ES8301841A1 - Un procedimiento para la separacion de urea, amoniaco y dio-xido de carbono a partir de soluciones acuosas diluidas. - Google Patents

Un procedimiento para la separacion de urea, amoniaco y dio-xido de carbono a partir de soluciones acuosas diluidas.

Info

Publication number
ES8301841A1
ES8301841A1 ES507512A ES507512A ES8301841A1 ES 8301841 A1 ES8301841 A1 ES 8301841A1 ES 507512 A ES507512 A ES 507512A ES 507512 A ES507512 A ES 507512A ES 8301841 A1 ES8301841 A1 ES 8301841A1
Authority
ES
Spain
Prior art keywords
urea
ammonia
carbon dioxide
removal
aqueous solutions
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES507512A
Other languages
English (en)
Other versions
ES507512A0 (es
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Unie Van Kunstmestfabrieken BV
Original Assignee
Unie Van Kunstmestfabrieken BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Unie Van Kunstmestfabrieken BV filed Critical Unie Van Kunstmestfabrieken BV
Publication of ES507512A0 publication Critical patent/ES507512A0/es
Publication of ES8301841A1 publication Critical patent/ES8301841A1/es
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/26—Fractionating columns in which vapour and liquid flow past each other, or in which the fluid is sprayed into the vapour, or in which a two-phase mixture is passed in one direction
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00—Multistage treatment of water, waste water or sewage
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/58—Treatment of water, waste water, or sewage by removing specified dissolved compounds
    • C02F1/586—Treatment of water, waste water, or sewage by removing specified dissolved compounds by removing ammoniacal nitrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/02—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds
    • C07C273/04—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of urea, its salts, complexes or addition compounds from carbon dioxide and ammonia
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/025—Thermal hydrolysis
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/02—Treatment of water, waste water, or sewage by heating
    • C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
    • C02F1/048—Purification of waste water by evaporation
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/58—Treatment of water, waste water, or sewage by removing specified dissolved compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/16—Nitrogen compounds, e.g. ammonia

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Water Supply & Treatment (AREA)
  • Engineering & Computer Science (AREA)
  • Hydrology & Water Resources (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Gas Separation By Absorption (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Treating Waste Gases (AREA)

Abstract

PROCEDIMIENTO PARA LA SEPARACION DE UREA, AMONIACO Y DIOXIDO DE CARBONO, A PARTIR DE DISOLUCIONES ACUOSAS DILUIDAS POR HIDROLISIS DE UREA, SEGUIDA POR DESORCION DE AMONIACO Y DIOXIDO DE CARBONO. CONSISTE EN PASAR LA DISOLUCION, A UNA PRESION ENTRE 10 Y 30 BARES, AL INTERIOR DE LA PARTE SUPERIOR DE UNA COLUMNA DE REACCION; HACERLA FLUIR EN DIRECCION DESCENDENTE EN CONTRACORRIENTE CON UNA CORRIENTE DE GASES; MANTENIENDO EN LA PARTE SUPERIOR DE LA COLUMNA UNA TEMPERATURA ENTRE 170<025>C Y 220<025>C Y EN EL FONDO ENTRE 180<025>C Y 230<025>C. RETIRAR DEL EXTREMO SUPERIOR DE LA COLUMNA UNA MEZCLA GASEOSA QUE CONTIENE AMONIACO, DIOXIDO DE CARBONO Y VAPOR DE AGUA; Y POR EL FONDO UNA DISOLUCION DE AMONIACO Y DIOXIDO DE CARBONO.
ES507512A 1980-11-28 1981-11-27 Un procedimiento para la separacion de urea, amoniaco y dio-xido de carbono a partir de soluciones acuosas diluidas. Expired ES8301841A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL8006477A NL8006477A (nl) 1980-11-28 1980-11-28 Werkwijze voor het verwijderen van ureum, ammoniak en kooldioxide uit verdunde waterige oplossing.

Publications (2)

Publication Number Publication Date
ES507512A0 ES507512A0 (es) 1983-01-01
ES8301841A1 true ES8301841A1 (es) 1983-01-01

Family

ID=19836250

Family Applications (1)

Application Number Title Priority Date Filing Date
ES507512A Expired ES8301841A1 (es) 1980-11-28 1981-11-27 Un procedimiento para la separacion de urea, amoniaco y dio-xido de carbono a partir de soluciones acuosas diluidas.

Country Status (33)

Country Link
US (1) US4456535A (es)
EP (1) EP0053410B1 (es)
JP (1) JPS57118011A (es)
KR (2) KR860000189B1 (es)
AU (1) AU547371B2 (es)
BR (1) BR8107728A (es)
CA (1) CA1201726A (es)
CS (1) CS227021B2 (es)
CU (1) CU21419A (es)
DE (1) DE3171612D1 (es)
ES (1) ES8301841A1 (es)
FI (1) FI74947C (es)
GR (1) GR75396B (es)
HU (1) HU188717B (es)
IE (1) IE53218B1 (es)
IL (1) IL64392A (es)
IN (1) IN156310B (es)
MA (1) MA19335A1 (es)
MY (1) MY8600489A (es)
NL (1) NL8006477A (es)
NO (1) NO154749C (es)
NZ (1) NZ199085A (es)
OA (1) OA06958A (es)
PH (1) PH19196A (es)
PL (1) PL134841B1 (es)
PT (1) PT74046B (es)
RO (1) RO83971B (es)
SG (1) SG100285G (es)
SU (1) SU1378781A3 (es)
TR (1) TR21827A (es)
YU (1) YU41999B (es)
ZA (1) ZA818269B (es)
ZW (1) ZW28781A1 (es)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4522727A (en) * 1984-10-22 1985-06-11 Atec Inc. Process for continuous removal of ammoniacal nitrogen from aqueous streams
AT388157B (de) * 1987-07-16 1989-05-10 Vogelbusch Gmbh Verfahren zur aufbereitung von ammoniak und/oder sonstige geruchsaktive substanzen sowie feststoffe enthaltenden organisch belasteten abwaessern
NL8702530A (nl) * 1987-10-23 1989-05-16 Stamicarbon Werkwijze voor de bereiding van ureum en water uitgaande van ammoniak en kooldioxide.
IT1232670B (it) * 1989-09-15 1992-03-02 Snam Progetti Procedimento per la purificazione delle acque reflue prodotte dagli impianti di produzione dell'urea.
RU2056408C1 (ru) * 1991-10-23 1996-03-20 Уриа Казале С.А. Способ гидролиза мочевины, содержащейся в отработанной воде с установок синтеза мочевины, и колонный аппарат для его осуществления
US5525237A (en) * 1993-12-23 1996-06-11 United Technologies Corporation Process for removing free and dissolved CO2 from aqueous solutions
US5518626A (en) * 1993-12-23 1996-05-21 United Technologies Corporation Process employing thermally sterilizable aqueous polishing agents
US5597454A (en) * 1995-04-06 1997-01-28 Lee; Jing M. Process for producing urea
KR100398799B1 (ko) * 2001-04-04 2003-09-19 한화석유화학 주식회사 질소 함유 유기물을 포함하는 폐수의 처리공정
US6761868B2 (en) * 2001-05-16 2004-07-13 The Chemithon Corporation Process for quantitatively converting urea to ammonia on demand
US6755029B2 (en) 2002-01-08 2004-06-29 Marvin Ralph Bertrand, Jr. Ammonia separator and neutralizer
US20040177644A1 (en) * 2002-01-08 2004-09-16 Masterson James A. Method and apparatus for separating and neutralizing ammonia
US7272953B2 (en) * 2002-01-08 2007-09-25 Masterson James A Method and apparatus for separating and neutralizing ammonia
US6887449B2 (en) * 2002-11-21 2005-05-03 The Chemithon Corporation Method of quantitatively producing ammonia from urea
CN100400430C (zh) * 2006-05-18 2008-07-09 刘国胜 尿素工艺冷凝液节能净化回收工艺
EP2386346A1 (en) 2010-05-11 2011-11-16 Stamicarbon B.V. Process for the reduction of ammonia emissions in a urea manufacturing process
JP6634342B2 (ja) * 2016-05-24 2020-01-22 東洋エンジニアリング株式会社 尿素水溶液の処理方法および装置
EP3665152A1 (en) * 2017-08-11 2020-06-17 Nouryon Chemicals International B.V. Process for converting cyclic alkylene ureas into their corresponding alkylene amines
DE102019208859A1 (de) * 2019-06-18 2020-12-24 Skw Stickstoffwerke Piesteritz Gmbh Verfahren zur kontinuierlichen Herstellung reiner Harnstofflösungen durch Verwertung von Prozesswasser
CN111137906A (zh) * 2020-03-13 2020-05-12 安徽六国化工股份有限公司 一种尿素稀尿溶液处理装置及方法
CN112744945A (zh) * 2020-11-30 2021-05-04 安徽金禾实业股份有限公司 三氯蔗糖精馏废水氧化碱解的方法及装置

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE146751C (es) *
DE146752C (es) *
US3390058A (en) * 1964-06-08 1968-06-25 Toyo Koatsu Ind Inc Plural stage pressure distillation of urea synthesis effluent with liquified gas addition
ES318356A1 (es) * 1964-10-16 1966-05-16 Toyo Koatsu Ind Incorporated Metodo de depuracion de un efluente en la obtencion de urea sintetica.
US4341640A (en) * 1976-09-27 1982-07-27 Standard Oil Company Urea hydrolysis
JPS5826909B2 (ja) * 1979-09-14 1983-06-06 東洋エンジニアリング株式会社 尿素水溶液の濃縮方法

Also Published As

Publication number Publication date
IE812785L (en) 1982-05-28
IL64392A0 (en) 1982-02-28
NO814070L (no) 1982-06-01
US4456535A (en) 1984-06-26
AU7794181A (en) 1982-06-03
KR830007109A (ko) 1983-10-14
FI813811L (fi) 1982-05-29
YU274181A (en) 1983-02-28
NO154749C (no) 1986-12-17
FI74947C (fi) 1988-04-11
NL8006477A (nl) 1982-06-16
TR21827A (tr) 1985-08-15
RO83971A (ro) 1984-06-21
CA1201726A (en) 1986-03-11
ES507512A0 (es) 1983-01-01
HU188717B (en) 1986-05-28
SU1378781A3 (ru) 1988-02-28
SG100285G (en) 1986-07-18
EP0053410B1 (en) 1985-07-31
RO83971B (ro) 1984-08-30
IL64392A (en) 1984-10-31
PT74046A (fr) 1981-12-01
NZ199085A (en) 1985-08-30
GR75396B (es) 1984-07-13
MA19335A1 (fr) 1982-07-01
ZW28781A1 (en) 1982-02-24
JPS57118011A (en) 1982-07-22
OA06958A (fr) 1983-07-31
PT74046B (fr) 1983-04-26
KR860000189B1 (ko) 1986-03-03
DE3171612D1 (en) 1985-09-05
MY8600489A (en) 1986-12-31
AU547371B2 (en) 1985-10-17
PH19196A (en) 1986-01-28
IN156310B (es) 1985-06-22
PL134841B1 (en) 1985-09-30
ZA818269B (en) 1983-06-29
FI74947B (fi) 1987-12-31
EP0053410A1 (en) 1982-06-09
BR8107728A (pt) 1982-08-31
CU21419A (es) 1983-12-21
NO154749B (no) 1986-09-08
IE53218B1 (en) 1988-09-14
PL234005A1 (es) 1982-06-21
YU41999B (en) 1988-04-30
CS227021B2 (en) 1984-04-16

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