JP2004513089A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2004513089A5 JP2004513089A5 JP2002531072A JP2002531072A JP2004513089A5 JP 2004513089 A5 JP2004513089 A5 JP 2004513089A5 JP 2002531072 A JP2002531072 A JP 2002531072A JP 2002531072 A JP2002531072 A JP 2002531072A JP 2004513089 A5 JP2004513089 A5 JP 2004513089A5
- Authority
- JP
- Japan
- Prior art keywords
- ppm
- dtpa
- stabilizer
- liquid phase
- concentration
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000034 method Methods 0.000 description 17
- 239000003381 stabilizer Substances 0.000 description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 5
- 239000007791 liquid phase Substances 0.000 description 5
- QPCDCPDFJACHGM-UHFFFAOYSA-N N,N-bis{2-[bis(carboxymethyl)amino]ethyl}glycine Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(=O)O)CCN(CC(O)=O)CC(O)=O QPCDCPDFJACHGM-UHFFFAOYSA-N 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 229960003330 pentetic acid Drugs 0.000 description 4
- 239000003352 sequestering agent Substances 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 239000000178 monomer Substances 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- NWVVVBRKAWDGAB-UHFFFAOYSA-N p-methoxyphenol Chemical compound COC1=CC=C(O)C=C1 NWVVVBRKAWDGAB-UHFFFAOYSA-N 0.000 description 3
- UZFMOKQJFYMBGY-UHFFFAOYSA-N 4-hydroxy-TEMPO Chemical compound CC1(C)CC(O)CC(C)(C)N1[O] UZFMOKQJFYMBGY-UHFFFAOYSA-N 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N 1,4-Benzenediol Natural products OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 1
- WJFKNYWRSNBZNX-UHFFFAOYSA-N 10H-phenothiazine Chemical compound C1=CC=C2NC3=CC=CC=C3SC2=C1 WJFKNYWRSNBZNX-UHFFFAOYSA-N 0.000 description 1
- FCKYPQBAHLOOJQ-UWVGGRQHSA-N 2-[[(1s,2s)-2-[bis(carboxymethyl)amino]cyclohexyl]-(carboxymethyl)amino]acetic acid Chemical compound OC(=O)CN(CC(O)=O)[C@H]1CCCC[C@@H]1N(CC(O)=O)CC(O)=O FCKYPQBAHLOOJQ-UWVGGRQHSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- MWUXSHHQAYIFBG-UHFFFAOYSA-N Nitric oxide Chemical class O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- IXPUJMULXNNEHS-UHFFFAOYSA-L copper;n,n-dibutylcarbamodithioate Chemical compound [Cu+2].CCCCN(C([S-])=S)CCCC.CCCCN(C([S-])=S)CCCC IXPUJMULXNNEHS-UHFFFAOYSA-L 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 229960004337 hydroquinone Drugs 0.000 description 1
- 125000000687 hydroquinonyl group Chemical group C1(O)=C(C=C(O)C=C1)* 0.000 description 1
- 229940071125 manganese acetate Drugs 0.000 description 1
- UOGMEBQRZBEZQT-UHFFFAOYSA-L manganese(2+);diacetate Chemical compound [Mn+2].CC([O-])=O.CC([O-])=O UOGMEBQRZBEZQT-UHFFFAOYSA-L 0.000 description 1
- 229960003505 mequinol Drugs 0.000 description 1
- CXKWCBBOMKCUKX-UHFFFAOYSA-M methylene blue Chemical compound [Cl-].C1=CC(N(C)C)=CC2=[S+]C3=CC(N(C)C)=CC=C3N=C21 CXKWCBBOMKCUKX-UHFFFAOYSA-M 0.000 description 1
- 229960000907 methylthioninium chloride Drugs 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 229950000688 phenothiazine Drugs 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 150000004897 thiazines Chemical class 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- -1 transition metal salts Chemical class 0.000 description 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR0012422A FR2814741B1 (fr) | 2000-09-29 | 2000-09-29 | Procede de stabilisation de monomeres acryliques |
| PCT/FR2001/002965 WO2002026685A1 (fr) | 2000-09-29 | 2001-09-25 | Procede de stabilisation de monomeres acryliques |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2004513089A JP2004513089A (ja) | 2004-04-30 |
| JP2004513089A5 true JP2004513089A5 (https=) | 2008-11-06 |
Family
ID=8854820
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2002531072A Withdrawn JP2004513089A (ja) | 2000-09-29 | 2001-09-25 | アクリルモノマーの安定化法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20040011638A1 (https=) |
| EP (1) | EP1324969A1 (https=) |
| JP (1) | JP2004513089A (https=) |
| KR (1) | KR100806558B1 (https=) |
| CN (1) | CN1250509C (https=) |
| AU (1) | AU2001291986A1 (https=) |
| FR (1) | FR2814741B1 (https=) |
| WO (1) | WO2002026685A1 (https=) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10339633A1 (de) * | 2002-10-17 | 2004-04-29 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäure und (Meth)acrylsäureestern |
| JP2005343845A (ja) * | 2004-06-04 | 2005-12-15 | Hakuto Co Ltd | アクリロニトリルの重合抑制剤および重合抑制方法 |
| JP4959158B2 (ja) * | 2005-08-05 | 2012-06-20 | 旭化成ケミカルズ株式会社 | アクリロニトリルの分離回収方法 |
| EP2135656A1 (en) * | 2008-05-30 | 2009-12-23 | Rohm and Haas Company | Method for production of purified (Meth)acrylic acid |
| DE102012223695A1 (de) * | 2012-12-19 | 2014-06-26 | Basf Se | Verfahren zur Stabilisierung von polymerisationsfähigen Verbindungen |
| EP3426287A4 (en) | 2016-03-09 | 2020-03-11 | Los Angeles Biomedical Research Institute at Harbor-UCLA Medical Center | Methods and kits for use in preventing and treating vulvovaginal candidiasis |
| CN111051488B (zh) * | 2017-08-31 | 2021-11-26 | 富士胶片株式会社 | 药液的纯化方法及药液 |
| JP7159453B2 (ja) | 2018-08-24 | 2022-10-24 | ビーエル テクノロジーズ、インコーポレイテッド | 重合を阻害するための相乗的組み合わせ |
| US20250263387A1 (en) | 2022-03-25 | 2025-08-21 | Mitsubishi Gas Chemical Company, Inc. | Method for purifying (meth)acrylic acid monomer and/or (meth)acrylic acid ester monomer |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1601979A (en) * | 1978-01-06 | 1981-11-04 | Rohm & Haas | Polymerization inhibition |
| US4929660A (en) * | 1986-03-14 | 1990-05-29 | The Kendall Company | Acrylic adhesive compositions having improved stability |
| JP2758780B2 (ja) * | 1992-04-15 | 1998-05-28 | 株式会社クラレ | （メタ）アクリル酸の重合防止方法 |
| JP3197947B2 (ja) * | 1992-05-21 | 2001-08-13 | 株式会社クラレ | （メタ）アクリル酸の重合防止法 |
| TW294658B (https=) * | 1994-06-02 | 1997-01-01 | Nippon Catalytic Chem Ind | |
| FR2750696B1 (fr) * | 1996-07-08 | 1998-10-30 | Atochem Elf Sa | Solutions aqueuses stabilisees de sels d'ammoniums quaternaires insatures |
| DE19920796A1 (de) * | 1999-05-06 | 2000-11-09 | Roehm Gmbh | Verfahren zur Herstellung von Isobornylmethacrylat |
| FR2801306B1 (fr) * | 1999-11-24 | 2001-12-28 | Atofina | Procede de purification des monomeres (meth) acryliques par distillation |
-
2000
- 2000-09-29 FR FR0012422A patent/FR2814741B1/fr not_active Expired - Fee Related
-
2001
- 2001-09-25 KR KR1020037004262A patent/KR100806558B1/ko not_active Expired - Fee Related
- 2001-09-25 CN CNB018166059A patent/CN1250509C/zh not_active Expired - Fee Related
- 2001-09-25 EP EP01972199A patent/EP1324969A1/fr not_active Withdrawn
- 2001-09-25 AU AU2001291986A patent/AU2001291986A1/en not_active Abandoned
- 2001-09-25 US US10/381,795 patent/US20040011638A1/en not_active Abandoned
- 2001-09-25 JP JP2002531072A patent/JP2004513089A/ja not_active Withdrawn
- 2001-09-25 WO PCT/FR2001/002965 patent/WO2002026685A1/fr not_active Ceased
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2004513089A5 (https=) | ||
| TWI537250B (zh) | 乙烯系不飽和單體之多組分聚合反應抑制劑 | |
| JP6764472B2 (ja) | 重合抑制剤組成物の使用 | |
| JP2002543223A5 (https=) | ||
| KR100471957B1 (ko) | 비닐화합물의중합방지방법 | |
| JP3863694B2 (ja) | ビニル化合物中のｎ−オキシル化合物の安定化方法 | |
| JP2009501243A (ja) | 重合阻害剤としてのオルト−ニトロソフェノール | |
| KR100806558B1 (ko) | 아크릴 모노머의 안정화 방법 | |
| JP3197947B2 (ja) | （メタ）アクリル酸の重合防止法 | |
| JP3493083B2 (ja) | ビニル化合物の重合防止方法 | |
| JP4131005B2 (ja) | 蒸留による（メタ）アクリルモノマーの精製方法 | |
| EP2030963B1 (en) | Derivatives of 1-oxyl-4-hydroxy-2,2,6,6-tetramethylpiperidine as polymerization inhibitors for (meth) acrylate monomers | |
| ID23835A (id) | Metode untuk menghambat polimerisasi suatu senyawa vinil | |
| JPH0873405A (ja) | （メタ）アクリル酸エステルの重合防止剤組成物および該組成物を用いた（メタ）アクリル酸エステルの重合防止方法 | |
| TWI255819B (en) | Process for inhibition of polymerization of (meth)acrylate ester | |
| JP4442845B2 (ja) | レジスト用モノマーおよびその精製方法 | |
| JPH0881397A (ja) | ビニル化合物の重合防止方法 | |
| JP3885486B2 (ja) | ビニル単量体用重合防止剤組成物及び高純度（メタ）アクリル酸の製造方法 | |
| JP2758780B2 (ja) | （メタ）アクリル酸の重合防止方法 | |
| RU2006122956A (ru) | Способ очистки (мет)акриловой кислоты | |
| JP2758239B2 (ja) | 酸モノマーの重合を禁止する方法 | |
| JPH09316022A (ja) | （メタ）アクリル酸およびそのエステルの重合防止方法 | |
| JP2016098368A (ja) | ビニル化合物の重合防止剤組成物及びそれを用いるビニル化合物の重合防止方法 | |
| JP2001172224A (ja) | ビニル化合物の重合防止方法 | |
| JP3312638B2 (ja) | （メタ）アクリル酸の重合防止剤組成物および該組成物を用いた（メタ）アクリル酸の重合防止方法 |