FI88728C - Separering av nickel fraon koppar i autoklav - Google Patents
Separering av nickel fraon koppar i autoklav Download PDFInfo
- Publication number
- FI88728C FI88728C FI871780A FI871780A FI88728C FI 88728 C FI88728 C FI 88728C FI 871780 A FI871780 A FI 871780A FI 871780 A FI871780 A FI 871780A FI 88728 C FI88728 C FI 88728C
- Authority
- FI
- Finland
- Prior art keywords
- nickel
- copper
- particles
- solution
- sulfide
- Prior art date
Links
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims description 214
- 229910052759 nickel Inorganic materials 0.000 title claims description 106
- 238000000926 separation method Methods 0.000 title claims description 25
- 238000000605 extraction Methods 0.000 claims description 102
- 239000010949 copper Substances 0.000 claims description 87
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 85
- 229910052802 copper Inorganic materials 0.000 claims description 85
- 239000000243 solution Substances 0.000 claims description 73
- 239000002184 metal Substances 0.000 claims description 58
- 229910052751 metal Inorganic materials 0.000 claims description 58
- 238000000034 method Methods 0.000 claims description 58
- 239000000460 chlorine Substances 0.000 claims description 57
- 229910052801 chlorine Inorganic materials 0.000 claims description 55
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 54
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims description 52
- 239000002245 particle Substances 0.000 claims description 52
- 239000000725 suspension Substances 0.000 claims description 52
- 239000007787 solid Substances 0.000 claims description 47
- 239000000203 mixture Substances 0.000 claims description 27
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 22
- 239000010970 precious metal Substances 0.000 claims description 18
- KZBUYRJDOAKODT-UHFFFAOYSA-N Chlorine Chemical compound ClCl KZBUYRJDOAKODT-UHFFFAOYSA-N 0.000 claims description 17
- 229910017052 cobalt Inorganic materials 0.000 claims description 16
- 239000010941 cobalt Substances 0.000 claims description 16
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims description 16
- 239000004575 stone Substances 0.000 claims description 15
- YOCUPQPZWBBYIX-UHFFFAOYSA-N copper nickel Chemical compound [Ni].[Cu] YOCUPQPZWBBYIX-UHFFFAOYSA-N 0.000 claims description 13
- 238000001556 precipitation Methods 0.000 claims description 11
- 238000004090 dissolution Methods 0.000 claims description 9
- 239000003929 acidic solution Substances 0.000 claims description 8
- BWFPGXWASODCHM-UHFFFAOYSA-N copper monosulfide Chemical compound [Cu]=S BWFPGXWASODCHM-UHFFFAOYSA-N 0.000 claims description 7
- 238000011084 recovery Methods 0.000 claims description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 5
- 239000001301 oxygen Substances 0.000 claims description 5
- 229910052760 oxygen Inorganic materials 0.000 claims description 5
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 4
- 239000007789 gas Substances 0.000 claims description 4
- 239000007900 aqueous suspension Substances 0.000 claims description 3
- OMZSGWSJDCOLKM-UHFFFAOYSA-N copper(II) sulfide Chemical compound [S-2].[Cu+2] OMZSGWSJDCOLKM-UHFFFAOYSA-N 0.000 claims description 3
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims description 2
- 239000007788 liquid Substances 0.000 claims description 2
- 239000011593 sulfur Substances 0.000 claims description 2
- 229910052717 sulfur Inorganic materials 0.000 claims description 2
- 229910021586 Nickel(II) chloride Inorganic materials 0.000 claims 11
- QMMRZOWCJAIUJA-UHFFFAOYSA-L nickel dichloride Chemical compound Cl[Ni]Cl QMMRZOWCJAIUJA-UHFFFAOYSA-L 0.000 claims 11
- 239000003570 air Substances 0.000 claims 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- 241000283073 Equus caballus Species 0.000 claims 1
- 239000012080 ambient air Substances 0.000 claims 1
- 239000011449 brick Substances 0.000 claims 1
- 210000000078 claw Anatomy 0.000 claims 1
- 238000010924 continuous production Methods 0.000 claims 1
- 229910000365 copper sulfate Inorganic materials 0.000 claims 1
- 125000001033 ether group Chemical group 0.000 claims 1
- 239000000463 material Substances 0.000 claims 1
- 239000011343 solid material Substances 0.000 claims 1
- WWNBZGLDODTKEM-UHFFFAOYSA-N sulfanylidenenickel Chemical compound [Ni]=S WWNBZGLDODTKEM-UHFFFAOYSA-N 0.000 claims 1
- 239000011435 rock Substances 0.000 description 38
- 239000000956 alloy Substances 0.000 description 11
- 229910045601 alloy Inorganic materials 0.000 description 11
- 229910000570 Cupronickel Inorganic materials 0.000 description 6
- 238000003756 stirring Methods 0.000 description 6
- 150000004763 sulfides Chemical class 0.000 description 6
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 239000012141 concentrate Substances 0.000 description 5
- 238000002474 experimental method Methods 0.000 description 5
- 239000000706 filtrate Substances 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 230000002378 acidificating effect Effects 0.000 description 3
- 238000002347 injection Methods 0.000 description 3
- 239000007924 injection Substances 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000003723 Smelting Methods 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 238000007792 addition Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000005868 electrolysis reaction Methods 0.000 description 2
- 239000012527 feed solution Substances 0.000 description 2
- -1 ferrous metals Chemical class 0.000 description 2
- 239000000543 intermediate Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
- MBMLMWLHJBBADN-UHFFFAOYSA-N Ferrous sulfide Chemical compound [Fe]=S MBMLMWLHJBBADN-UHFFFAOYSA-N 0.000 description 1
- 235000019738 Limestone Nutrition 0.000 description 1
- 101000986989 Naja kaouthia Acidic phospholipase A2 CM-II Proteins 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- 229910052770 Uranium Inorganic materials 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- INPLXZPZQSLHBR-UHFFFAOYSA-N cobalt(2+);sulfide Chemical compound [S-2].[Co+2] INPLXZPZQSLHBR-UHFFFAOYSA-N 0.000 description 1
- 239000013256 coordination polymer Substances 0.000 description 1
- IYRDVAUFQZOLSB-UHFFFAOYSA-N copper iron Chemical compound [Fe].[Cu] IYRDVAUFQZOLSB-UHFFFAOYSA-N 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- HZPCELLLBIXAIO-UHFFFAOYSA-L dichlorocopper nickel Chemical compound [Ni].Cl[Cu]Cl HZPCELLLBIXAIO-UHFFFAOYSA-L 0.000 description 1
- ZOMNIUBKTOKEHS-UHFFFAOYSA-L dimercury dichloride Chemical class Cl[Hg][Hg]Cl ZOMNIUBKTOKEHS-UHFFFAOYSA-L 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000009854 hydrometallurgy Methods 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009533 lab test Methods 0.000 description 1
- 239000006028 limestone Substances 0.000 description 1
- 239000006193 liquid solution Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 210000000582 semen Anatomy 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 229910021653 sulphate ion Inorganic materials 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B23/00—Obtaining nickel or cobalt
- C22B23/04—Obtaining nickel or cobalt by wet processes
- C22B23/0407—Leaching processes
- C22B23/0415—Leaching processes with acids or salt solutions except ammonium salts solutions
- C22B23/0423—Halogenated acids or salts thereof
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Applications Claiming Priority (4)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US06/855,897 US4828809A (en) | 1983-10-18 | 1986-04-24 | Separation of nickel from copper in autoclave |
| US85589786 | 1986-04-24 | ||
| CA539730 | 1987-06-15 | ||
| CA 539730 CA1327452C (en) | 1986-04-24 | 1987-06-15 | Separation of nickel from copper in autoclave |
Publications (4)
| Publication Number | Publication Date |
|---|---|
| FI871780A0 FI871780A0 (fi) | 1987-04-23 |
| FI871780L FI871780L (fi) | 1987-10-25 |
| FI88728B FI88728B (fi) | 1993-03-15 |
| FI88728C true FI88728C (fi) | 1993-06-28 |
Family
ID=25671382
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FI871780A FI88728C (fi) | 1986-04-24 | 1987-04-23 | Separering av nickel fraon koppar i autoklav |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP0248518B1 (forum.php) |
| JP (1) | JP2552136B2 (forum.php) |
| AU (1) | AU589519B2 (forum.php) |
| CA (1) | CA1327452C (forum.php) |
| FI (1) | FI88728C (forum.php) |
| NO (1) | NO173613C (forum.php) |
| ZA (1) | ZA872869B (forum.php) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA2137124C (en) * | 1994-12-01 | 1999-03-16 | Tao Xue | Pressure leaching of nickel and cobalt sulphides with chlorine under controlled redox potential conditions |
| US6428604B1 (en) * | 2000-09-18 | 2002-08-06 | Inco Limited | Hydrometallurgical process for the recovery of nickel and cobalt values from a sulfidic flotation concentrate |
| AU2005245514A1 (en) * | 2004-05-21 | 2005-12-01 | Wmc Resources Ltd | Recovery of nickel |
| JP4924754B2 (ja) * | 2010-06-21 | 2012-04-25 | 住友金属鉱山株式会社 | 含銅塩化ニッケル溶液の銅イオン除去方法並びに電気ニッケルの製造方法 |
| JP5803492B2 (ja) * | 2011-09-22 | 2015-11-04 | 住友金属鉱山株式会社 | 金属硫化物の塩素浸出方法 |
| JP5803491B2 (ja) * | 2011-09-22 | 2015-11-04 | 住友金属鉱山株式会社 | 金属硫化物の塩素浸出方法、並びに金属の湿式製錬方法 |
| JP5884870B1 (ja) * | 2014-08-13 | 2016-03-15 | 住友金属鉱山株式会社 | ニッケルの回収方法 |
| JP6540548B2 (ja) * | 2016-03-01 | 2019-07-10 | 住友金属鉱山株式会社 | 塩化ニッケル水溶液の銅イオン除去方法、銅イオン除去処理装置 |
| JP6897466B2 (ja) | 2017-09-29 | 2021-06-30 | 住友金属鉱山株式会社 | 銅とニッケルおよびコバルトの分離方法 |
| JP6519628B2 (ja) | 2017-10-23 | 2019-05-29 | 住友金属鉱山株式会社 | 銅とニッケルおよびコバルトの分離方法 |
| JP6915497B2 (ja) | 2017-10-23 | 2021-08-04 | 住友金属鉱山株式会社 | 銅とニッケルおよびコバルトの分離方法 |
| JP6939506B2 (ja) | 2017-12-18 | 2021-09-22 | 住友金属鉱山株式会社 | 銅とニッケルおよびコバルトの分離方法 |
| CN108977662A (zh) * | 2018-07-13 | 2018-12-11 | 兰州金川新材料科技股份有限公司 | 一种利用钴铁合金制备氯化钴溶液和硫酸铜溶液的方法 |
| CN109762986A (zh) * | 2019-03-20 | 2019-05-17 | 金川集团股份有限公司 | 一种从镍电解铜渣中提取镍的装置及其方法 |
| KR20220127893A (ko) | 2020-02-21 | 2022-09-20 | 스미토모 긴조쿠 고잔 가부시키가이샤 | 합금의 처리 방법 |
| JP7604806B2 (ja) | 2020-08-17 | 2024-12-24 | 住友金属鉱山株式会社 | 硫化物の処理方法 |
| CN112095016B (zh) * | 2020-08-27 | 2022-06-10 | 矿冶科技集团有限公司 | 一种高冰镍浸出渣热压处理降低镍含量的方法 |
| JP7245423B1 (ja) | 2021-09-29 | 2023-03-24 | 住友金属鉱山株式会社 | 合金の処理方法 |
| CN113957243B (zh) * | 2021-10-22 | 2023-10-17 | 金川镍钴研究设计院有限责任公司 | 实现高镍锍中镍、铜、铁分别开路并富集贵金属的方法 |
| WO2023106210A1 (ja) | 2021-12-06 | 2023-06-15 | 住友金属鉱山株式会社 | 合金の処理方法 |
| JP2024024163A (ja) | 2022-08-09 | 2024-02-22 | 住友金属鉱山株式会社 | 廃電池の処理方法 |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR367717A (fr) * | 1906-07-04 | 1906-11-08 | Metals Extraction Corp Ltd | Procédé pour l'extraction et la récupération de cobalt et de nickel, de minerais et de mattes oxydées |
| FR441785A (fr) * | 1911-07-08 | 1912-08-16 | Alexander Mckechnie | Procédé de traitement des mattes de nickel-cuivre |
| US3085054A (en) * | 1960-02-25 | 1963-04-09 | Falconbridge Nickel Mines Ltd | Recovery of nickel |
| GB1456065A (en) * | 1971-03-18 | 1976-11-17 | Falconbridge Nickel Mines Ltd | Oxygen-acid leach process |
| US3880653A (en) * | 1971-03-18 | 1975-04-29 | Falconbridge Nickel Mines Ltd | Chlorine leach process |
| US3975189A (en) * | 1971-03-18 | 1976-08-17 | Falconbridge Nickel Mines Limited | Recovery of copper sulphide and nickel from solution |
| GB1401615A (en) * | 1971-07-16 | 1975-07-16 | Int Nickel Canada | Roorda h j extraction of non-ferrous metals from iron-containing materials |
| CA970166A (en) * | 1972-04-17 | 1975-07-01 | James A.E. Bell | Preferential sulfiding of nickel and cobalt oxides |
| AU487488B2 (en) * | 1975-06-02 | 1976-12-09 | Falconbridge Limited | Copper sulphide precipitation from nickeliferous solution containing dissolved copper |
| US3981962A (en) * | 1975-06-30 | 1976-09-21 | The United States Of America As Represented By The Secretary Of The Interior | Decomposition leach of sulfide ores with chlorine and oxygen |
| FR2340376A1 (fr) * | 1976-02-06 | 1977-09-02 | Minemet Rech Sa | Procede hydrometallurgique pour la dissolution selective de melanges de composes oxygenes |
| DE2840424A1 (de) * | 1978-09-16 | 1980-04-24 | Duisburger Kupferhuette | Verfahren zur herstellung von sulfidischen kupferkonzentraten |
| US4384940A (en) * | 1982-01-21 | 1983-05-24 | Inco Limited | Chlorine leaching of nickel-cobalt-iron sulphides |
| CA1193107A (en) * | 1982-09-28 | 1985-09-10 | Robert W. Stanley | Process for the selective dissolution of cobalt from cobaltite-pyrite concentrates |
| NO833784L (no) * | 1983-10-18 | 1985-04-19 | Thomas Thomassen | Autoklav-klorluting av kobbersulfidkonsentrater |
-
1987
- 1987-04-23 ZA ZA872869A patent/ZA872869B/xx unknown
- 1987-04-23 EP EP19870303580 patent/EP0248518B1/en not_active Expired - Lifetime
- 1987-04-23 FI FI871780A patent/FI88728C/fi not_active IP Right Cessation
- 1987-04-23 NO NO871686A patent/NO173613C/no unknown
- 1987-04-24 AU AU71952/87A patent/AU589519B2/en not_active Expired
- 1987-04-24 JP JP10024087A patent/JP2552136B2/ja not_active Expired - Lifetime
- 1987-06-15 CA CA 539730 patent/CA1327452C/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| FI871780L (fi) | 1987-10-25 |
| NO173613C (no) | 1994-01-05 |
| EP0248518A1 (en) | 1987-12-09 |
| AU589519B2 (en) | 1989-10-12 |
| CA1327452C (en) | 1994-03-08 |
| NO871686L (no) | 1987-10-26 |
| EP0248518B1 (en) | 1991-11-13 |
| ZA872869B (forum.php) | 1987-10-12 |
| NO173613B (no) | 1993-09-27 |
| AU7195287A (en) | 1987-10-29 |
| FI871780A0 (fi) | 1987-04-23 |
| JP2552136B2 (ja) | 1996-11-06 |
| NO871686D0 (no) | 1987-04-23 |
| JPS63259033A (ja) | 1988-10-26 |
| FI88728B (fi) | 1993-03-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| BB | Publication of examined application | ||
| FG | Patent granted |
Owner name: FALCONBRIDGE LIMITED |
|
| MA | Patent expired |