IN2014KN02966A - - Google Patents

Info

Publication number
IN2014KN02966A
IN2014KN02966A IN2966KON2014A IN2014KN02966A IN 2014KN02966 A IN2014KN02966 A IN 2014KN02966A IN 2966KON2014 A IN2966KON2014 A IN 2966KON2014A IN 2014KN02966 A IN2014KN02966 A IN 2014KN02966A
Authority
IN
India
Prior art keywords
calcium carbonate
ammonium sulfate
reaction
processes
fgd gypsum
Prior art date
Application number
Other languages
English (en)
Inventor
Murray P Hasinoff
Taylor Pursell
Joseph A Saiia
Arthur R Shirley
Keith D Cochran
Timothy G Holt
Original Assignee
Sparstane Technologies LLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Sparstane Technologies LLC filed Critical Sparstane Technologies LLC
Publication of IN2014KN02966A publication Critical patent/IN2014KN02966A/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/20Obtaining alkaline earth metals or magnesium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F11/00Compounds of calcium, strontium, or barium
    • C01F11/18Carbonates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/24Sulfates of ammonium
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/24Sulfates of ammonium
    • C01C1/244Preparation by double decomposition of ammonium salts with sulfates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01FCOMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F11/00Compounds of calcium, strontium, or barium
    • C01F11/46Sulfates
    • C01F11/468Purification of calcium sulfates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00274Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
    • B01J2219/00277Apparatus
    • B01J2219/00479Means for mixing reactants or products in the reaction vessels
    • B01J2219/00484Means for mixing reactants or products in the reaction vessels by shaking, vibrating or oscillating of the reaction vessels
    • B01J2219/00486Means for mixing reactants or products in the reaction vessels by shaking, vibrating or oscillating of the reaction vessels by sonication or ultrasonication
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/30Particle morphology extending in three dimensions
    • C01P2004/38Particle morphology extending in three dimensions cube-like
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/50Agglomerated particles
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Engineering & Computer Science (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
  • Treating Waste Gases (AREA)
IN2966KON2014 2012-08-10 2013-08-09 IN2014KN02966A (th)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201261681795P 2012-08-10 2012-08-10
PCT/US2013/054354 WO2014026120A2 (en) 2012-08-10 2013-08-09 Process for converting fgd gypsum to ammonium sulfate and calcium carbonate

Publications (1)

Publication Number Publication Date
IN2014KN02966A true IN2014KN02966A (th) 2015-05-08

Family

ID=50066299

Family Applications (1)

Application Number Title Priority Date Filing Date
IN2966KON2014 IN2014KN02966A (th) 2012-08-10 2013-08-09

Country Status (10)

Country Link
US (1) US8758719B2 (th)
EP (1) EP2882879A4 (th)
JP (1) JP5965549B2 (th)
KR (1) KR101588320B1 (th)
CN (1) CN104854251B (th)
AU (1) AU2013299456B2 (th)
CL (1) CL2015000279A1 (th)
IN (1) IN2014KN02966A (th)
WO (1) WO2014026120A2 (th)
ZA (1) ZA201501579B (th)

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CN107532388A (zh) * 2015-01-14 2018-01-02 英默里斯美国公司 用于沉淀碳酸钙的受控方法
US9682868B2 (en) * 2015-01-30 2017-06-20 Sparstane Technologies LLC Partially continuous countercurrent process for converting gypsum to ammonium sulfate and calcium carbonate
PL412427A1 (pl) * 2015-05-20 2016-11-21 Włodzimierz Merka Sposób kompleksowej utylizacji fosfogipsów
US10723935B2 (en) * 2015-11-05 2020-07-28 Halliburton Energy Services, Inc. Calcium carbonate lost circulation material morphologies for use in subterranean formation operations
US20180072972A1 (en) * 2016-09-09 2018-03-15 Alpha Revolution, Inc. Systems, devices and methods for fermenting beverages
CN107311111A (zh) * 2017-05-04 2017-11-03 武汉科技大学 一种基于微波辐照和连续逆流法制备碳酸钙的方法
CN107583466A (zh) * 2017-09-27 2018-01-16 四川恒泰环境技术有限责任公司 一种将湿法脱硫石膏直接转化为硫酸铵和碳酸钙并循环利用的方法
CN109019652B (zh) * 2018-08-03 2021-01-05 江西华明纳米碳酸钙有限公司 一种内侧分离钙离子的生产食品碳酸钙的设备
US11479472B2 (en) 2019-01-24 2022-10-25 Elixsys, Inc. Systems and methods to recover value-added materials from gypsum
US11148956B2 (en) 2019-01-24 2021-10-19 Elixsys, Inc. Systems and methods to treat flue gas desulfurization waste to produce ammonium sulfate and calcium carbonate products
EP3898518A4 (en) * 2019-01-24 2022-09-28 Elixsys Inc. FLUE GAS AND WASTE METALLIC STREAM DESULPHURIZATION TREATMENT SYSTEMS AND METHODS FOR RECOVERING VALUE-ADDED MATERIALS
CN109985497A (zh) * 2019-04-10 2019-07-09 通用技术集团工程设计有限公司 一种钙、氨双段脱硫工艺及设备
CN110697731A (zh) * 2019-11-05 2020-01-17 浙江浙能技术研究院有限公司 一种以脱硫石膏制备硫酸铵和碳酸钙的方法
US11999664B2 (en) 2019-11-12 2024-06-04 Scott Severson Processes and systems for producing ammonia products and/or calcium carbonate products
JP6900992B2 (ja) * 2019-11-22 2021-07-14 宇部興産株式会社 亜硫酸カルシウム含有石膏、セメント組成物、地盤改良材及び地盤改良土
CN111410212A (zh) * 2020-03-09 2020-07-14 安徽海德化工科技有限公司 一种硫酸生产废水回收利用的方法
CN111606346A (zh) * 2020-06-05 2020-09-01 瀜矿环保科技(上海)有限公司 基于二氧化碳浸取的钙镁离子溶液制备碳酸钙镁的系统
FR3113050B1 (fr) * 2020-07-31 2023-04-21 Ocp Sa Procédé de fabrication de sulfate d’ammonium et de carbonate de calcium à partir de phosphogypse
CN112608233A (zh) * 2020-12-23 2021-04-06 安徽英特力工业工程技术有限公司 一种硫酸钙废渣的回收再利用工艺
WO2022245733A1 (en) * 2021-05-15 2022-11-24 Elixsys, Inc. Systems and methods to recover value-added materials from gypsum
CN115520879B (zh) * 2021-06-24 2024-03-26 中国石油化工股份有限公司 异相晶种连续制备颗粒硫酸铵的方法及装置
CN114057215A (zh) * 2021-11-17 2022-02-18 郑州大学 一种利用脱硫石膏制备高纯度硫酸钙的方法
IT202200004001A1 (it) * 2022-03-03 2023-09-03 Milano Politecnico Processo di sequestro di anidride carbonica e relativa trasformazione in prodotti chimici ad alto valore aggiunto
CN115504695B (zh) * 2022-09-06 2023-12-12 宜昌邦普循环科技有限公司 一种磷石膏的回收方法
CN116212607A (zh) * 2023-01-31 2023-06-06 西安热工研究院有限公司 一种加速脱硫石膏直接矿化烟气二氧化碳的系统及方法

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Also Published As

Publication number Publication date
JP2015528431A (ja) 2015-09-28
KR20150043400A (ko) 2015-04-22
US20140044619A1 (en) 2014-02-13
US8758719B2 (en) 2014-06-24
KR101588320B1 (ko) 2016-01-25
AU2013299456B2 (en) 2016-04-28
AU2013299456A1 (en) 2015-01-22
CN104854251B (zh) 2017-03-01
JP5965549B2 (ja) 2016-08-10
CN104854251A (zh) 2015-08-19
CL2015000279A1 (es) 2015-10-02
EP2882879A4 (en) 2016-11-23
WO2014026120A2 (en) 2014-02-13
WO2014026120A3 (en) 2015-07-30
ZA201501579B (en) 2016-07-27
EP2882879A2 (en) 2015-06-17

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