HK1204387A1 - Cellulose nanofibril decorated with magnetic nanoparticles - Google Patents

Cellulose nanofibril decorated with magnetic nanoparticles

Info

Publication number
HK1204387A1
HK1204387A1 HK15104779.2A HK15104779A HK1204387A1 HK 1204387 A1 HK1204387 A1 HK 1204387A1 HK 15104779 A HK15104779 A HK 15104779A HK 1204387 A1 HK1204387 A1 HK 1204387A1
Authority
HK
Hong Kong
Prior art keywords
decorated
magnetic nanoparticles
cellulose nanofibril
nanofibril
cellulose
Prior art date
Application number
HK15104779.2A
Other languages
English (en)
Chinese (zh)
Inventor
Sylvain Galland
Richard T Olsson
Lars Berglund
Original Assignee
Cellutech Ab
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Cellutech Ab filed Critical Cellutech Ab
Publication of HK1204387A1 publication Critical patent/HK1204387A1/xx

Links

Classifications

    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/01Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00Compounds of iron
    • C01G49/0018Mixed oxides or hydroxides
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00Compounds of iron
    • C01G49/0018Mixed oxides or hydroxides
    • C01G49/0072Mixed oxides or hydroxides containing manganese
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01GCOMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G49/00Compounds of iron
    • C01G49/02Oxides; Hydroxides
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/32Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/36Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
    • D06M11/49Oxides or hydroxides of elements of Groups 8, 9,10 or 18 of the Periodic Table; Ferrates; Cobaltates; Nickelates; Ruthenates; Osmates; Rhodates; Iridates; Palladates; Platinates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/83Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with metals; with metal-generating compounds, e.g. metal carbonyls; Reduction of metal compounds on textiles
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21CPRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
    • D21C9/00After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters ; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere
    • D21C9/001Modification of pulp properties
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H11/00Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
    • D21H11/16Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only modified by a particular after-treatment
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/63Inorganic compounds
    • D21H17/67Water-insoluble compounds, e.g. fillers, pigments
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/0036Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties showing low dimensional magnetism, i.e. spin rearrangements due to a restriction of dimensions, e.g. showing giant magnetoresistivity
    • H01F1/0045Zero dimensional, e.g. nanoparticles, soft nanoparticles for medical/biological use
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y25/00Nanomagnetism, e.g. magnetoimpedance, anisotropic magnetoresistance, giant magnetoresistance or tunneling magnetoresistance
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/64Nanometer sized, i.e. from 1-100 nanometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/42Magnetic properties
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/01Magnetic additives
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/14Polymer mixtures characterised by other features containing polymeric additives characterised by shape
    • C08L2205/16Fibres; Fibrils
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres
    • D06M2101/06Vegetal fibres cellulosic
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F1/00Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
    • H01F1/0036Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties showing low dimensional magnetism, i.e. spin rearrangements due to a restriction of dimensions, e.g. showing giant magnetoresistivity
    • H01F1/0045Zero dimensional, e.g. nanoparticles, soft nanoparticles for medical/biological use
    • H01F1/0063Zero dimensional, e.g. nanoparticles, soft nanoparticles for medical/biological use in a non-magnetic matrix, e.g. granular solids
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913Rod, strand, filament or fiber
    • Y10T428/2927Rod, strand, filament or fiber including structurally defined particulate matter
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913Rod, strand, filament or fiber
    • Y10T428/2933Coated or with bond, impregnation or core
    • Y10T428/294Coated or with bond, impregnation or core including metal or compound thereof [excluding glass, ceramic and asbestos]
    • Y10T428/2958Metal or metal compound in coating

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Textile Engineering (AREA)
  • Power Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Molecular Biology (AREA)
  • Nanotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Wood Science & Technology (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Hard Magnetic Materials (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Paper (AREA)
HK15104779.2A 2012-02-10 2015-05-19 Cellulose nanofibril decorated with magnetic nanoparticles HK1204387A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
SE1200087 2012-02-10
US201261598282P 2012-02-13 2012-02-13
PCT/SE2013/050115 WO2013119179A1 (en) 2012-02-10 2013-02-11 Cellulose nanofibril decorated with magnetic nanoparticles

Publications (1)

Publication Number Publication Date
HK1204387A1 true HK1204387A1 (en) 2015-11-13

Family

ID=48947831

Family Applications (1)

Application Number Title Priority Date Filing Date
HK15104779.2A HK1204387A1 (en) 2012-02-10 2015-05-19 Cellulose nanofibril decorated with magnetic nanoparticles

Country Status (7)

Country Link
US (1) US9767944B2 (xx)
EP (1) EP2812900B1 (xx)
JP (1) JP6345122B2 (xx)
CN (1) CN104221101B (xx)
CA (1) CA2861563C (xx)
HK (1) HK1204387A1 (xx)
WO (1) WO2013119179A1 (xx)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103834064B (zh) * 2014-02-20 2016-01-06 钟春燕 一种细菌纤维素/铁氧体复合吸波材料及其制备方法
US10626191B2 (en) 2015-05-04 2020-04-21 Upm-Kymmene Corporation Nanofibrillar cellulose product
CN106884309B (zh) * 2015-12-15 2020-10-02 深圳先进技术研究院 一种纤维杂化颗粒及聚合物基复合材料
KR102416571B1 (ko) * 2015-12-22 2022-07-01 삼성전자주식회사 자성 시트, 그의 제조 방법 및 자성 시트를 포함하는 스피커
CN106243392B (zh) * 2016-08-01 2018-10-02 南京林业大学 一种抗静电纤维素纳米微晶包装复合膜的制备方法
US20200385547A1 (en) * 2016-11-28 2020-12-10 Nippon Paper Industries Co., Ltd. Complexes of fibers and inorganic particles
US10287413B2 (en) * 2016-12-19 2019-05-14 3M Innovative Properties Company Thermoplastic polymer composite containing soft, ferromagnetic particulate material and methods of making thereof
JP6954523B2 (ja) * 2017-02-10 2021-10-27 国立大学法人山口大学 遷移金属酸化物及びセルロースナノファイバーを含有する複合膜並びにその製造方法
JP6442574B2 (ja) * 2017-03-16 2018-12-19 太平洋セメント株式会社 ナノ粒子集合体、ナノ粒子焼成物、及びこれらの製造方法
JP7265750B2 (ja) * 2019-02-08 2023-04-27 国立大学法人九州工業大学 樹脂混合用ハイブリッドフィラー及びその製造方法
CN110164642A (zh) * 2019-04-23 2019-08-23 中北大学 一种氧化石墨烯修饰磁性纳米材料的超重力制备方法和装置
DE112020003417T5 (de) 2019-07-16 2022-03-31 Rogers Corporation Magneto-dielektrische Materialien, Verfahren zu ihrer Herstellung und ihre Verwendungen
CN110305364A (zh) * 2019-07-30 2019-10-08 济南大学 一种新型磁性聚乙烯醇缩甲醛海绵的制备方法
WO2021242067A1 (ko) * 2020-05-29 2021-12-02 주식회사 엘지화학 피브릴화 섬유 및 이의 제조 방법
CN112280343B (zh) * 2020-11-10 2022-07-19 山东鲁阳节能材料股份有限公司 一种高温纳米复合涂料及其制备方法,以及小袋软包装涂料
CN114747714A (zh) * 2021-01-11 2022-07-15 天津科技大学 一种新型植物源缓释抗菌磁性气凝胶的制备方法
AU2022287908A1 (en) 2021-06-09 2023-12-14 Soane Materials Llc Articles of manufacture comprising nanocellulose elements
CN114323080A (zh) * 2021-11-15 2022-04-12 华中科技大学 一种磁性纳米纤维素基的可降解柔性运动传感器及其制备
CN116351420A (zh) * 2023-03-31 2023-06-30 山东大学 一种非均相光芬顿催化降解染料的铁酸铜纤维及其制备方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3689940T2 (de) 1985-04-16 1995-02-23 Agency Ind Science Techn Formmasse auf Basis von bakteriell hergestellter Cellulose.
JPS6365085A (ja) 1986-09-05 1988-03-23 Nippon Paint Co Ltd 粒子または繊維状物のフエライト被覆方法
US5143583A (en) 1991-04-02 1992-09-01 Marchessault Robert H Preparation and synthesis of magnetic fibers
JP3413963B2 (ja) * 1994-05-26 2003-06-09 ジェイエスアール株式会社 磁性粒子の製造方法
JP2000243612A (ja) * 1999-02-22 2000-09-08 Daido Steel Co Ltd 強磁性粉末と紙パルプの複合強磁性体及びその製造方法
US20040146855A1 (en) 2003-01-27 2004-07-29 Marchessault Robert H. Formation of superparamagnetic particles
US7431862B2 (en) * 2004-04-30 2008-10-07 Coldwatt, Inc. Synthesis of magnetic, dielectric or phosphorescent NANO composites
ES2635724T3 (es) * 2007-03-29 2017-10-04 Cellutech Ab Material de celulosa de nanopartículas magnéticas
JP2011162377A (ja) * 2010-02-08 2011-08-25 Teijin Ltd N−オキシル化合物担持磁性粒子
CN102093840B (zh) * 2011-01-06 2015-06-17 西南科技大学 一种碳化细菌纤维素/磁性复合吸波材料及其制备方法
CN102336920B (zh) * 2011-05-28 2012-11-14 东华大学 一种具有双疏性能的磁性细菌纤维素膜及其制备方法

Also Published As

Publication number Publication date
EP2812900B1 (en) 2019-10-23
CN104221101A (zh) 2014-12-17
WO2013119179A1 (en) 2013-08-15
JP2015513569A (ja) 2015-05-14
EP2812900A4 (en) 2015-12-02
CA2861563A1 (en) 2013-08-15
CA2861563C (en) 2020-04-21
CN104221101B (zh) 2018-03-30
US9767944B2 (en) 2017-09-19
US20150357099A1 (en) 2015-12-10
JP6345122B2 (ja) 2018-06-20
EP2812900A1 (en) 2014-12-17

Similar Documents

Publication Publication Date Title
HK1204387A1 (en) Cellulose nanofibril decorated with magnetic nanoparticles
HK1204529A1 (en) Diterpene production
EP2888806A4 (en) ROTOR WITH MAGNETIC PATTERN
EP2833926A4 (en) NEUROPHILIC NANOPARTICLES
EP2910574A4 (en) CELLULOSE NANO FIBERS
EP2877996A4 (en) DYNAMIC DETECTION CIRCUIT
PL2823519T3 (pl) Silnie porowata folia separatorowa z częściową powłoką
EP2807936A4 (en) CLOTHING
EP2896842A4 (en) MAGNETIC BEARING
PL2712594T3 (pl) Tampon z wydłużonymi rowkami
SG11201503403QA (en) Encapsulated Nanoparticles
EP2838966A4 (en) AQUEOUS COATING COMPOSITION WITH IMPROVED STABILITY
EP2811852A4 (en) SUBSTITUTED CELLULOSE ACETATES AND USES THEREOF
GB201508581D0 (en) Energy-saving magnetic lock
SG11201508111QA (en) Modified g-quadruplex nanoparticles
EP2857421A4 (en) CELLULOSE POWDER
GB201216930D0 (en) Nanoparticles
SG11201403144XA (en) Improvements in coating technology
EP2806842A4 (en) SUBSTITUTED CELLULOSE ACETATE AND USES THEREOF
GB201214826D0 (en) Oxidised cellulose
TWI562725B (en) Reel body and spinning reel
EP2932284A4 (en) MAGNETOMETER WITH LARGE DYNAMIC RANGE
EP2880060A4 (en) SURFACE-MODIFIED NANOCRYSTALLINE CELLULOSE AND USES THEREOF
EP2867155A4 (en) NANOSTRUCTURE COMPRISING FUNCTIONALLY DIFFERENT SIDES
HK1205035A1 (en) Figurine

Legal Events

Date Code Title Description
PC Patent ceased (i.e. patent has lapsed due to the failure to pay the renewal fee)

Effective date: 20230216