IL50070A - Process for the production of 1,1,2,3-tetrachloropropene - Google Patents
Process for the production of 1,1,2,3-tetrachloropropeneInfo
- Publication number
- IL50070A IL50070A IL50070A IL5007072A IL50070A IL 50070 A IL50070 A IL 50070A IL 50070 A IL50070 A IL 50070A IL 5007072 A IL5007072 A IL 5007072A IL 50070 A IL50070 A IL 50070A
- Authority
- IL
- Israel
- Prior art keywords
- effluent
- fractionating
- passing
- fraction
- chlorinator
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 24
- UMGQVBVEWTXECF-UHFFFAOYSA-N 1,1,2,3-tetrachloroprop-1-ene Chemical compound ClCC(Cl)=C(Cl)Cl UMGQVBVEWTXECF-UHFFFAOYSA-N 0.000 title claims description 4
- 238000004519 manufacturing process Methods 0.000 title description 5
- 239000003518 caustics Substances 0.000 claims description 11
- 239000008187 granular material Substances 0.000 claims description 8
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 7
- 239000000460 chlorine Substances 0.000 claims description 7
- 229910052801 chlorine Inorganic materials 0.000 claims description 7
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical class CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 claims description 5
- 239000004927 clay Substances 0.000 claims description 4
- VKEIPALYOJMDAC-UHFFFAOYSA-N 3,3,3-trichloroprop-1-ene Chemical class ClC(Cl)(Cl)C=C VKEIPALYOJMDAC-UHFFFAOYSA-N 0.000 claims description 3
- 239000003054 catalyst Substances 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 3
- FEKGWIHDBVDVSM-UHFFFAOYSA-N 1,1,1,2-tetrachloropropane Chemical compound CC(Cl)C(Cl)(Cl)Cl FEKGWIHDBVDVSM-UHFFFAOYSA-N 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 238000004064 recycling Methods 0.000 claims description 2
- 235000013849 propane Nutrition 0.000 claims 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical class O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 238000005660 chlorination reaction Methods 0.000 description 5
- 150000001875 compounds Chemical class 0.000 description 4
- 238000006317 isomerization reaction Methods 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N Propene Chemical compound CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 2
- 239000004009 herbicide Substances 0.000 description 2
- 239000010410 layer Substances 0.000 description 2
- 239000012044 organic layer Substances 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000001294 propane Substances 0.000 description 2
- 239000010453 quartz Substances 0.000 description 2
- 239000000377 silicon dioxide Substances 0.000 description 2
- FTCVHAQNWWBTIV-UHFFFAOYSA-N 1,1,1,2,2-pentachloropropane Chemical class CC(Cl)(Cl)C(Cl)(Cl)Cl FTCVHAQNWWBTIV-UHFFFAOYSA-N 0.000 description 1
- AVGQTJUPLKNPQP-UHFFFAOYSA-N 1,1,1-trichloropropane Chemical compound CCC(Cl)(Cl)Cl AVGQTJUPLKNPQP-UHFFFAOYSA-N 0.000 description 1
- PPJYSSNKSXAVDB-UHFFFAOYSA-N 3,3',5,5'-tetraiodothyroacetic acid Chemical compound IC1=CC(CC(=O)O)=CC(I)=C1OC1=CC(I)=C(O)C(I)=C1 PPJYSSNKSXAVDB-UHFFFAOYSA-N 0.000 description 1
- 241001331845 Equus asinus x caballus Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 101100400378 Mus musculus Marveld2 gene Proteins 0.000 description 1
- HRYILSDLIGTCOP-UHFFFAOYSA-N N-benzoylurea Chemical compound NC(=O)NC(=O)C1=CC=CC=C1 HRYILSDLIGTCOP-UHFFFAOYSA-N 0.000 description 1
- YKTSYUJCYHOUJP-UHFFFAOYSA-N [O--].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-] Chemical compound [O--].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-] YKTSYUJCYHOUJP-UHFFFAOYSA-N 0.000 description 1
- CNLWCVNCHLKFHK-UHFFFAOYSA-N aluminum;lithium;dioxido(oxo)silane Chemical compound [Li+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O CNLWCVNCHLKFHK-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- -1 diisopropyl thiol Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000001473 noxious effect Effects 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 229910052642 spodumene Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229910052882 wollastonite Inorganic materials 0.000 description 1
- 239000010456 wollastonite Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/10—Preparation of halogenated hydrocarbons by replacement by halogens of hydrogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
- C07C17/04—Preparation of halogenated hydrocarbons by addition of halogens to unsaturated halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/35—Preparation of halogenated hydrocarbons by reactions not affecting the number of carbon or of halogen atoms in the reaction
- C07C17/358—Preparation of halogenated hydrocarbons by reactions not affecting the number of carbon or of halogen atoms in the reaction by isomerisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C21/00—Acyclic unsaturated compounds containing halogen atoms
- C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
- C07C21/04—Chloro-alkenes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US21026871A | 1971-12-17 | 1971-12-17 | |
| US00212742A US3823195A (en) | 1971-12-27 | 1971-12-27 | Preparation of 1,1,2,3-tetrachloropropene from 1,2,3-trichloropropane |
| US30216372A | 1972-10-30 | 1972-10-30 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IL50070A true IL50070A (en) | 1977-05-31 |
Family
ID=27395474
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL50070A IL50070A (en) | 1971-12-17 | 1972-12-15 | Process for the production of 1,1,2,3-tetrachloropropene |
| IL41101A IL41101A (en) | 1971-12-17 | 1972-12-15 | Process for preparing 1,2,3-trichloropropene |
| IL7650070A IL50070A0 (en) | 1971-12-17 | 1976-07-20 | Process for the production of 1,1,2,3-tetrachloropropene |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IL41101A IL41101A (en) | 1971-12-17 | 1972-12-15 | Process for preparing 1,2,3-trichloropropene |
| IL7650070A IL50070A0 (en) | 1971-12-17 | 1976-07-20 | Process for the production of 1,1,2,3-tetrachloropropene |
Country Status (13)
| Country | Link |
|---|---|
| JP (2) | JPS4867209A (https=) |
| BE (1) | BE792789A (https=) |
| BG (1) | BG21599A3 (https=) |
| CH (1) | CH584173A5 (https=) |
| DD (1) | DD101140A5 (https=) |
| DE (1) | DE2261516C3 (https=) |
| FR (2) | FR2169817B1 (https=) |
| GB (1) | GB1381619A (https=) |
| IL (3) | IL50070A (https=) |
| IT (1) | IT974728B (https=) |
| NL (1) | NL160542C (https=) |
| RO (1) | RO60573A (https=) |
| YU (1) | YU39903B (https=) |
Families Citing this family (30)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| ES3036520T3 (en) * | 2006-01-03 | 2025-09-19 | Honeywell Int Inc | Method for producing fluorinated organic compounds |
| US8258355B2 (en) * | 2007-07-25 | 2012-09-04 | Honeywell International Inc. | Processes for preparing 1,1,2,3-tetrachloropropene |
| US8115038B2 (en) | 2007-12-19 | 2012-02-14 | Occidental Chemical Corporation | Methods of making chlorinated hydrocarbons |
| MY152994A (en) * | 2009-06-24 | 2014-12-31 | Tokuyama Corp | Process of making a chlorinated hydrocarbon |
| JP5782038B2 (ja) | 2009-10-09 | 2015-09-24 | ダウ グローバル テクノロジーズ エルエルシー | 等温多管式反応器及び該反応器を組み込んだプロセス |
| BR112012007916A2 (pt) | 2009-10-09 | 2019-09-24 | Dow Global Technologies Llc | processo de etapa para a produção de propenos clorados ou fluorados e processo para preparar 1,1,3,3 - tetrafluorprop-1-eno |
| JP5767231B2 (ja) | 2009-10-09 | 2015-08-19 | ダウ グローバル テクノロジーズ エルエルシー | 塩素化及び／又はフッ素化されたプロペン及びより高級なアルケンを製造するプロセス |
| WO2012166394A1 (en) * | 2011-05-31 | 2012-12-06 | Dow Global Technologies, Llc | Process for the production of chlorinated propenes |
| JP6212035B2 (ja) * | 2011-05-31 | 2017-10-11 | ブルー キューブ アイピー エルエルシー | 塩素化プロペンの製造方法 |
| JP6267114B2 (ja) | 2011-06-08 | 2018-01-24 | ダウ アグロサイエンシィズ エルエルシー | 塩素化および／またはフッ素化プロペンを生成するためのプロセス |
| CN103717557A (zh) | 2011-08-07 | 2014-04-09 | 陶氏环球技术有限责任公司 | 生产氯化的丙烯的方法 |
| CN108929192A (zh) * | 2011-08-07 | 2018-12-04 | 蓝立方知识产权有限责任公司 | 生产氯化的丙烯的方法 |
| WO2013074394A1 (en) * | 2011-11-18 | 2013-05-23 | Dow Global Technologies, Llc | Process for the production of chlorinated propanes and/or propenes |
| IN2014CN03748A (https=) | 2011-11-21 | 2015-09-25 | Dow Global Technologies Llc | |
| JP6050375B2 (ja) | 2011-12-02 | 2016-12-21 | ブルー キューブ アイピー エルエルシー | クロロアルカンの製造方法 |
| CA2856545A1 (en) | 2011-12-02 | 2013-06-06 | Dow Global Technologies Llc | Process for the production of chlorinated alkanes |
| JP6170068B2 (ja) | 2011-12-13 | 2017-07-26 | ブルー キューブ アイピー エルエルシー | 塩素化プロパン及びプロペンの製造方法 |
| IN2014CN04418A (https=) | 2011-12-22 | 2015-09-04 | Dow Global Technologies Llc | |
| WO2013096706A1 (en) | 2011-12-23 | 2013-06-27 | Dow Global Technologies, Llc | Process for the production of alkenes and/or aromatic compounds |
| US9598334B2 (en) | 2012-09-20 | 2017-03-21 | Blue Cube Ip Llc | Process for the production of chlorinated propenes |
| EP2897930A1 (en) | 2012-09-20 | 2015-07-29 | Dow Global Technologies LLC | Process for the production of chlorinated propenes |
| CA2885329A1 (en) | 2012-09-30 | 2014-03-04 | Dow Global Technologies Llc | Weir quench and processes incorporating the same |
| US10065157B2 (en) | 2012-10-26 | 2018-09-04 | Blue Cube Ip Llc | Mixer and processes incorporating the same |
| JP6247311B2 (ja) | 2012-12-18 | 2017-12-13 | ブルー キューブ アイピー エルエルシー | 塩素化プロペンを生成するための方法 |
| CA2894168C (en) | 2012-12-19 | 2018-04-24 | Dow Global Technologies Llc | Process for the production of chlorinated propenes |
| US8889929B2 (en) * | 2013-02-19 | 2014-11-18 | Honeywell International Inc. | Process to make 1,1,2,3-tetrachloropropene from 1,1,3-trichloropropene and/or 3,3,3-trichloropropene |
| CA2901450A1 (en) | 2013-02-27 | 2014-09-04 | Blue Cube Ip Llc | Process for the production of chlorinated propenes |
| CA2903760C (en) | 2013-03-09 | 2018-02-20 | Blue Cube Ip Llc | Process for the production of chlorinated alkanes |
| CN115108882B (zh) * | 2022-06-07 | 2024-04-12 | 浙江衢化氟化学有限公司 | 一种1,1,1,2,3-五氯丙烷的连续制备方法 |
| CN117285407A (zh) * | 2023-09-25 | 2023-12-26 | 广东电网有限责任公司 | 一种1,1,2-三氯丙烯的制备方法 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1459842A (fr) * | 1964-07-29 | 1966-06-17 | Knapsack Ag | Procédé de préparation de 2-chlorobutène-(2) |
| GB1152021A (en) * | 1965-08-30 | 1969-05-14 | Pullman Inc | Dehydrohalogenation Process |
-
1972
- 1972-12-12 NL NL7216840.A patent/NL160542C/xx not_active IP Right Cessation
- 1972-12-15 IL IL50070A patent/IL50070A/en unknown
- 1972-12-15 YU YU3143/72A patent/YU39903B/xx unknown
- 1972-12-15 RO RO73167A patent/RO60573A/ro unknown
- 1972-12-15 JP JP47125368A patent/JPS4867209A/ja active Pending
- 1972-12-15 IL IL41101A patent/IL41101A/en unknown
- 1972-12-15 GB GB5803872A patent/GB1381619A/en not_active Expired
- 1972-12-15 DE DE2261516A patent/DE2261516C3/de not_active Expired
- 1972-12-15 DD DD167592A patent/DD101140A5/xx unknown
- 1972-12-15 BE BE792789D patent/BE792789A/xx not_active IP Right Cessation
- 1972-12-15 BG BG022127A patent/BG21599A3/xx unknown
- 1972-12-15 FR FR7244864A patent/FR2169817B1/fr not_active Expired
- 1972-12-18 IT IT33069/72A patent/IT974728B/it active
-
1973
- 1973-06-12 FR FR7321260A patent/FR2202065A1/fr active Granted
- 1973-06-12 CH CH849373A patent/CH584173A5/xx not_active IP Right Cessation
- 1973-06-15 JP JP6697973A patent/JPS5346807B2/ja not_active Expired
-
1976
- 1976-07-20 IL IL7650070A patent/IL50070A0/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DD101140A5 (https=) | 1973-10-20 |
| FR2169817A1 (https=) | 1973-09-14 |
| IL50070A0 (en) | 1976-09-30 |
| DE2261516B2 (de) | 1979-11-22 |
| CH584173A5 (https=) | 1977-01-31 |
| DE2261516C3 (de) | 1980-07-31 |
| FR2202065B1 (https=) | 1977-05-06 |
| IL41101A0 (en) | 1973-02-28 |
| IL41101A (en) | 1977-05-31 |
| JPS4867209A (https=) | 1973-09-13 |
| YU39903B (en) | 1985-06-30 |
| DE2261516A1 (de) | 1973-06-28 |
| NL160542B (nl) | 1979-06-15 |
| NL160542C (nl) | 1979-11-15 |
| FR2202065A1 (en) | 1974-05-03 |
| IT974728B (it) | 1974-07-10 |
| FR2169817B1 (https=) | 1977-08-05 |
| JPS504006A (https=) | 1975-01-16 |
| GB1381619A (en) | 1975-01-22 |
| YU314372A (en) | 1982-08-31 |
| JPS5346807B2 (https=) | 1978-12-16 |
| RO60573A (https=) | 1976-10-15 |
| BE792789A (fr) | 1973-06-15 |
| NL7216840A (https=) | 1973-06-19 |
| BG21599A3 (bg) | 1976-07-20 |
| AU480375A (https=) | 1974-12-05 |
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