GB1591874A - N-methoxy-carbonyl-n'-supphonylhydrazines - Google Patents
N-methoxy-carbonyl-n'-supphonylhydrazines Download PDFInfo
- Publication number
- GB1591874A GB1591874A GB765/80A GB76580A GB1591874A GB 1591874 A GB1591874 A GB 1591874A GB 765/80 A GB765/80 A GB 765/80A GB 76580 A GB76580 A GB 76580A GB 1591874 A GB1591874 A GB 1591874A
- Authority
- GB
- United Kingdom
- Prior art keywords
- methoxycarbonyl
- formula
- iii
- room temperature
- supphonylhydrazines
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000001875 compounds Chemical class 0.000 claims description 9
- XPDWGBQVDMORPB-UHFFFAOYSA-N Fluoroform Chemical compound FC(F)F XPDWGBQVDMORPB-UHFFFAOYSA-N 0.000 claims description 5
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 15
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 10
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 9
- WJKHJLXJJJATHN-UHFFFAOYSA-N triflic anhydride Chemical compound FC(F)(F)S(=O)(=O)OS(=O)(=O)C(F)(F)F WJKHJLXJJJATHN-UHFFFAOYSA-N 0.000 description 8
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 6
- WFJRIDQGVSJLLH-UHFFFAOYSA-N methyl n-aminocarbamate Chemical compound COC(=O)NN WFJRIDQGVSJLLH-UHFFFAOYSA-N 0.000 description 5
- 239000007787 solid Substances 0.000 description 5
- 125000000217 alkyl group Chemical group 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 125000004432 carbon atom Chemical group C* 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 3
- 125000002768 hydroxyalkyl group Chemical group 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 125000004103 aminoalkyl group Chemical group 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000012259 ether extract Substances 0.000 description 2
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- ITMCEJHCFYSIIV-UHFFFAOYSA-N triflic acid Chemical compound OS(=O)(=O)C(F)(F)F ITMCEJHCFYSIIV-UHFFFAOYSA-N 0.000 description 2
- CXCHEKCRJQRVNG-UHFFFAOYSA-N 2,2,2-trifluoroethanesulfonyl chloride Chemical compound FC(F)(F)CS(Cl)(=O)=O CXCHEKCRJQRVNG-UHFFFAOYSA-N 0.000 description 1
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 125000002252 acyl group Chemical group 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 125000003236 benzoyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C(*)=O 0.000 description 1
- GDTBXPJZTBHREO-UHFFFAOYSA-N bromine Chemical group BrBr GDTBXPJZTBHREO-UHFFFAOYSA-N 0.000 description 1
- 229910052794 bromium Chemical group 0.000 description 1
- 125000001589 carboacyl group Chemical group 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- 125000001309 chloro group Chemical group Cl* 0.000 description 1
- 239000013058 crude material Substances 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 125000004177 diethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- OAKJQQAXSVQMHS-UHFFFAOYSA-N hydrazine Substances NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- OUQAXJFMGKIKRS-UHFFFAOYSA-N methyl n-(sulfonylamino)carbamate Chemical class COC(=O)NN=S(=O)=O OUQAXJFMGKIKRS-UHFFFAOYSA-N 0.000 description 1
- SOEMFPLGOUBPJQ-NTUHNPAUSA-N methyl n-[(e)-quinoxalin-2-ylmethylideneamino]carbamate Chemical compound C1=CC=CC2=NC(/C=N/NC(=O)OC)=CN=C21 SOEMFPLGOUBPJQ-NTUHNPAUSA-N 0.000 description 1
- 239000012299 nitrogen atmosphere Substances 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- -1 sulphonyl group Chemical group 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D241/00—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings
- C07D241/36—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings condensed with carbocyclic rings or ring systems
- C07D241/50—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings condensed with carbocyclic rings or ring systems with hetero atoms directly attached to ring nitrogen atoms
- C07D241/52—Oxygen atoms
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/04—Antibacterial agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P33/00—Antiparasitic agents
- A61P33/02—Antiprotozoals, e.g. for leishmaniasis, trichomoniasis, toxoplasmosis
Landscapes
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Veterinary Medicine (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Pharmacology & Pharmacy (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Chemical & Material Sciences (AREA)
- Oncology (AREA)
- Communicable Diseases (AREA)
- Tropical Medicine & Parasitology (AREA)
- Engineering & Computer Science (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Dermatology (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Saccharide Compounds (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US69626376A | 1976-06-15 | 1976-06-15 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1591874A true GB1591874A (en) | 1981-07-01 |
Family
ID=24796354
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB765/80A Expired GB1591874A (en) | 1976-06-15 | 1977-05-18 | N-methoxy-carbonyl-n'-supphonylhydrazines |
| GB764/80A Expired GB1591873A (en) | 1976-06-15 | 1977-05-18 | Methyl 3-(2-quinoxalinylmethylene)carbazate-n1,n4-dioxides |
| GB20800/77A Expired GB1591872A (en) | 1976-06-15 | 1977-05-18 | Process for producing methyl 3-(2-quinoxalinylmethylene) carbazate-n1,n4-dioxides |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB764/80A Expired GB1591873A (en) | 1976-06-15 | 1977-05-18 | Methyl 3-(2-quinoxalinylmethylene)carbazate-n1,n4-dioxides |
| GB20800/77A Expired GB1591872A (en) | 1976-06-15 | 1977-05-18 | Process for producing methyl 3-(2-quinoxalinylmethylene) carbazate-n1,n4-dioxides |
Country Status (31)
-
1977
- 1977-05-16 SE SE7705744A patent/SE428925B/xx not_active IP Right Cessation
- 1977-05-17 CA CA278,574A patent/CA1087616A/en not_active Expired
- 1977-05-18 ZA ZA00772979A patent/ZA772979B/xx unknown
- 1977-05-18 GB GB765/80A patent/GB1591874A/en not_active Expired
- 1977-05-18 GB GB764/80A patent/GB1591873A/en not_active Expired
- 1977-05-18 GB GB20800/77A patent/GB1591872A/en not_active Expired
- 1977-05-20 GR GR53522A patent/GR72289B/el unknown
- 1977-05-20 NZ NZ184167A patent/NZ184167A/xx unknown
- 1977-05-20 IE IE1040/77A patent/IE44684B1/en not_active IP Right Cessation
- 1977-05-25 IL IL52166A patent/IL52166A0/xx unknown
- 1977-05-26 CH CH650777A patent/CH620911A5/fr not_active IP Right Cessation
- 1977-05-26 PH PH19820A patent/PH14866A/en unknown
- 1977-05-27 YU YU1327/77A patent/YU39492B/xx unknown
- 1977-05-30 JP JP6315177A patent/JPS52153986A/ja active Granted
- 1977-05-31 PT PT66618A patent/PT66618B/pt unknown
- 1977-05-31 NL NL7705938.A patent/NL166685C/xx not_active IP Right Cessation
- 1977-05-31 NO NO771903A patent/NO146864C/no unknown
- 1977-05-31 IT IT49637/77A patent/IT1078874B/it active
- 1977-05-31 DE DE19772725023 patent/DE2725023A1/de active Pending
- 1977-05-31 CS CS773581A patent/CS200218B2/cs unknown
- 1977-06-01 DK DK240777AA patent/DK142497B/da unknown
- 1977-06-01 FI FI771742A patent/FI771742A7/fi not_active Application Discontinuation
- 1977-06-01 AT AT387077A patent/AT357562B/de not_active IP Right Cessation
- 1977-06-02 AR AR267928A patent/AR221207A1/es active
- 1977-06-02 DD DD7700199261A patent/DD131371A5/xx unknown
- 1977-06-02 LU LU77474A patent/LU77474A1/xx unknown
- 1977-06-02 DD DD77204377A patent/DD135080A5/xx not_active IP Right Cessation
- 1977-06-13 BG BG036608A patent/BG35595A3/xx unknown
- 1977-06-14 ES ES459750A patent/ES459750A1/es not_active Expired
- 1977-06-14 ES ES459745A patent/ES459745A1/es not_active Expired
- 1977-06-14 SU SU772494213A patent/SU657746A3/ru active
- 1977-06-15 PL PL1977198873A patent/PL105555B1/pl unknown
- 1977-11-09 PH PH20413A patent/PH14481A/en unknown
-
1979
- 1979-11-10 JP JP14596079A patent/JPS5589256A/ja active Granted
-
1980
- 1980-05-06 SE SE8003393A patent/SE437985B/sv not_active IP Right Cessation
- 1980-12-10 NL NL8006697A patent/NL8006697A/nl not_active Application Discontinuation
-
1981
- 1981-09-22 NO NO813221A patent/NO147422C/no unknown
-
1982
- 1982-10-11 SG SG49282A patent/SG49282G/en unknown
-
1983
- 1983-01-13 HK HK18/83A patent/HK1883A/xx unknown
- 1983-01-13 HK HK20/83A patent/HK2083A/xx unknown
- 1983-01-13 HK HK19/83A patent/HK1983A/xx unknown
- 1983-12-30 MY MY230/83A patent/MY8300230A/xx unknown
- 1983-12-30 MY MY229/83A patent/MY8300229A/xx unknown
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |
Effective date: 19940518 |