVPNOZ-UHFFFAOYSA-M 0.000 claims description 2
• 150000003138 primary alcohols Chemical class 0.000 claims description 2
• 229920002545 silicone oil Polymers 0.000 claims description 2
• 239000005720 sucrose Substances 0.000 claims description 2
• 150000003626 triacylglycerols Chemical class 0.000 claims description 2
• 235000015112 vegetable and seed oil Nutrition 0.000 claims description 2
• 239000008158 vegetable oil Substances 0.000 claims description 2
• 150000001733 carboxylic acid esters Chemical class 0.000 claims 1
• 125000000113 cyclohexyl group Chemical class [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 claims 1
• 229940052296 esters of benzoic acid for local anesthesia Drugs 0.000 claims 1
• RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 27
• 239000001993 wax Substances 0.000 description 22
• PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 17
• 235000002639 sodium chloride Nutrition 0.000 description 16
• 239000003795 chemical substances by application Substances 0.000 description 15
• 150000003839 salts Chemical class 0.000 description 14
• 239000000126 substance Substances 0.000 description 14
• CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 12
• 150000001875 compounds Chemical class 0.000 description 12
• 239000000047 product Substances 0.000 description 12
• 238000009826 distribution Methods 0.000 description 11
• 229920001296 polysiloxane Polymers 0.000 description 10
• 229920001577 copolymer Polymers 0.000 description 9
• 239000012071 phase Substances 0.000 description 9
• 229920000642 polymer Polymers 0.000 description 9
• 229920000151 polyglycol Polymers 0.000 description 8
• 239000010695 polyglycol Substances 0.000 description 8
• IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 7
• IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 7
• 239000000975 dye Substances 0.000 description 7
• 239000003925 fat Substances 0.000 description 7
• 235000019197 fats Nutrition 0.000 description 7
• 235000011187 glycerol Nutrition 0.000 description 7
• 239000002304 perfume Substances 0.000 description 7
• 239000004094 surface-active agent Substances 0.000 description 7
• DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
• QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 6
• 125000002091 cationic group Chemical group 0.000 description 6
• 239000010419 fine particle Substances 0.000 description 6
• 239000000787 lecithin Substances 0.000 description 6
• 229940067606 lecithin Drugs 0.000 description 6
• 235000010445 lecithin Nutrition 0.000 description 6
• 238000002360 preparation method Methods 0.000 description 6
• 235000018102 proteins Nutrition 0.000 description 6
• 238000004945 emulsification Methods 0.000 description 5
• 108090000765 processed proteins & peptides Proteins 0.000 description 5
• 102000004196 processed proteins & peptides Human genes 0.000 description 5
• 239000002562 thickening agent Substances 0.000 description 5
• JNYAEWCLZODPBN-JGWLITMVSA-N (2r,3r,4s)-2-[(1r)-1,2-dihydroxyethyl]oxolane-3,4-diol Chemical compound OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O JNYAEWCLZODPBN-JGWLITMVSA-N 0.000 description 4
• WRMNZCZEMHIOCP-UHFFFAOYSA-N 2-phenylethanol Chemical compound OCCC1=CC=CC=C1 WRMNZCZEMHIOCP-UHFFFAOYSA-N 0.000 description 4
• GLZPCOQZEFWAFX-UHFFFAOYSA-N Geraniol Chemical compound CC(C)=CCCC(C)=CCO GLZPCOQZEFWAFX-UHFFFAOYSA-N 0.000 description 4
• 229910019142 PO4 Inorganic materials 0.000 description 4
• NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 4
• GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 4
• XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 4
• 150000001412 amines Chemical class 0.000 description 4
• 235000010323 ascorbic acid Nutrition 0.000 description 4
• 239000011668 ascorbic acid Substances 0.000 description 4
• XNEFYCZVKIDDMS-UHFFFAOYSA-N avobenzone Chemical compound C1=CC(OC)=CC=C1C(=O)CC(=O)C1=CC=C(C(C)(C)C)C=C1 XNEFYCZVKIDDMS-UHFFFAOYSA-N 0.000 description 4
• TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 4
• WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 4
• ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical compound C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 description 4
• QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 description 4
• 230000000035 biogenic effect Effects 0.000 description 4
• QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 description 4
• 150000002170 ethers Chemical class 0.000 description 4
• 150000002576 ketones Chemical class 0.000 description 4
• CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 description 4
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• 229920001223 polyethylene glycol Polymers 0.000 description 4
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• YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 description 4
• 239000003381 stabilizer Substances 0.000 description 4
• 230000008961 swelling Effects 0.000 description 4
• 239000000341 volatile oil Substances 0.000 description 4
• ULQISTXYYBZJSJ-UHFFFAOYSA-N 12-hydroxyoctadecanoic acid Chemical compound CCCCCCC(O)CCCCCCCCCCC(O)=O ULQISTXYYBZJSJ-UHFFFAOYSA-N 0.000 description 3
• 239000004808 2-ethylhexylester Substances 0.000 description 3
• FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 3
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• KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 3
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• 239000004166 Lanolin Substances 0.000 description 3
• WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical group C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 description 3
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• YBGZDTIWKVFICR-JLHYYAGUSA-N Octyl 4-methoxycinnamic acid Chemical compound CCCCC(CC)COC(=O)\C=C\C1=CC=C(OC)C=C1 YBGZDTIWKVFICR-JLHYYAGUSA-N 0.000 description 3
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• 229920002125 Sokalan® Polymers 0.000 description 3
• 235000021355 Stearic acid Nutrition 0.000 description 3
• ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 3
• 239000000654 additive Substances 0.000 description 3
• 125000003342 alkenyl group Chemical group 0.000 description 3
• FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 3
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• 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 3
• QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 3
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• 125000001117 oleyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])/C([H])=C([H])\C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 3
• 230000036961 partial effect Effects 0.000 description 3
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• 230000005501 phase interface Effects 0.000 description 3
• 150000003904 phospholipids Chemical class 0.000 description 3
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• PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 description 3
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• 239000002023 wood Substances 0.000 description 3
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• DSEKYWAQQVUQTP-XEWMWGOFSA-N (2r,4r,4as,6as,6as,6br,8ar,12ar,14as,14bs)-2-hydroxy-4,4a,6a,6b,8a,11,11,14a-octamethyl-2,4,5,6,6a,7,8,9,10,12,12a,13,14,14b-tetradecahydro-1h-picen-3-one Chemical compound C([C@H]1[C@]2(C)CC[C@@]34C)C(C)(C)CC[C@]1(C)CC[C@]2(C)[C@H]4CC[C@@]1(C)[C@H]3C[C@@H](O)C(=O)[C@@H]1C DSEKYWAQQVUQTP-XEWMWGOFSA-N 0.000 description 2
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• BZANQLIRVMZFOS-ZKZCYXTQSA-N (3r,4s,5s,6r)-2-butoxy-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound CCCCOC1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O BZANQLIRVMZFOS-ZKZCYXTQSA-N 0.000 description 2
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• FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 2
• KIHBGTRZFAVZRV-UHFFFAOYSA-N 2-Hydroxyoctadecanoic acid Natural products CCCCCCCCCCCCCCCCC(O)C(O)=O KIHBGTRZFAVZRV-UHFFFAOYSA-N 0.000 description 2
• YIWUKEYIRIRTPP-UHFFFAOYSA-N 2-ethylhexan-1-ol Chemical compound CCCCC(CC)CO YIWUKEYIRIRTPP-UHFFFAOYSA-N 0.000 description 2
• SVTBMSDMJJWYQN-UHFFFAOYSA-N 2-methylpentane-2,4-diol Chemical compound CC(O)CC(C)(C)O SVTBMSDMJJWYQN-UHFFFAOYSA-N 0.000 description 2
• 235000007173 Abies balsamea Nutrition 0.000 description 2
• KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical class CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 2
• NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
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