ES478008A1 - Procedimiento para preparar cicloalcanoles y cicloalcanonas. - Google Patents

Procedimiento para preparar cicloalcanoles y cicloalcanonas.

Info

Publication number
ES478008A1
ES478008A1 ES478008A ES478008A ES478008A1 ES 478008 A1 ES478008 A1 ES 478008A1 ES 478008 A ES478008 A ES 478008A ES 478008 A ES478008 A ES 478008A ES 478008 A1 ES478008 A1 ES 478008A1
Authority
ES
Spain
Prior art keywords
cycloalkanones
cycloalkanols
cycloalkyl hydroperoxide
organic phase
neutralized
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES478008A
Other languages
English (en)
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Stamicarbon BV
Original Assignee
Stamicarbon BV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Stamicarbon BV filed Critical Stamicarbon BV
Publication of ES478008A1 publication Critical patent/ES478008A1/es
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
    • C07C45/53—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of hydroperoxides
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/132—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of an oxygen containing functional group
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Procedimiento para preparar cicloalconoles y cicloalcanonas por oxidación, en fase líquida, de un cicloalcano de 5 a 12 átomos de carbono en el anillo, mediante un gas que contiene oxígeno molecular, obteniendo así una mezcla de oxidación que contiene hidroperóxido de cicloalcohilo, la cual mezcla de oxidación, en la etapa b), se trata, en presencia de una solución acuosa de un hidróxido de metal alcalino, con una sal metálica que causa la descomposición del hidroperóxido de cicloalcohilo, caracterizado porque, antes del tratamiento con la sal metálica en la etapa b), los ácidos presentes en la mezcla de oxidación son parcial o totalmente neutralizados en la etapa a).
ES478008A 1978-02-25 1979-02-23 Procedimiento para preparar cicloalcanoles y cicloalcanonas. Expired ES478008A1 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL7802125A NL7802125A (nl) 1978-02-25 1978-02-25 Werkwijze voor het bereiden van cycloalkanolen en cycloalkanonen.

Publications (1)

Publication Number Publication Date
ES478008A1 true ES478008A1 (es) 1979-07-01

Family

ID=19830398

Family Applications (1)

Application Number Title Priority Date Filing Date
ES478008A Expired ES478008A1 (es) 1978-02-25 1979-02-23 Procedimiento para preparar cicloalcanoles y cicloalcanonas.

Country Status (13)

Country Link
US (1) US4238415A (es)
EP (1) EP0004105B1 (es)
JP (1) JPS54135748A (es)
AR (1) AR219789A1 (es)
BR (1) BR7901214A (es)
CA (1) CA1118453A (es)
CS (1) CS227668B2 (es)
DE (1) DE2960603D1 (es)
ES (1) ES478008A1 (es)
IN (1) IN150726B (es)
MX (1) MX5676E (es)
NL (1) NL7802125A (es)
PL (1) PL114149B1 (es)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS57169438A (en) * 1981-04-14 1982-10-19 Ube Ind Ltd Preparation of cyclohexanol and cyclohexanone
NL8201695A (nl) * 1982-04-23 1983-11-16 Stamicarbon Werkwijze voor de bereiding van cyclohexanol en cyclohexanon.
DE3403410A1 (de) * 1984-02-01 1985-08-01 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen herstellung von cyclohexylhydroperoxid sowie cyclohexanol und cyclohexanon enthaltenden gemischen
US5206441A (en) * 1992-04-06 1993-04-27 E. I. Du Pont De Nemours And Company High rate process for preparation of cyclohexanol and cyclohexanone
BE1007904A3 (nl) * 1993-12-23 1995-11-14 Dsm Nv Werkwijze voor de bereiding van een alkanol en/of een alkanon.
BE1009662A3 (nl) * 1995-10-13 1997-06-03 Dsm Nv Werkwijze voor het ontleden van cycloalkylhydroperoxide.
US5780683A (en) * 1996-09-11 1998-07-14 Abb Lummus Global Inc. Cyclohexane oxidation
BE1011041A3 (nl) * 1997-03-12 1999-04-06 Dsm Nv Werkwijze voor het ontleden van cycloalkylhydroperoxide.
RU2239624C2 (ru) * 1998-08-26 2004-11-10 Е.И.Дюпон Де Немур Энд Компани Способ разложения гидропероксида
FR2802526B1 (fr) * 1999-12-17 2003-04-18 Rhodia Polyamide Intermediates Procede de preparation de melanges alcools/cetones
US6806390B1 (en) 2000-08-18 2004-10-19 Inuista North America S.àr.l. Hydroperoxide decomposition catalyst
US6700022B2 (en) * 2002-06-05 2004-03-02 E. I. Du Pont De Nemours And Company High yield cyclohexyl hydroperoxide decompostition process
US7091365B2 (en) 2004-03-08 2006-08-15 Abb Lummus Global Inc. Process for olefin epoxidation and co-production of nylon precursor
JP2008513359A (ja) * 2004-08-24 2008-05-01 インヴィスタ テクノロジー エスアエルエル シクロヘキセノン含有有機混合物のシクロヘキセノン含量を低減するための方法
UA95064C2 (en) * 2004-10-27 2011-07-11 ДСМ АйПи АСЕТС Б.В. Process for the preparation of cyclohexanol and cyclohexanone
DE602005024436D1 (de) * 2004-12-22 2010-12-09 Dsm Ip Assets Bv Verfahren zum zersetzen von cyclohexylhydroperoxid
MX2007008983A (es) * 2005-01-25 2007-09-21 Dsm Ip Assets Bv Procedimiento para preparar ciclohexanona y ciclohexanol.
US7491856B2 (en) 2007-06-27 2009-02-17 H R D Corporation Method of making alkylene glycols
US7592493B2 (en) * 2007-06-27 2009-09-22 H R D Corporation High shear process for cyclohexanol production
US8304584B2 (en) 2007-06-27 2012-11-06 H R D Corporation Method of making alkylene glycols
TW200944497A (en) * 2008-04-17 2009-11-01 China Petrochemical Dev Corp System and method for producing naphthenone
CN101607875B (zh) * 2008-06-17 2012-07-25 中国石油化学工业开发股份有限公司 制造环烷酮的方法
EA027382B1 (ru) 2011-12-07 2017-07-31 Кап Iii Б.В. Способ получения смеси, содержащей циклогексанол и циклогексанон
CN103987683B (zh) 2011-12-07 2015-12-02 帝斯曼知识产权资产管理有限公司 包含环己醇和环己酮的混合物的制备方法
US10099985B2 (en) 2014-10-31 2018-10-16 Ube Industries, Ltd. Method for producing ketone and/or alcohol, and system thereof
CN108602736A (zh) * 2015-12-07 2018-09-28 宇部兴产株式会社 制造酮和/或醇的方法及其系统
WO2019201819A1 (en) * 2018-04-17 2019-10-24 Dsm Ip Assets B.V. Oxidation of alkylated p-hydroquinones in aqueous solutions by oxygen
CN110871064B (zh) * 2018-08-29 2022-09-23 中国石油化工股份有限公司 一种碳材料组合处理液及其制备方法、碳材料及其应用

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2070977A5 (es) * 1969-12-12 1971-09-17 Rhone Poulenc Sa
DE2127520A1 (de) * 1971-06-03 1972-12-14 Badische Anilin- & Soda-Fabrik Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Cycloalkanol- und Cycloalkanon-Gemischen
DE2148322B2 (de) * 1971-09-28 1977-02-10 Davy International Ag, 6000 Frankfurt Kreislaufverfahren zur entfernung der bei der partiellen oxidation von cycloalkan entstandenen carbonsaeuren und carbonsaeurederivate aus den erhaltenen oxidationsprodukten
IL43433A (en) * 1972-10-21 1976-09-30 Stamicarbon Process for preparing cycloalkanones and cycloalkanols
JPS5432416A (en) * 1977-08-19 1979-03-09 Sumitomo Chem Co Ltd Treatment of oxidized liquid

Also Published As

Publication number Publication date
PL114149B1 (en) 1981-01-31
JPS6257607B2 (es) 1987-12-02
MX5676E (es) 1983-12-08
EP0004105B1 (en) 1981-08-12
DE2960603D1 (en) 1981-11-12
BR7901214A (pt) 1979-10-02
CS227668B2 (en) 1984-05-14
CA1118453A (en) 1982-02-16
EP0004105A1 (en) 1979-09-19
PL213694A1 (pl) 1979-12-17
AR219789A1 (es) 1980-09-15
US4238415A (en) 1980-12-09
IN150726B (es) 1982-11-27
NL7802125A (nl) 1979-08-28
JPS54135748A (en) 1979-10-22

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Legal Events

Date Code Title Description
FD1A Patent lapsed

Effective date: 20000201