GB1329086A - Bleaching composition - Google Patents

Bleaching composition

Info

Publication number
GB1329086A
GB1329086A GB4323569A GB1329086DA GB1329086A GB 1329086 A GB1329086 A GB 1329086A GB 4323569 A GB4323569 A GB 4323569A GB 1329086D A GB1329086D A GB 1329086DA GB 1329086 A GB1329086 A GB 1329086A
Authority
GB
United Kingdom
Prior art keywords
composition
alkali
active agent
surface active
hypochlorite
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB4323569A
Other languages
English (en)
Inventor
B Hynam
J Wilby
J Young
Parker J Pieczka
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Unilever PLC
Original Assignee
Unilever PLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Unilever PLC filed Critical Unilever PLC
Publication of GB1329086A publication Critical patent/GB1329086A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00—Compositions of detergents, not provided for by one single preceding group
    • C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/395—Bleaching agents
    • C11D3/3953—Inorganic bleaching agents
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/395—Bleaching agents
    • C11D3/3956—Liquid compositions
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/75—Amino oxides
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/90—Betaines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)
GB4323569A 1969-08-29 1969-08-29 Bleaching composition Expired GB1329086A (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
GB4323569 1969-08-29
GB4223569 1969-08-29
GB2509870 1970-05-26

Publications (1)

Publication Number Publication Date
GB1329086A true GB1329086A (en) 1973-09-05

Family

ID=27258401

Family Applications (1)

Application Number Title Priority Date Filing Date
GB4323569A Expired GB1329086A (en) 1969-08-29 1969-08-29 Bleaching composition

Country Status (7)

Country Link
US (1) US3684722A (ko)
BE (1) BE755338A (ko)
CH (1) CH542922A (ko)
DE (1) DE2042037C3 (ko)
FR (1) FR2059755B1 (ko)
GB (1) GB1329086A (ko)
NL (2) NL148103B (ko)

Cited By (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2837880A1 (de) * 1977-09-02 1979-03-15 Ici Ltd Bleich- und reinigungsmittel
US4337163A (en) 1979-12-05 1982-06-29 Lever Brothers Company Liquid, thickened chlorine bleaching composition
EP0030825B1 (en) * 1979-12-06 1983-12-28 Economics Laboratory, Inc. Methods and compositions for bleaching of mycological stains
JPS5998200A (ja) * 1982-11-02 1984-06-06 インペリアル・ケミカル・インダストリ−ズ・ピ−エルシ− 漂白剤組成物
US4552680A (en) * 1983-11-04 1985-11-12 The Procter & Gamble Company Hypochlorite bleach containing surfactant and organic antifoamant
US4576728A (en) * 1983-11-11 1986-03-18 The Procter & Gamble Company Cleaning compositions
EP0244611A1 (en) * 1986-04-04 1987-11-11 Unilever N.V. Thickened liquid bleaching composition
US4708816A (en) * 1984-01-27 1987-11-24 The Clorox Company Bleach composition containing controlled density capsules
US4775492A (en) * 1986-02-11 1988-10-04 Lever Brothers Company Thickened liquid bleaching composition
US4783283A (en) * 1985-05-28 1988-11-08 The Procter & Gamble Company Cleaning compositions
US4828748A (en) * 1986-01-03 1989-05-09 The Drackett Company Thickened alkali metal hypochlorite compositions
EP0137871B1 (en) * 1983-10-14 1989-10-18 The Procter & Gamble Company Cleaning compositions
US4929383A (en) * 1984-01-27 1990-05-29 The Clorox Company Stable emulstified bleaching compositions
US4931207A (en) * 1984-01-27 1990-06-05 The Clorox Company Bleaching and bluing composition and method
US4946619A (en) * 1988-07-19 1990-08-07 The Clorox Company Solubilization of brighter in liquid hypochlorite
US4952333A (en) * 1984-01-27 1990-08-28 The Clorox Company Bleaching and brightening composition and method
US5075029A (en) * 1984-01-27 1991-12-24 The Clorox Company Stable emulsified bleaching compositions
US5104571A (en) * 1984-01-27 1992-04-14 The Clorox Company Bleaching and brightening composition and method
US5389157A (en) * 1988-05-20 1995-02-14 The Clorox Company Viscoelastic cleaning compositions with long relaxation times
EP0693548A1 (en) * 1994-07-18 1996-01-24 The Procter & Gamble Company A stable concentrated premix and its use for manufacturing aqueous detergent compositions
US5804545A (en) * 1993-11-24 1998-09-08 West Argo, Inc. Stable alkaline chlorine compositions
US6100228A (en) * 1993-10-29 2000-08-08 The Clorox Company Bleaching gel cleaner thickened with amine oxide, soap and solvent
WO2000052125A1 (de) * 1999-02-27 2000-09-08 Henkel Kommanditgesellschaft Auf Aktien Aktivchlorhaltige zubereitungen mit färbemitteln in mikrokapseln
WO2008141847A1 (en) * 2007-05-18 2008-11-27 Unilever Plc Triphenyl methane and xanthene pigments
CN108467804A (zh) * 2018-03-27 2018-08-31 珠海市洁丽雅生物科技有限公司 一种医用杀菌洗涤剂

Families Citing this family (70)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3876551A (en) * 1972-02-14 1975-04-08 Int Flavors & Fragrances Inc Perfumed aqueous hypochlorite composition and method for preparation of same
US4005027A (en) * 1973-07-10 1977-01-25 The Procter & Gamble Company Scouring compositions
JPS565800B2 (ko) * 1973-12-11 1981-02-06
JPS5139967B2 (ko) * 1974-09-27 1976-10-30
US3996152A (en) * 1975-03-27 1976-12-07 The Procter & Gamble Company Bleaching composition
US4011172A (en) * 1975-03-27 1977-03-08 The Procter & Gamble Company Bleaching articles
US4017412A (en) * 1975-03-27 1977-04-12 The Procter & Gamble Company Bleaching composition
US4017411A (en) * 1975-03-27 1977-04-12 The Procter & Gamble Company Bleaching articles
US3989638A (en) * 1975-03-27 1976-11-02 The Procter & Gamble Company Bleaching article
JPS538604A (en) * 1976-07-14 1978-01-26 Lion Corp Colored liquid detergent composition
US4116849A (en) * 1977-03-14 1978-09-26 The Procter & Gamble Company Thickened bleach compositions for treating hard-to-remove soils
US4116851A (en) * 1977-06-20 1978-09-26 The Procter & Gamble Company Thickened bleach compositions for treating hard-to-remove soils
US4113645A (en) * 1977-07-26 1978-09-12 Polak's Frutal Works, Inc. Bleach compositions containing perfume oils
DE2849225A1 (de) * 1977-11-18 1979-05-23 Unilever Nv Giessfaehige, fluessige bleichmittel
GB2051162A (en) * 1979-05-30 1981-01-14 Reckitt & Colmann Prod Ltd Thickened aqueous alkali metal hypochlorite solutions
CH647543A5 (de) * 1980-05-13 1985-01-31 Sandoz Ag Reinigungsmittel auf hypochlorit-basis mit verdickungsmitteln.
US4335009A (en) * 1980-06-19 1982-06-15 International Flavors & Fragrances Inc. Mixture of aliphatic C10 branched olefin epoxides and use thereof in augmenting or enhancing the aroma of perfumes and/or articles
US4342663A (en) * 1980-09-18 1982-08-03 International Flavors & Fragrances, Inc. Use of mixture of aliphatic C10 branched olefins in augmenting or enhancing the aroma of articles subjected to action of aqueous hypochlorites
US4330425A (en) * 1980-06-19 1982-05-18 International Flavors & Fragrances Inc. Use of mixture of aliphatic C10 branched olefin epoxides in augmenting or enhancing the aroma of articles subjected to action of aqueous hypochlorites
US4287084A (en) * 1980-06-19 1981-09-01 International Flavors & Fragrances Inc. Use of mixture of aliphatic C10 branched olefins in augmenting or enhancing the aroma of perfumed alkaline metal hypochlorite solutions
US4339344A (en) * 1980-09-18 1982-07-13 International Flavors & Fragrances Inc. Use of mixture of aliphatic C10 -branched olefins in augmenting or enhancing the aroma of perfumes and/or perfumed articles
US4354951A (en) * 1980-10-09 1982-10-19 International Flavors & Fragrances Inc. Mixture of aliphatic C10 branched olefin epoxides and use thereof in augmenting or enhancing the aroma of perfumes and/or articles
DE3268705D1 (en) * 1981-11-07 1986-03-06 Procter & Gamble Cleaning compositions
US4388204A (en) * 1982-03-23 1983-06-14 The Drackett Company Thickened alkali metal hypochlorite compositions
GB8315838D0 (en) * 1983-06-09 1983-07-13 Unilever Plc Coloured bleaching compositions
US4599186A (en) * 1984-04-20 1986-07-08 The Clorox Company Thickened aqueous abrasive scouring cleanser
US4695394A (en) * 1984-04-20 1987-09-22 The Clorox Company Thickened aqueous cleanser
US4657692A (en) * 1984-04-20 1987-04-14 The Clorox Company Thickened aqueous abrasive scouring cleanser
US4790953A (en) * 1984-12-28 1988-12-13 The Proctor & Gamble Company Liquid hypochlorite bleach containing optical brightener solubilized by amine oxide
GB8500116D0 (en) * 1985-01-03 1985-02-13 Unilever Plc Liquid bleaching compositions
US4800036A (en) * 1985-05-06 1989-01-24 The Dow Chemical Company Aqueous bleach compositions thickened with a viscoelastic surfactant
US5427707A (en) * 1985-06-14 1995-06-27 Colgate Palmolive Co. Thixotropic aqueous compositions containing adipic or azelaic acid stabilizer
US5064553A (en) * 1989-05-18 1991-11-12 Colgate-Palmolive Co. Linear-viscoelastic aqueous liquid automatic dishwasher detergent composition
GR862954B (en) * 1986-01-07 1987-05-08 Colgate Palmolive Co Thixotropic aqueous suspensions
US4847089A (en) * 1986-07-16 1989-07-11 David N. Kramer Cleansing and distinfecting compositions, including bleaching agents, and sponges and other applicators incorporating the same
EP0256638B1 (en) * 1986-08-07 1991-01-23 The Clorox Company Thickened hypochlorite composition and use thereof
US4743395A (en) * 1986-09-12 1988-05-10 The Drackett Company Thickened acid cleaner compositions containing quaternary ammonium germicides and having improved thermal stability
GB8630845D0 (en) * 1986-12-24 1987-02-04 Ici Plc Bleaching compositions
US4789495A (en) * 1987-05-18 1988-12-06 The Drackett Company Hypochlorite compositions containing a tertiary alcohol
US4863633A (en) * 1987-08-07 1989-09-05 The Clorox Company Mitigation of stress-cracking in stacked loads of fragranced bleach-containing bottles
US5080826A (en) * 1987-08-07 1992-01-14 The Clorox Company Stable fragranced bleaching composition
US5227366A (en) * 1987-08-07 1993-07-13 The Clorox Company Mitigation of stress-cracking in fragranced bleach-containing bottles
GB8719776D0 (en) * 1987-08-21 1987-09-30 Unilever Plc Machine dishwashing compositions
US4842757A (en) * 1988-01-21 1989-06-27 The Clorox Company Thickened liquid, improved stability abrasive cleanser
GB8807752D0 (en) * 1988-03-31 1988-05-05 Unilever Plc Bleaching composition
US4917814A (en) * 1988-08-11 1990-04-17 The Drackett Company Pigmented hypochlorite compositions
CA2003857C (en) * 1988-12-15 1995-07-18 Lisa Michele Finley Stable thickened aqueous bleach compositions
US5075027A (en) * 1989-02-06 1991-12-24 Colgate Palmolive Co. Thixotropic aqueous scented automatic dishwasher detergent compositions
US4986926A (en) * 1989-04-10 1991-01-22 The Drackett Company Thickened alkali metal hypochlorite compositions
US5188752A (en) * 1991-04-22 1993-02-23 Colgate-Palmolive Company Linear viscoelastic automatic dishwasher compositions containing a crosslinked methyl vinyl ether/maleic anhydride copolymer
EP0517311A1 (en) 1991-06-07 1992-12-09 Colgate-Palmolive Company Linear viscoelastic aqueous liquid automatic dishwasher detergent composition
ZA935882B (en) * 1992-10-19 1994-03-11 Clorox Co Composition and method for developing extensional viscosity in cleaning compositions.
EP0701601B1 (en) 1993-06-01 2000-07-05 Ecolab Inc. Thickened hard surface cleaner
US5470499A (en) * 1993-09-23 1995-11-28 The Clorox Company Thickened aqueous abrasive cleanser with improved rinsability
US5728665A (en) * 1995-09-13 1998-03-17 The Clorox Company Composition and method for developing extensional viscosity in cleaning compositions
US5972866A (en) * 1997-02-05 1999-10-26 Ecolab, Inc. Thickened noncorrosive cleaner
US5985817A (en) * 1997-02-24 1999-11-16 Reckitt & Colman South Africa Ltd. Pourable, thickened aqueous bleach and abrasive containing compositions
US6258859B1 (en) * 1997-06-10 2001-07-10 Rhodia, Inc. Viscoelastic surfactant fluids and related methods of use
SE514784C2 (sv) * 1998-08-17 2001-04-23 Mediteam Dental Ab Metod och preparat för rengöring av rotytor och omgivande vävnader hos tänder
CA2280259C (en) 1998-08-26 2009-10-27 The Clorox Company Method for increasing brightness retention of laundered fabrics
SE513433C2 (sv) * 1999-01-19 2000-09-11 Mediteam Dentalutveckling I Go Preparat för kemisk-mekanisk tandbehandling innehållande en aminhaltig förening som reaktivitetsdämpande komponent
SE513404C2 (sv) * 1999-01-19 2000-09-11 Mediteam Dentalutveckling I Go Preparat för kemisk-mekanisk tandbehandling innehållande en klorförening som aktiv komponent
JP5000040B2 (ja) * 2001-01-12 2012-08-15 花王株式会社 液体漂白洗浄剤組成物
EP1233055A1 (en) * 2001-02-15 2002-08-21 Givaudan SA Bleaching composition
BRPI0607200B1 (pt) * 2005-02-16 2016-05-24 Unilever Nv composições aquosas alvejantes líquidas e método para prover atividade antimicrobiana duradoura
US20080108537A1 (en) * 2006-11-03 2008-05-08 Rees Wayne M Corrosion inhibitor system for mildly acidic to ph neutral halogen bleach-containing cleaning compositions
MX2012008499A (es) * 2010-01-21 2013-02-21 Univ South Dakota Sistemas polimericos para el suministro de sales de hipohalito.
US10208273B2 (en) 2012-09-10 2019-02-19 The Clorox Company Drain formulation for enhanced hair dissolution
US9487742B2 (en) 2012-09-10 2016-11-08 The Clorox Company Drain formulation for enhanced hair dissolution
US9637708B2 (en) 2014-02-14 2017-05-02 Ecolab Usa Inc. Reduced misting and clinging chlorine-based hard surface cleaner

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3172861A (en) * 1965-03-09 Hypochlorite bleaching compositions
GB334364A (en) * 1929-08-14 1930-09-04 Viktor Szidon Improvements in the preparation of hypochlorites of alkali metals
DE664425C (de) * 1932-02-04 1938-08-29 I G Farbenindustrie Akt Ges Verfahren zur Herstellung von Oxydationsprodukten hochmolekularer Amine
US2834737A (en) * 1957-01-15 1958-05-13 Texize Chem Inc Foaming bleach
GB886084A (en) * 1959-10-22 1962-01-03 Domestos Ltd Aqueous hypochlorite solution containing a hypochlorite-resistant perfume
DE1467665A1 (de) * 1964-11-25 1969-01-09 Carlo Pelizza Fluessige Waschmittelzusammensetzung
ZA674667B (ko) * 1966-08-11

Cited By (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2837880A1 (de) * 1977-09-02 1979-03-15 Ici Ltd Bleich- und reinigungsmittel
US4337163A (en) 1979-12-05 1982-06-29 Lever Brothers Company Liquid, thickened chlorine bleaching composition
EP0030825B1 (en) * 1979-12-06 1983-12-28 Economics Laboratory, Inc. Methods and compositions for bleaching of mycological stains
JPS5998200A (ja) * 1982-11-02 1984-06-06 インペリアル・ケミカル・インダストリ−ズ・ピ−エルシ− 漂白剤組成物
JPH0425319B2 (ko) * 1982-11-02 1992-04-30 Ici Plc
EP0137871B1 (en) * 1983-10-14 1989-10-18 The Procter & Gamble Company Cleaning compositions
US4552680A (en) * 1983-11-04 1985-11-12 The Procter & Gamble Company Hypochlorite bleach containing surfactant and organic antifoamant
US4576728A (en) * 1983-11-11 1986-03-18 The Procter & Gamble Company Cleaning compositions
US4929383A (en) * 1984-01-27 1990-05-29 The Clorox Company Stable emulstified bleaching compositions
US5104571A (en) * 1984-01-27 1992-04-14 The Clorox Company Bleaching and brightening composition and method
US5075029A (en) * 1984-01-27 1991-12-24 The Clorox Company Stable emulsified bleaching compositions
US4952333A (en) * 1984-01-27 1990-08-28 The Clorox Company Bleaching and brightening composition and method
US4708816A (en) * 1984-01-27 1987-11-24 The Clorox Company Bleach composition containing controlled density capsules
US4931207A (en) * 1984-01-27 1990-06-05 The Clorox Company Bleaching and bluing composition and method
US4783283A (en) * 1985-05-28 1988-11-08 The Procter & Gamble Company Cleaning compositions
US4828748A (en) * 1986-01-03 1989-05-09 The Drackett Company Thickened alkali metal hypochlorite compositions
US4775492A (en) * 1986-02-11 1988-10-04 Lever Brothers Company Thickened liquid bleaching composition
EP0244611A1 (en) * 1986-04-04 1987-11-11 Unilever N.V. Thickened liquid bleaching composition
US5389157A (en) * 1988-05-20 1995-02-14 The Clorox Company Viscoelastic cleaning compositions with long relaxation times
US4946619A (en) * 1988-07-19 1990-08-07 The Clorox Company Solubilization of brighter in liquid hypochlorite
US6100228A (en) * 1993-10-29 2000-08-08 The Clorox Company Bleaching gel cleaner thickened with amine oxide, soap and solvent
US5804545A (en) * 1993-11-24 1998-09-08 West Argo, Inc. Stable alkaline chlorine compositions
EP0693548A1 (en) * 1994-07-18 1996-01-24 The Procter & Gamble Company A stable concentrated premix and its use for manufacturing aqueous detergent compositions
WO2000052125A1 (de) * 1999-02-27 2000-09-08 Henkel Kommanditgesellschaft Auf Aktien Aktivchlorhaltige zubereitungen mit färbemitteln in mikrokapseln
WO2008141847A1 (en) * 2007-05-18 2008-11-27 Unilever Plc Triphenyl methane and xanthene pigments
CN108467804A (zh) * 2018-03-27 2018-08-31 珠海市洁丽雅生物科技有限公司 一种医用杀菌洗涤剂
CN108467804B (zh) * 2018-03-27 2020-05-08 珠海市洁丽雅生物科技有限公司 一种医用杀菌洗涤剂

Also Published As

Publication number Publication date
DE2042037A1 (de) 1971-03-04
NL7012822A (ko) 1971-03-02
FR2059755A1 (ko) 1971-06-04
CH542922A (de) 1973-11-30
DE2042037C3 (de) 1985-10-03
NL148103B (nl) 1975-12-15
DE2042037B2 (de) 1978-05-11
FR2059755B1 (ko) 1976-09-03
NL134221C (ko)
US3684722A (en) 1972-08-15
BE755338A (fr) 1971-02-26

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PE20 Patent expired after termination of 20 years