GB894364A - Complex silicate fillers - Google Patents

Complex silicate fillers

Info

Publication number
GB894364A
GB894364A GB2669359A GB2669359A GB894364A GB 894364 A GB894364 A GB 894364A GB 2669359 A GB2669359 A GB 2669359A GB 2669359 A GB2669359 A GB 2669359A GB 894364 A GB894364 A GB 894364A
Authority
GB
United Kingdom
Prior art keywords
sodium
solution
silicate
ammonium salt
aluminate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2669359A
Inventor
Raymond Craig Herron
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Chemical Industries Ltd
Original Assignee
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Imperial Chemical Industries Ltd filed Critical Imperial Chemical Industries Ltd
Priority to GB2669359A priority Critical patent/GB894364A/en
Publication of GB894364A publication Critical patent/GB894364A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/20Silicates
    • C01B33/36Silicates having base-exchange properties but not having molecular sieve properties
    • C01B33/38Layered base-exchange silicates, e.g. clays, micas or alkali metal silicates of kenyaite or magadiite type
    • C01B33/42Micas ; Interstratified clay-mica products
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/20Silicates
    • C01B33/26Aluminium-containing silicates, i.e. silico-aluminates
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/20Silicates
    • C01B33/36Silicates having base-exchange properties but not having molecular sieve properties
    • C01B33/38Layered base-exchange silicates, e.g. clays, micas or alkali metal silicates of kenyaite or magadiite type
    • C01B33/40Clays
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00Silicon; Compounds thereof
    • C01B33/20Silicates
    • C01B33/36Silicates having base-exchange properties but not having molecular sieve properties
    • C01B33/46Amorphous silicates, e.g. so-called "amorphous zeolites"
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/34Silicon-containing compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Dispersion Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Detergent Compositions (AREA)

Abstract

Sodium aluminium silicates, defined as the complexes of aluminium oxide, sodium oxide, and silicon oxide obtained by the process of Specification 841,831, which may be homogeneous or contain, in addition particles of silica, having an average particle size of less than 50 millimicrons, and containing 2-30% Al2O3, 65-80% SiO2, 1-5% Na2O, together with 10-15% water that can be driven off on ignition, are prepared by adding a sodium silicate solution and a sodium aluminate solution in that order to a solution of an ammonium salt of a strong acid in the presence of sodium sulphate, the mixture being stirred continuously and its temperature being maintained above 60 DEG C. during the reaction, and thereafter filtering, washing and drying the product. The sodium silicate has a motor ratio Na2O:SiO2 in the range 1:2 to 1:4, and the sodium aluminate has a molar ratio Na2O: Al2O3 in the range 1,3:1 to 3:1. The sodium silicate solution contains 150-220 g.p.l. SiO2, and the sodium aluminate solution contains 50-250 g.p.l. Al2O3. The amount of ammonium salt solution employed is 2-10% in excess of that required to neutralize the sodium silicate and aluminate. The ammonium salt solution is preferably one of 80-130 g.p.l. ammonium chloride, and preferably contains 5-60 g.p.l. sodium sulphate. The product is suitable for use as a rubber filler.ALSO:A rubber mix has the following composition by weight .natural rubber (pale crepe).100 .zinc oxide.1 .stearic acid.1 .Vulcafor FN.1,5 .Vulcafor ZDC.0,5 .benzoic acid.1,25 .triethanolamine.2 .sulphur.2,5 .sodium aluminium silicate.40 .("Vulcafor" is a Registered Trade Mark) The sodium aluminium silicate is prepared by adding solutions of sodium silicate and sodium aluminate in that order to a solution of an ammonium salt of a strong acid in the presence of sodium sulphate. Specification 841,831 is referred to.
GB2669359A 1959-08-05 1959-08-05 Complex silicate fillers Expired GB894364A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB2669359A GB894364A (en) 1959-08-05 1959-08-05 Complex silicate fillers

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB2669359A GB894364A (en) 1959-08-05 1959-08-05 Complex silicate fillers

Publications (1)

Publication Number Publication Date
GB894364A true GB894364A (en) 1962-04-18

Family

ID=10247711

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2669359A Expired GB894364A (en) 1959-08-05 1959-08-05 Complex silicate fillers

Country Status (1)

Country Link
GB (1) GB894364A (en)

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