FI57773C - Ammoniumsalter av sulfonsyragrupper innehaollande stilbenazo- och/eller stilbenazoxifaergaemnen - Google Patents
Ammoniumsalter av sulfonsyragrupper innehaollande stilbenazo- och/eller stilbenazoxifaergaemnen Download PDFInfo
- Publication number
- FI57773C FI57773C FI65173A FI65173A FI57773C FI 57773 C FI57773 C FI 57773C FI 65173 A FI65173 A FI 65173A FI 65173 A FI65173 A FI 65173A FI 57773 C FI57773 C FI 57773C
- Authority
- FI
- Finland
- Prior art keywords
- dyes
- parts
- lithium
- ammonium
- salts
- Prior art date
Links
- 239000000975 dye Substances 0.000 claims description 48
- 150000003863 ammonium salts Chemical class 0.000 claims description 21
- 239000000203 mixture Substances 0.000 claims description 18
- 229910003002 lithium salt Inorganic materials 0.000 claims description 13
- 159000000002 lithium salts Chemical class 0.000 claims description 13
- 125000000542 sulfonic acid group Chemical class 0.000 claims description 10
- 150000001768 cations Chemical class 0.000 claims description 9
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 7
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 claims description 5
- 229940006487 lithium cation Drugs 0.000 claims description 4
- 150000003839 salts Chemical class 0.000 claims description 3
- 238000004043 dyeing Methods 0.000 claims description 2
- BDHFUVZGWQCTTF-UHFFFAOYSA-N sulfonic acid Chemical class OS(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-N 0.000 claims description 2
- 229910006146 SO3M1 Inorganic materials 0.000 claims 3
- 150000002500 ions Chemical class 0.000 claims 2
- 229910001416 lithium ion Inorganic materials 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 18
- PJANXHGTPQOBST-VAWYXSNFSA-N Stilbene Natural products C=1C=CC=CC=1/C=C/C1=CC=CC=C1 PJANXHGTPQOBST-VAWYXSNFSA-N 0.000 description 13
- 235000021286 stilbenes Nutrition 0.000 description 13
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 12
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 8
- 239000000987 azo dye Substances 0.000 description 7
- 238000006243 chemical reaction Methods 0.000 description 7
- 235000019270 ammonium chloride Nutrition 0.000 description 6
- 229910052744 lithium Inorganic materials 0.000 description 6
- 239000000725 suspension Substances 0.000 description 6
- 239000003086 colorant Substances 0.000 description 5
- -1 lithium cations Chemical class 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- PJANXHGTPQOBST-UHFFFAOYSA-N stilbene Chemical compound C=1C=CC=CC=1C=CC1=CC=CC=C1 PJANXHGTPQOBST-UHFFFAOYSA-N 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 239000002250 absorbent Substances 0.000 description 3
- 230000002745 absorbent Effects 0.000 description 3
- 229920002678 cellulose Polymers 0.000 description 3
- 239000001913 cellulose Substances 0.000 description 3
- PQVSTLUFSYVLTO-UHFFFAOYSA-N ethyl n-ethoxycarbonylcarbamate Chemical compound CCOC(=O)NC(=O)OCC PQVSTLUFSYVLTO-UHFFFAOYSA-N 0.000 description 3
- GLXDVVHUTZTUQK-UHFFFAOYSA-M lithium hydroxide monohydrate Substances [Li+].O.[OH-] GLXDVVHUTZTUQK-UHFFFAOYSA-M 0.000 description 3
- 229940040692 lithium hydroxide monohydrate Drugs 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 238000010186 staining Methods 0.000 description 3
- 239000001043 yellow dye Substances 0.000 description 3
- SPFMQWBKVUQXJV-BTVCFUMJSA-N (2r,3s,4r,5r)-2,3,4,5,6-pentahydroxyhexanal;hydrate Chemical compound O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O SPFMQWBKVUQXJV-BTVCFUMJSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 2
- 235000011130 ammonium sulphate Nutrition 0.000 description 2
- 235000012000 cholesterol Nutrition 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000010893 paper waste Substances 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 2
- 229910021653 sulphate ion Inorganic materials 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- ZDTXQHVBLWYPHS-UHFFFAOYSA-N 4-nitrotoluene-2-sulfonic acid Chemical compound CC1=CC=C([N+]([O-])=O)C=C1S(O)(=O)=O ZDTXQHVBLWYPHS-UHFFFAOYSA-N 0.000 description 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-M Acetate Chemical compound CC([O-])=O QTBSBXVTEAMEQO-UHFFFAOYSA-M 0.000 description 1
- USFZMSVCRYTOJT-UHFFFAOYSA-N Ammonium acetate Chemical compound N.CC(O)=O USFZMSVCRYTOJT-UHFFFAOYSA-N 0.000 description 1
- 239000005695 Ammonium acetate Substances 0.000 description 1
- 239000004254 Ammonium phosphate Substances 0.000 description 1
- 235000018185 Betula X alpestris Nutrition 0.000 description 1
- 235000018212 Betula X uliginosa Nutrition 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 229920001131 Pulp (paper) Polymers 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 description 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 238000004026 adhesive bonding Methods 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 235000013334 alcoholic beverage Nutrition 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 229940043376 ammonium acetate Drugs 0.000 description 1
- 235000019257 ammonium acetate Nutrition 0.000 description 1
- 229910000148 ammonium phosphate Inorganic materials 0.000 description 1
- 235000019289 ammonium phosphates Nutrition 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 239000001166 ammonium sulphate Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 238000000502 dialysis Methods 0.000 description 1
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 239000000834 fixative Substances 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 235000015203 fruit juice Nutrition 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000001048 orange dye Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 239000011122 softwood Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B56/00—Azo dyes containing other chromophoric systems
- C09B56/04—Stilbene-azo dyes
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Paper (AREA)
- Coloring (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CH347772A CH569065A5 (enrdf_load_stackoverflow) | 1972-03-09 | 1972-03-09 | |
CH347772 | 1972-03-09 |
Publications (2)
Publication Number | Publication Date |
---|---|
FI57773B FI57773B (fi) | 1980-06-30 |
FI57773C true FI57773C (fi) | 1980-10-10 |
Family
ID=4256813
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FI65173A FI57773C (fi) | 1972-03-09 | 1973-03-02 | Ammoniumsalter av sulfonsyragrupper innehaollande stilbenazo- och/eller stilbenazoxifaergaemnen |
Country Status (8)
Country | Link |
---|---|
JP (1) | JPS48102125A (enrdf_load_stackoverflow) |
CH (1) | CH569065A5 (enrdf_load_stackoverflow) |
DE (1) | DE2311072C3 (enrdf_load_stackoverflow) |
FI (1) | FI57773C (enrdf_load_stackoverflow) |
FR (1) | FR2175107B1 (enrdf_load_stackoverflow) |
GB (1) | GB1420381A (enrdf_load_stackoverflow) |
IT (1) | IT979778B (enrdf_load_stackoverflow) |
SE (1) | SE389125B (enrdf_load_stackoverflow) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CH606290A5 (enrdf_load_stackoverflow) | 1972-03-17 | 1978-10-31 | Sandoz Ag | |
DE2601470C2 (de) * | 1976-01-16 | 1977-04-28 | Bayer Ag | Verfahren zur Herstellung von Kondensationsfarbstoffen |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR734932A (fr) * | 1931-04-18 | 1932-10-31 | Ig Farbenindustrie Ag | Perfectionnements aux colorants, acides et substantifs employés dans la teinture du cuir |
US2865908A (en) * | 1954-10-25 | 1958-12-23 | American Cyanamid Co | Stilbene azo dyes |
US3122529A (en) * | 1959-11-16 | 1964-02-25 | Gen Aniline & Film Corp | Preparation of stilbene azo dyes |
-
1972
- 1972-03-09 CH CH347772A patent/CH569065A5/xx not_active IP Right Cessation
-
1973
- 1973-03-01 SE SE7302899A patent/SE389125B/xx unknown
- 1973-03-02 FI FI65173A patent/FI57773C/fi active
- 1973-03-06 GB GB1071473A patent/GB1420381A/en not_active Expired
- 1973-03-06 DE DE19732311072 patent/DE2311072C3/de not_active Expired
- 1973-03-07 FR FR7308045A patent/FR2175107B1/fr not_active Expired
- 1973-03-07 JP JP2625173A patent/JPS48102125A/ja active Pending
- 1973-03-09 IT IT4869573A patent/IT979778B/it active
Also Published As
Publication number | Publication date |
---|---|
FR2175107B1 (enrdf_load_stackoverflow) | 1977-02-04 |
DE2311072C3 (de) | 1978-12-21 |
DE2311072B2 (de) | 1978-05-03 |
CH569065A5 (enrdf_load_stackoverflow) | 1975-11-14 |
FR2175107A1 (enrdf_load_stackoverflow) | 1973-10-19 |
JPS48102125A (enrdf_load_stackoverflow) | 1973-12-22 |
DE2311072A1 (de) | 1973-09-13 |
IT979778B (it) | 1974-09-30 |
SE389125B (sv) | 1976-10-25 |
GB1420381A (en) | 1976-01-07 |
FI57773B (fi) | 1980-06-30 |
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